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公开(公告)号：US11173481B2
公开(公告)日：2021-11-16
申请号：US16534216
申请日：2019-08-07
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY , GLOBAL FRONTIER CENTER FOR MULTISCALE ENERGY SYSTEMS
Inventor： Sung Jong Yoo , Injoon Jang , Hee-Young Park , So Young Lee , Hyun Seo Park , Jin Young Kim , Jong Hyun Jang , Hyoung-Juhn Kim
Abstract: Disclosed are a metal single-atom catalyst and a method for preparing the same. The method uses a minimal amount of chemicals and is thus environmentally friendly compared to conventional chemical and/or physical methods. In addition, the method enables the preparation of a single-atom catalyst in a simple and economical manner without the need for further treatment such as acid treatment or heat treatment. Furthermore, the method is universally applicable to the preparation of single-atom catalysts irrespective of the kinds of metals and supports, unlike conventional methods that suffer from very limited choices of metal materials and supports. Therefore, the method can be widely utilized to prepare various types of metal single-atom catalysts. All metal atoms in the metal single-atom catalyst can participate in catalytic reactions. This optimal atom utilization achieves maximum reactivity per unit mass and can minimize the amount of the metal used, which is very economical.
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公开(公告)号：US10854886B2
公开(公告)日：2020-12-01
申请号：US16268856
申请日：2019-02-06
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Jong Hyun Jang , Hee-Young Park , Jea-woo Jung , Hyoung-Juhn Kim , Dirk Henkensmeier , Sung Jong Yoo , Jin Young Kim , So Young Lee , Hyun Seo Park
IPC: H01M4/92
Abstract: A method for preparing a carbon-supported, platinum-cobalt alloy, nanoparticle catalyst includes mixing a solution containing, in combination, a platinum precursor, a transition metal precursor consisting of a transition metal that is cobalt, carbon, a stabilizer that is oleyl amine, and a reducing agent that is sodium borohydride to provide carbon-supported, platinum-cobalt alloy nanoparticles, and washing the carbon-supported, platinum-cobalt alloy, nanoparticles using ethanol and distilled water individually or in combination followed by drying at room temperature to obtain dried carbon-supported, platinum-cobalt alloy, nanoparticles; treating the dried carbon-supported, platinum-cobalt alloy, nanoparticles with an acetic acid solution having a concentration ranging from 1-16M to provide acetic acid-treated nanoparticles, and washing the acetic acid-treated nanoparticles using distilled water followed by drying at room temperature to obtain dried acetic acid-treated nanoparticles; and heat treating the dried acetic acid-treated nanoparticles at a temperature ranging from 600 to 1000° C. under a hydrogen-containing atmosphere.
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公开(公告)号：US10669640B2
公开(公告)日：2020-06-02
申请号：US15241798
申请日：2016-08-19
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Jong Hyun Jang , Soo-Kil Kim , Sang Hyun Ahn , Hyoung-Juhn Kim , Jin Young Kim , Sung Jong Yoo , Dirk Henkensmeier , Jonghee Han , Jaeyune Ryu
Abstract: Provided is an electrocatalyst for anion exchange membrane water electrolysis, including a carbonaceous material, and nickel electrodeposited on the carbonaceous material, wherein nickel is partially substituted with platinum and the substitution with platinum provides increased hydrogen evolution activity as compared to the same electrocatalyst before substitution with platinum. Also provided are a method for preparing the electrocatalyst and an anion exchange membrane water electrolyzer using the same. The nickel electrocatalyst coated with an ultralow loading amount of platinum for anion exchange membrane water electrolysis shows excellent hydrogen evolution activity and has a small thickness of catalyst, thereby providing high mass transfer and high catalyst availability. In addition, the electrocatalyst uses a particle-type electrode to facilitate emission of hydrogen bubbles generated during hydrogen evolution reaction and oxygen bubbles generated during oxygen evolution reaction, and requires low cost for preparation to provide high cost-efficiency.
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公开(公告)号：US10601052B2
公开(公告)日：2020-03-24
申请号：US15360034
申请日：2016-11-23
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Jong Hyun Jang , Byungseok Lee , Hee-Young Park , Hyoung-Juhn Kim , Dirk Henkensmeier , Sung Jong Yoo , Jin Young Kim , So Young Lee , Jaeyune Ryu , Sung Pil Yoon , Jonghee Han , Suk Woo Nam
Abstract: Disclosed are a reversible fuel cell oxygen electrode in which IrO2 is electrodeposited and formed on a porous carbon material and platinum is applied thereon to form a porous platinum layer, a reversible fuel cell including the same, and a method for preparing the same. According to the corresponding reversible fuel cell oxygen electrode, as the loading amounts of IrO2 and platinum used in the reversible fuel cell oxygen electrode can be lowered, it is possible to exhibit excellent reversible fuel cell performances (excellent fuel cell performance and water electrolysis performance) by improving the mass transport of water and oxygen while being capable of reducing the loading amounts of IrO2 and platinum. Further, it is possible to exhibit a good activity of a catalyst when the present disclosure is applied to a reversible fuel cell oxygen electrode and to reduce corrosion of carbon.
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公开(公告)号：US10396383B2
公开(公告)日：2019-08-27
申请号：US15679562
申请日：2017-08-17
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Hyoung-Juhn Kim , So Young Lee , Jieon Chae , Jong Hyun Jang , Sung Jong Yoo , Jin Young Kim , Hyun Seo Park , Dirk Henkensmeier
IPC: H01M8/1004 , H01M8/1016 , H01M8/04089 , H01M8/04291
Abstract: A membrane electrode assembly includes a cation exchange membrane electrode assembly and an anion exchange membrane electrode assembly. The cation exchange membrane includes a cation exchange membrane, a first cathode electrode disposed on the cation exchange membrane, and a first anode electrode disposed under the cation exchange membrane. The anion exchange membrane electrode assembly includes an anion exchange membrane, a second cathode electrode disposed on the anion exchange membrane, and a second anode electrode disposed under the anion exchange membrane. The cation exchange membrane and the anion exchange membrane partially contact each other, and the first cathode electrode, the first anode electrode, the second cathode electrode, and the second anode electrode do not contact one another.
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Patent Agency Ranking
公开(公告)号：US10367206B2
公开(公告)日：2019-07-30
申请号：US15910290
申请日：2018-03-02
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Sung Jong Yoo , Dong Wook Lee , So Young Lee , Jin Young Kim , Jong Hyun Jang , Hyoung-Juhn Kim , Hyun Seo Park , Gil-Pyo Kim
IPC: H01M4/90 , H01M8/1018 , H01M4/92
Abstract: A method for preparing a metal catalyst supported on a porous carbon support using a plant, including: (a) a step of preparing a plant; (b) a step of preparing a metal precursor-absorbed plant by absorbing a metal precursor into the plant; (c) a step of preparing a catalyst precursor by drying the metal precursor-absorbed plant; (d) a step of preparing a char by charring the catalyst precursor; and (e) a step of preparing a metal catalyst supported on a porous carbon support by treating the char with an acid. The method for preparing a metal catalyst supported on a porous carbon support of the present disclosure, whereby a plant itself is charred, is environment-friendly and allows for convenient large-scale synthesis. The metal catalyst supported on a porous carbon support prepared thereby can be used as electrode materials of various energy devices, particularly as an electrode catalyst of a fuel cell.
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公开(公告)号：US20180202970A1
公开(公告)日：2018-07-19
申请号：US15861998
申请日：2018-01-04
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： So Young LEE , Hyoung-Juhn Kim , Young Seung Na , Jin Young Kim , Sung Jong Yoo , Jong Hyun Jang , Jonghee Han , Suk Woo Nam
Abstract: An ionic conductivity measurement device of an electrolytic membrane includes a humidification chamber configured to accommodate an ion-conductive electrolytic membrane and having concave grooves respectively formed at both sides thereof which face the electrolytic membrane to form a measurement space for measuring ionic conductivity of the electrolytic membrane; a plurality of channels formed at a bottom surface of each of the concave grooves; a gas distribution unit detachably coupled to each of the concave grooves with the electrolytic membrane being interposed therebetween; and a plurality of electrodes provided in contact with one side of the electrolytic membrane and supported by the gas distribution unit, the plurality of electrodes being disposed side by side to measure an impedance of the electrolytic membrane.
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公开(公告)号：US09751078B2
公开(公告)日：2017-09-05
申请号：US14921567
申请日：2015-10-23
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Sung Jong Yoo , Jaeyune Ryu , Jong Hyun Jang , Jin Young Kim , Hyoung-Juhn Kim , Sung Pil Yoon , Jonghee Han , Suk Woo Nam , Tae Hoon Lim
CPC classification number: B01J27/1853 , B01J23/75 , B01J35/06 , B82Y30/00 , C25B1/02 , C25B11/035 , C25B11/0405 , C25B11/0415 , C25B11/0447
Abstract: Disclosed is a non-precious metal based water electrolysis catalyst represented by CoX/C (X is at least one selected from the group consisting of P, O, B, S and N) for evolution of hydrogen and oxygen at a cathode and anode, respectively, at the same time, the catalyst including a cobalt-containing compound fixed to a carbon carrier.
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公开(公告)号：US11695147B2
公开(公告)日：2023-07-04
申请号：US17013918
申请日：2020-09-08
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： So Young Lee , Seung Ju Lee , Hyun Seo Park , Jin Young Kim , Sung Jong Yoo , Jong Hyun Jang , Hyoung-Juhn Kim , Hee-Young Park
IPC: H01M8/1051 , H01M8/1039 , C08K3/32 , C08K7/08 , C08F14/18 , H01M8/10
CPC classification number: H01M8/1051 , C08F14/185 , C08K3/32 , C08K7/08 , H01M8/1039 , C08K2003/328 , C08K2201/003 , C08K2201/011 , H01M2008/1095 , H01M2300/0082
Abstract: Disclosed is an antioxidant for a polymer electrolyte membrane of a fuel cell including cerium hydrogen phosphate (CeHPO4). The presence of cerium hydrogen phosphate in the antioxidant enhances the dissolution stability of cerium and improves the ability to capture water, leading to an increase in proton conductivity. In addition, the cerium hydrogen phosphate has a crystal structure composed of smaller cerium particles. This crystal structure greatly improves the ability of the antioxidant to prevent oxidation of the electrolyte membrane. Also disclosed are an electrolyte membrane including the antioxidant, a fuel cell including the electrolyte membrane, a method for preparing the antioxidant, a method for producing the electrolyte membrane, and a method for fabricating the fuel cell.
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公开(公告)号：US11430996B2
公开(公告)日：2022-08-30
申请号：US16802206
申请日：2020-02-26
Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventor： Sung Jong Yoo , Injoon Jang , Hee-Young Park , So Young Lee , Hyun Seo Park , Jin Young Kim , Jong Hyun Jang , Hyoung-Juhn Kim
Abstract: A method is disclosed for preparing a metal single-atom catalyst for a fuel cell including the steps of depositing metal single atoms to a nitrogen precursor powder, mixing the metal single atom-deposited nitrogen precursor powder with a carbonaceous support, and carrying out heat treatment. The step of depositing metal single atoms is carried out by sputtering, thermal evaporation, E-beam evaporation or atomic layer deposition. The method uses a relatively lower amount of chemical substances as compared to conventional methods, is eco-friendly, and can produce a single-atom catalyst at low cost. In addition, unlike conventional methods which are limited to certain metallic materials, the present method can be applied regardless of the type of metal.
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