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公开(公告)号:US20230183570A1
公开(公告)日:2023-06-15
申请号:US18076511
申请日:2022-12-07
Applicant: CORNING INCORPORATED
Inventor: Xinyu Cao , Ling Chen , Wanghui Chen , Jiangwei Feng , Robert Randall Hancock, JR. , Yuhui Jin , Aize Li , Meng Shang
Abstract: An etchant comprises: greater than or equal to 20 wt % and less than or equal to 45 wt % ammonium bifluoride; greater than or equal to 0.25 wt % and less than or equal to 10 wt % of a silicon compound; greater than or equal to 5 wt % and less than or equal to 30 wt % hydrochloric acid; greater than or equal to 25 wt % and less than or equal to 60 wt % water; and greater than or equal to 0.5 wt % and less than or equal to 20 wt % of polyhydric alcohol. The silicon compound comprises silica, silica gel, ammonium hexafluorosilicate, potassium hexafluorosilicate, sodium hexafluorosilicate, magnesium hexafluorosilicate, or a combination thereof.
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公开(公告)号:US20230064818A1
公开(公告)日:2023-03-02
申请号:US17893398
申请日:2022-08-23
Applicant: CORNING INCORPORATED
Inventor: Huayun Deng , Melanie Lian Geiger , Richard Allen Hayes , Mingqian He , Yuhui Jin , Govindarajan Natarajan , Weijun Niu , Brian Paul Usiak , David Lee Weidman
IPC: C03C15/00
Abstract: Glass-based substrates are described herein that may be processed by methods including applying a cover article onto a glass-based substrate, submerging the glass-based substrate in an etchant, and maintaining the submersion of the glass-based substrate in the etchant. The glass-based substrate may include a covered surface portion and an exposed surface portion. At least a portion of the covered surface portion may be in direct contact with the cover article. The covered surface portion may not be in contact with the etchant and the exposed surface portion may be in direct contact with the etchant. The etchant may contact the exposed surface portion and the cover article fora time sufficient to etch the exposed surface portion. The cover article may provide a barrier between the etchant and the covered surface portion for the entirety of the submerging.
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公开(公告)号:US11560330B2
公开(公告)日:2023-01-24
申请号:US16767992
申请日:2018-11-29
Applicant: CORNING INCORPORATED
Inventor: Hongmei Hu , Yuhui Jin , Richard Alan Quinn
Abstract: A patterned article that includes: an alkali silicate glass substrate comprising a thickness and a primary surface, the substrate having a bulk composition; a patterned region defined by at least a portion of the primary surface; and a compressive stress region that extends from the at least a portion of the primary surface to a first depth within the substrate. The patterned region comprises a surface roughness (Ra) from about 1 nm to about 600 nm and at least one of a plurality of protrusions and a plurality of depressions. Further, each of the compressive stress region and the patterned region comprises a concentration of at least one alkali metal ion that is different than the concentration of the at least one alkali metal ion in the bulk composition.
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公开(公告)号:US20220348496A1
公开(公告)日:2022-11-03
申请号:US17642432
申请日:2020-09-10
Applicant: CORNING INCORPORATED
Inventor: David Eugene Baker , Albert Joseph Fahey , Qiang Fu , Yuhui Jin , Wei Sun , Ljerka Ukrainczyk , Shelby Kerin Wilson
IPC: C03C21/00
Abstract: Methods for regenerating a salt bath composition include heating the salt bath composition to an ion exchange temperature to form a molten salt bath. The methods may further include contacting at least a portion of an ion-exchangeable article that includes lithium oxide (Li2O) with the molten salt bath. Lithium cations may diffuse from the ion-exchangeable article and into the molten salt bath. Additionally, the methods may include adding a first phosphate salt to the molten salt bath. A lithium phosphate salt that includes at least a portion of the lithium cations may be formed and precipitate from the molten salt bath. Furthermore, the methods may include adding a multivalent salt that includes a multivalent metal cation to the molten salt bath. A second phosphate salt that includes the multivalent metal cation may be formed and precipitate from the molten salt bath.
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公开(公告)号:US20220267201A1
公开(公告)日:2022-08-25
申请号:US17738438
申请日:2022-05-06
Applicant: CORNING INCORPORATED
Inventor: Yuhui Jin , Pascale Oram , Rostislav Vatchev Roussev
IPC: C03C21/00
Abstract: A method of reworking lithium containing ion exchanged glass-based articles is provided. The method includes a reverse ion exchange process that returns the glass-based article to approximately the composition of the glass from which the glass-based article was produced, before being subjected to ion exchange.
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公开(公告)号:US20220267195A1
公开(公告)日:2022-08-25
申请号:US17626223
申请日:2020-07-06
Applicant: CORNING INCORPORATED
Inventor: Haixing Chen , Ling Chen , Jiangwei Feng , Yuhui Jin , Jianqiang Zhu
Abstract: The present disclosure includes a method of making an article including etching a surface of a substrate with an etching suspension comprising an etching cream and glycerin, such that the surface is an anti-glare surface and the article comprises a sparkle of no more than 1%. An article made by the method can include a substrate having a textured surface and comprises a sparkle of no more than 1%.
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公开(公告)号:US20220194844A1
公开(公告)日:2022-06-23
申请号:US16129091
申请日:2018-09-12
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Robert Randall Hancock, JR. , Raymond Chih Chung Hsiao , Yuhui Jin , Aize Li
Abstract: An article that includes: a glass-based substrate comprising a thickness, a primary surface and a compressive stress region that extends from the primary surface to a selected depth; and a textured region defined by the primary surface. The textured region comprises a surface roughness (Ra) of at least 10 nm. The article can also comprise a Knoop Scratch Threshold of at least 9 Newtons (N).
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公开(公告)号:US11352293B2
公开(公告)日:2022-06-07
申请号:US16425290
申请日:2019-05-29
Applicant: CORNING INCORPORATED
Inventor: Yuhui Jin , Pascale Oram , Rostislav Vatchev Roussev
Abstract: A method of reworking lithium containing ion exchanged glass-based articles is provided. The method includes a reverse ion exchange process that returns the glass-based article to approximately the composition of the glass from which the glass-based article was produced, before being subjected to ion exchange.
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公开(公告)号:US11306024B2
公开(公告)日:2022-04-19
申请号:US16886558
申请日:2020-05-28
Applicant: Corning Incorporated
Abstract: A glass article is provided that includes: a glass substrate comprising a thickness and a primary surface; and a textured region defined by the primary surface. The textured region comprises a plurality of sub-surface hillocks, each hillock having a top surface and a base, the base located below the primary surface of the substrate. The plurality of hillocks comprises an average lateral feature size from 0.1 μm to 3 μm and an average height from 5 nm to 200 nm. Further, the primary surface of the substrate is substantially planar.
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公开(公告)号:US20220073411A1
公开(公告)日:2022-03-10
申请号:US17527672
申请日:2021-11-16
Applicant: CORNING INCORPORATED
Inventor: Robert Randall Hancock, JR. , Kelleen Kaye Hughes , Yuhui Jin , Aize Li
IPC: C03C3/083 , C03C17/30 , C03C15/02 , C03C17/32 , C03C21/00 , C03C3/093 , C03C3/091 , C03C3/097 , C03C15/00
Abstract: A textured glass article that includes: a glass substrate comprising a thickness, a primary surface and a bulk composition at the midpoint of the thickness; and a textured region defined by the primary surface and comprising a textured region composition. The textured region comprises a sparkle of 2% or less. Further, the bulk composition comprises about 40 mol % to 80 mol % silica and the textured region composition comprises at least about 40 mol % silica.
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