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公开(公告)号：US20140187817A1
公开(公告)日：2014-07-03
申请号：US14240547
申请日：2011-09-16
Applicant: Torsten Balduf , Martin Koestner , Wenxing Zhang , Heidi Groen , Axel Hengstermann , Maya Krapfl
Inventor： Torsten Balduf , Martin Koestner , Wenxing Zhang , Heidi Groen , Axel Hengstermann , Maya Krapfl
IPC: C07C51/43
Abstract: The invention relates to a process for preparation of methacrylic acid, comprising process steps a) providing a crude methacrylic acid-comprising aqueous solution comprising at least one impurity at least partially dissolved therein; b) precipitation of at least a part of the at least one impurity from the crude methacrylic acid-comprising aqueous solution to form at least one solid impurity and a mother liquor; c) separation of at least a part of the at least one solid impurity from the mother liquor to obtain a purified methacrylic acid-comprising aqueous solution and a solid impurity; d) separation of methacrylic acid from the purified methacrylic acid-comprising aqueous solution.
Abstract translation: 本发明涉及一种制备甲基丙烯酸的方法，包括方法步骤a）提供包含至少部分溶解于其中的至少一种杂质的含粗甲基丙烯酸的水溶液; b）从含粗甲基丙烯酸的水溶液中沉淀至少一部分所述至少一种杂质以形成至少一种固体杂质和母液; c）从母液中分离出至少一部分固体杂质，得到纯化的含甲基丙烯酸的水溶液和固体杂质; d）从纯化的含甲基丙烯酸的水溶液中分离甲基丙烯酸。
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公开(公告)号：US08445617B2
公开(公告)日：2013-05-21
申请号：US13668899
申请日：2012-11-05
Applicant: Torsten Balduf , Gunther Bub , Jurgen Mosler , Andreas Sabbagh , Jurgen Kohn , Arndt Selbach
Inventor： Torsten Balduf , Gunther Bub , Jurgen Mosler , Andreas Sabbagh , Jurgen Kohn , Arndt Selbach
IPC: C08F220/06 , C08L33/02
Abstract: The invention relates to producing a superabsorbent polymer comprising (I) producing a (meth)acrylic acid comprising the steps of (a) synthesizing a crude (meth)acrylic acid phase; (b) distillatively working-up the crude (meth)acrylic acid phase to obtain a (meth)acrylic acid phase and a dimer phase comprising (meth)acrylic acid dimers and/or (meth)acrylic acid oligomers; (c) splitting at least a part of the (meth)acrylic acid dimers or of the (meth)acrylic acid oligomers or both from the dimer phase to obtain a (meth)acrylic acid-comprising a low boiling phase and a high boiling phase comprising less (meth)acrylic acid than the low boiling phase; (d) separating at least a part of the (meth)acrylic acid from the low boiling phase by forming crystals to obtain a pure (meth)acrylic acid, and a residue; (II) polymerizing a monomer phase comprising the pure (meth)acrylic acid to obtain a polymer phase; and (III) working-up the polymer phase to obtain the polymer.
Abstract translation: 本发明涉及制备超吸收性聚合物，其包括（I）生产（甲基）丙烯酸，其包括以下步骤：（a）合成粗制（甲基）丙烯酸相; （b）蒸馏处理粗（甲基）丙烯酸相以获得（甲基）丙烯酸相和包含（甲基）丙烯酸二聚体和/或（甲基）丙烯酸低聚物的二聚体相; （c）从二聚体相分解至少一部分（甲基）丙烯酸二聚体或（甲基）丙烯酸低聚物或两者，得到包含低沸点相和高沸点相的（甲基）丙烯酸 包括比低沸点相少的（甲基）丙烯酸; （d）通过形成晶体从低沸点相分离出至少一部分（甲基）丙烯酸，得到纯的（甲基）丙烯酸和残余物; （II）使包含纯（甲基）丙烯酸的单体相聚合以获得聚合物相; 和（III）加工聚合物相以获得聚合物。
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公开(公告)号：US08309668B2
公开(公告)日：2012-11-13
申请号：US13461220
申请日：2012-05-01
Applicant: Torsten Balduf , Günther Bub , Jürgen Mosler , Andreas Sabbagh , Jürgen Kohn , Arndt Selbach
Inventor： Torsten Balduf , Günther Bub , Jürgen Mosler , Andreas Sabbagh , Jürgen Kohn , Arndt Selbach
IPC: C08F220/06 , C08L33/02
Abstract: The present invention relates to a process for producing a superabsorbent a polymer comprises (I) producing a pure (meth)acrylic acid comprising the steps of (a) synthesizing a crude (meth)acrylic acid phase; (b) distillatively working-up the crude (meth)acrylic acid phase to obtain a (meth)acrylic acid phase and a dimer phase comprising (meth)acrylic acid dimers or (meth)acrylic acid oligomers or both; (c) splitting at least a part of the (meth)acrylic acid dimers or of the (meth)acrylic acid oligomers or both from the dimer phase to obtain a (meth)acrylic acid-comprising low boiling phase and a high boiling phase comprising less (meth)acrylic acid than the low boiling phase; (d) separating at least a part of the (meth)acrylic acid from the low boiling phase to obtain a pure (meth)acrylic acid, and a residue; (II) polymerizing a monomer phase comprising the pure (meth)acrylic acid to obtain a polymer phase; and (III) working-up the polymer phase to obtain the polymer.
Abstract translation: 本发明涉及聚合物的超吸收剂的制造方法，其特征在于：（I）制造纯（甲基）丙烯酸，其特征在于，包括：（a）合成粗制（甲基）丙烯酸相的工序; （b）蒸馏处理粗（甲基）丙烯酸相以获得（甲基）丙烯酸相和包含（甲基）丙烯酸二聚体或（甲基）丙烯酸低聚物或二者的二聚体相; （c）从二聚体相分离至少一部分（甲基）丙烯酸二聚体或（甲基）丙烯酸低聚物或两者，得到包含（甲基）丙烯酸的低沸点相和高沸点相，包括 较少（甲基）丙烯酸低于低沸点相; （d）从低沸点相分离出至少一部分（甲基）丙烯酸，得到纯（甲基）丙烯酸，残渣; （II）使包含纯（甲基）丙烯酸的单体相聚合以获得聚合物相; 和（III）加工聚合物相以获得聚合物。
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公开(公告)号：US07964689B2
公开(公告)日：2011-06-21
申请号：US12880633
申请日：2010-09-13
Applicant: Stefan Nordhoff , Axel Kobus , Stefan Gross , Hans-Rolf Lausch , Torsten Balduf , Roland Fornika , Guenther Bub
Inventor： Stefan Nordhoff , Axel Kobus , Stefan Gross , Hans-Rolf Lausch , Torsten Balduf , Roland Fornika , Guenther Bub
Abstract: The invention relates to a superabsorbent polymer that includes a (meth)acrylic acid made by a process that comprises the following process steps: a) (meth)acrylic acid is crystallized out from a mother liquor; b) crystallized (meth)acrylic acid is separated from the mother liquor; c) at least part of the separated (meth)acrylic acid crystals are melted; d) the melted part is at least partially recycled to the step a) or step b). The superabsorbent polymer according to the present invention includes an process to make (meth)acrylic acid, the apparatus suitable for implementing the process, and the use of the apparatus for the production of (meth)acrylic acid characterized by a high purity of the thereby obtainable (meth)acrylic acid as well as by a high efficiency with regard to the achievable yield and necessary energy requirement, thereby providing an improved superabsorbent polymer.
Abstract translation: 本发明涉及一种超吸收性聚合物，其包含通过包括以下工艺步骤的方法制备的（甲基）丙烯酸：a）（甲基）丙烯酸从母液中结晶出来; b）结晶的（甲基）丙烯酸与母液分离; c）至少部分分离的（甲基）丙烯酸晶体熔融; d）熔化的部分至少部分地再循环到步骤a）或步骤b）。 根据本发明的超吸收性聚合物包括制备（甲基）丙烯酸的方法，适用于实施该方法的装置，以及用于生产特征在于其高纯度的（甲基）丙烯酸的装置的用途 可获得的（甲基）丙烯酸，以及关于可实现的产率和所需的能量需求的高效率，从而提供改进的超吸收性聚合物。
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Patent Agency Ranking
公开(公告)号：US20110028664A1
公开(公告)日：2011-02-03
申请号：US12880633
申请日：2010-09-13
Applicant: Stefan Nordhoff , Axel Kobus , Stefan Gross , Hans-Rolf Lausch , Torsten Balduf , Roland Fornika , Guenther Bub
Inventor： Stefan Nordhoff , Axel Kobus , Stefan Gross , Hans-Rolf Lausch , Torsten Balduf , Roland Fornika , Guenther Bub
IPC: C08F2/00
Abstract: The invention relates to a superabsorbent polymer that includes a (meth)acrylic acid made by a process that comprises the following process steps: a) (meth)acrylic acid is crystallized out from a mother liquor; b) crystallized (meth)acrylic acid is separated from the mother liquor; c) at least part of the separated (meth)acrylic acid crystals are melted; d) the melted part is at least partially recycled to the step a) or step b). The superabsorbent polymer according to the present invention includes an process to make (meth)acrylic acid, the apparatus suitable for implementing the process, and the use of the apparatus for the production of (meth)acrylic acid characterized by a high purity of the thereby obtainable (meth)acrylic acid as well as by a high efficiency with regard to the achievable yield and necessary energy requirement, thereby providing an improved superabsorbent polymer.
Abstract translation: 本发明涉及一种超吸收性聚合物，其包含通过包括以下工艺步骤的方法制备的（甲基）丙烯酸：a）（甲基）丙烯酸从母液中结晶出来; b）结晶的（甲基）丙烯酸与母液分离; c）至少部分分离的（甲基）丙烯酸晶体熔融; d）熔化的部分至少部分地再循环到步骤a）或步骤b）。 根据本发明的超吸收性聚合物包括制备（甲基）丙烯酸的方法，适用于实施该方法的装置，以及用于生产特征在于其高纯度的（甲基）丙烯酸的装置的用途 可获得的（甲基）丙烯酸，以及关于可实现的产率和所需的能量需求的高效率，从而提供改进的超吸收性聚合物。
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46.发明授权(Meth)acrylic acid crystal and process for producing aqueous (meth)acrylic acid 有权（甲基）丙烯酸晶体和制备（甲基）丙烯酸水溶液的方法公开(公告)号：US07557245B2
公开(公告)日：2009-07-07
申请号：US10507969
申请日：2003-03-17
Applicant: Stefan Nordhoff , Torsten Balduf , Gunther Bub , Roland Fornika , Jurgen Mosler , Thomas Rathke , Axel Kobus , Dennis Thong
Inventor： Stefan Nordhoff , Torsten Balduf , Gunther Bub , Roland Fornika , Jurgen Mosler , Thomas Rathke , Axel Kobus , Dennis Thong
IPC: C07C51/42
Abstract: The present invention relates to processes for purifying a composition containing (meth)acrylic acid, at least one impurity and water, wherein the composition has a water content in the range of 0.55 to 90, based on the composition, to form a purified phase containing (meth)acrylic acid and at least one impurity, wherein, in the purified phase, the quantity of at least one impurity is less than 7% by weight, based on (meth)acrylic acid in the purified phase.
Abstract translation: 本发明涉及基于组合物纯化含有（甲基）丙烯酸，至少一种杂质和水的组合物的方法，其中组合物的水含量基于组合物为0.55至90，以形成含有 （甲基）丙烯酸和至少一种杂质，其中，在纯化相中，基于纯化相中的（甲基）丙烯酸，至少一种杂质的量小于7重量％。
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47.发明申请Process for Production of (Meth)Acrylic Acid with High Boiling Fraction Work-Up By Means of Crystallization 有权通过结晶法生产具有高沸点馏分的（甲基）丙烯酸的方法公开(公告)号：US20080287616A1
公开(公告)日：2008-11-20
申请号：US12063949
申请日：2006-08-11
Applicant: Torsten Balduf , Gunther Bub , Jurgen Mosler , Andreas Sabbagh , Jurgen Kohn , Arndt Selbach
Inventor： Torsten Balduf , Gunther Bub , Jurgen Mosler , Andreas Sabbagh , Jurgen Kohn , Arndt Selbach
IPC: C08F120/06 , C08F2/00 , B01J19/00 , C07C51/44
Abstract: A process for production of (meth)acrylic acid is disclosed. The process includes synthesizing and distillatively working-up a crude (meth)acrylic acid phase to obtain a (meth)acrylic acid phase and a dimer phase including (meth)acrylic acid dimers and/or (meth)acrylic acid oligomers. At least a part of the (meth)acrylic acid dimers and/or of the (meth)acrylic acid oligomers from the dimer phase is split to obtain a (meth)acrylic acid including a low-boiling phase and a high-boiling phase including less (meth)acrylic acid than the low-boiling phase. At least a part of the (meth)acrylic acid from the low-boiling phase is separated by forming of one or more crystals to obtain a pure (meth)acrylic acid and a residue. Also disclosed is a device for production of (meth)acrylic acid, a process for production of a polymer as well as chemical products based on or including (meth)acrylic acid or a polymer as well as the use of (meth)acrylic acid or polymers in chemical products.
Abstract translation: 公开了（甲基）丙烯酸的生产方法。 该方法包括合成和蒸馏处理粗（甲基）丙烯酸相以获得（甲基）丙烯酸相和包含（甲基）丙烯酸二聚体和/或（甲基）丙烯酸低聚物的二聚体相。 （甲基）丙烯酸二聚体和/或来自二聚体相的（甲基）丙烯酸低聚物的至少一部分被分裂，得到包含低沸点相和高沸点相的（甲基）丙烯酸，包括 （甲基）丙烯酸低于低沸点相。 通过形成一种或多种晶体将至少一部分来自低沸点相的（甲基）丙烯酸分离，得到纯的（甲基）丙烯酸和残余物。 还公开了用于生产（甲基）丙烯酸的装置，聚合物的制造方法以及基于（或）（甲基）丙烯酸或聚合物的化学产品，以及使用（甲基）丙烯酸或 化学产品中的聚合物。
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48.发明授权Process and device for carrying out reactions in reactor with slot-shaped reaction spaces 失效在具有槽形反应空间的反应器中进行反应的方法和装置公开(公告)号：US07332139B2
公开(公告)日：2008-02-19
申请号：US09934085
申请日：2001-08-22
Applicant: Rüdiger Schütte , Torsten Balduf , Catrin Becker , Ina Hemme , Birgit Bertsch-Frank , Werner Wildner , Jürgen Rollmann , Georg Markowz
Inventor： Rüdiger Schütte , Torsten Balduf , Catrin Becker , Ina Hemme , Birgit Bertsch-Frank , Werner Wildner , Jürgen Rollmann , Georg Markowz
CPC classification number: F28F3/12 , B01F5/0403 , B01F13/0059 , B01F15/00935 , B01F2215/0036 , B01J19/0093 , B01J19/249 , B01J2208/022 , B01J2219/00265 , B01J2219/00835 , B01J2219/0086 , B01J2219/00889 , B01J2219/2453 , B01J2219/2458 , B01J2219/2462 , B01J2219/2465 , B01J2219/2467 , B01J2219/2479 , B01J2219/2481 , B01J2219/2485 , B01J2219/2487 , B01J2219/2493 , B01J2219/2495 , B01J2219/2497 , B01J2219/2498 , C01B15/029 , C07C45/35 , C07C51/252 , C07D301/12 , F28D9/0081 , C07C47/22 , C07C57/04
Abstract: Reactions between at least two fluid reactants are performed in a reactor comprising wall elements (1), slot-shaped reaction spaces (3) and cavities (5) for conducting a fluid heat-carrier through. Depending on the process and throughput, a modular structural design is chosen wherein an arbitrary number of wall elements (1) are assembled to a right-parallelepipedal block (24), the reaction spaces (3) are formed between lateral surfaces (2) of right-parallelepipedal wall elements (1), the reactants are introduced into the reaction spaces (3) from edge regions of one side of the block (24) and are conducted through the reaction spaces (3) in parallel flows and the fluid heat-carrier is conducted through the tubular cavities (5) extending in the interior of the wall elements (1).
Abstract translation: 在包括壁元件（1），槽形反应空间（3）和空腔（5）的反应器中进行至少两种流体反应物之间的反应，用于使流体热载体通过。 根据工艺和生产量，选择模块化结构设计，其中任意数量的壁元件（1）组装到右平行六面体块（24），反作用空间（3）形成在 右平行六面体壁元件（1），将反应物从块体（24）的一侧的边缘区域引入反应空间（3）中，并通过平行流动的反应空间（3） 载体通过在壁元件（1）的内部延伸的管状空腔（5）进行。
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公开(公告)号：US20060276334A1
公开(公告)日：2006-12-07
申请号：US10566453
申请日：2004-07-30
Applicant: Torsten Balduf , Armin Lange De Oliveira , Werner Burkhardt , Guido Stochniol
Inventor： Torsten Balduf , Armin Lange De Oliveira , Werner Burkhardt , Guido Stochniol
IPC: B01J21/04
CPC classification number: C07C45/35 , B01J19/249 , B01J19/32 , B01J23/30 , B01J32/00 , B01J37/0203 , B01J37/0225 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2479 , B01J2219/2485 , B01J2219/3221 , B01J2219/32213 , B01J2219/32227 , B01J2219/32408 , B01J2219/32466 , B01J2219/32475 , C07C51/252 , F28F3/14 , C07C47/22 , C07C57/04
Abstract: A catalyst support including a body having a surface and a coating bonded to the surface is disclosed. The coating includes fissures exhibiting a total fissure length of at least about 500 m/m2 and an adhesive tensile strength of at least about 500 N/m2. Using a catalyst support body to serve in the catalytic reaction of reactants, for example, in a partial oxidation of propene and acrolein to acrolein and acrylic acid, is disclosed. Also disclosed are processes for the: (a) production of a coating for a catalyst support body, (b) preparation of an organic molecule containing at least one double bond and oxygen, (c) production of a water-absorbing polymer, and (d) production of a water-absorbing hygiene article, and chemical products or the use of (meth)acrylic acid in chemical products.
Abstract translation: 公开了一种催化剂载体，其包括具有表面的主体和与表面结合的涂层。 涂层包括表现出至少约500m / m 2的总裂缝长度和至少约500N / m 2的粘合抗拉强度的裂缝。 使用催化剂载体用于反应物的催化反应，例如，将丙烯和丙烯醛部分氧化成丙烯醛和丙烯酸。 还公开了以下方法：（a）生产催化剂载体的涂层，（b）制备含有至少一个双键和氧的有机分子，（c）制备吸水聚合物和（ d）生产吸水卫生用品，化学制品或化学产品中使用（甲基）丙烯酸。
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