公开(公告)号：US20110297450A1

公开(公告)日：2011-12-08

申请号：US13141042

申请日：2009-12-18

Applicant: Antionette Can ,  Geoffrey John Davies ,  Johannes Lodewikus Myburgh

Inventor： Antionette Can ,  Geoffrey John Davies ,  Johannes Lodewikus Myburgh

IPC: E21B10/36 ,  B01J3/06 ,  B24D3/04

CPC classification number: C04B35/62886 ,  A61F2/0059 ,  A61F2/78 ,  C04B35/528 ,  C04B35/5831 ,  C04B35/6265 ,  C04B35/62818 ,  C04B35/62831 ,  C04B35/645 ,  C04B2235/3217 ,  C04B2235/3839 ,  C04B2235/3886 ,  C04B2235/427 ,  C04B2235/786 ,  C09K3/1409 ,  C23C28/027 ,  C23C28/324 ,  C23C28/347 ,  C23C30/005

Abstract: The invention provides for an ultra hard or hard composite material comprising a primary ultra hard or hard particulate material and at least one secondary ultra hard or hard particulate material dispersed in a matrix material. The primary ultra hard or hard particulate material has a thermal expansion coefficient lower than that of the matrix material and the at least one secondary ultra hard or hard particulate material has a thermal expansion coefficient greater than that of the matrix material.

Abstract translation: 本发明提供一种超硬或硬复合材料，其包含主要的超硬或硬颗粒材料和分散在基体材料中的至少一种次级超硬或硬颗粒材料。 初级超硬或硬颗粒材料的热膨胀系数低于基体材料的热膨胀系数，并且至少一种次级超硬或硬颗粒材料的热膨胀系数大于基体材料的热膨胀系数。

公开(公告)号：US20110283629A1

公开(公告)日：2011-11-24

申请号：US13111333

申请日：2011-05-19

Applicant: Thomas Charles Easley

Inventor： Thomas Charles Easley

IPC: B24D3/04 ,  B24D18/00 ,  B01J3/06

CPC classification number: C04B35/52 ,  C04B35/6316 ,  C04B35/645 ,  C04B2235/3826 ,  C04B2235/386 ,  C04B2235/3865 ,  C04B2235/3873 ,  C04B2235/40 ,  C04B2235/404 ,  C04B2235/408 ,  C04B2235/427 ,  C04B2235/428 ,  C04B2235/5436 ,  C04B2235/5472 ,  C04B2235/5481 ,  C04B2235/616 ,  C04B2235/656 ,  C04B2235/6567 ,  C04B2235/6587 ,  C04B2235/721 ,  C04B2235/728 ,  C04B2235/77 ,  C04B2235/786 ,  C04B2235/80 ,  C04B2235/96

Abstract: The present disclosure provides a silicon carbide (SiC) bonded diamond compact having less than about 2 weight % unreacted Si and less than about 1 weight % graphite, as well as processes for making the same.

Abstract translation: 本公开内容提供了具有小于约2重量％的未反应的Si和小于约1重量％的石墨的碳化硅（SiC）结合的金刚石复合体，以及制备它们的方法。

公开(公告)号：US20110247278A1

公开(公告)日：2011-10-13

申请号：US13085089

申请日：2011-04-12

Applicant: Madapusi K. Keshavan ,  Ronald K. Eyre ,  Anthony Griffo ,  Peter Thomas Cariveau

Inventor： Madapusi K. Keshavan ,  Ronald K. Eyre ,  Anthony Griffo ,  Peter Thomas Cariveau

IPC: B24D3/10 ,  B01J3/06

CPC classification number: E21B10/55 ,  C22C1/05 ,  C22C26/00 ,  C22C2204/00 ,  E21B10/5673

Abstract: A method for making a polycrystalline diamond construction is disclosed, which includes the steps of treating a polycrystalline diamond body having a plurality of bonded together diamond crystals and a solvent catalyst material to remove the solvent catalyst material therefrom, wherein the solvent catalyst material is disposed within interstitial regions between the bonded together diamond crystals, replacing the removed solvent catalyst material with a replacement material, and treating the body having the replacement material to remove substantially all of the replacement material from a first region of the body extending a depth from a body surface, and allowing the remaining amount of the replacement material to reside in a second region of the body that is remote from the surface.

Abstract translation: 公开了一种制造多晶金刚石结构的方法，其包括以下步骤：处理具有多个结合在一起的金刚石晶体的多晶金刚石体和溶剂催化剂材料，以从其中除去溶剂催化剂材料，其中溶剂催化剂材料置于 接合在一起的金刚石晶体之间的间隙区域，用替换材料代替去除的溶剂催化剂材料，以及处理具有替换材料的主体，以从身体的第一区域移除基本上所有的替代材料，该第一区域从身体表面延伸深度 并且允许剩余量的替换材料驻留在远离表面的身体的第二区域中。

公开(公告)号：US20110189468A1

公开(公告)日：2011-08-04

申请号：US13085689

申请日：2011-04-13

Applicant: Kenneth E. Bertagnolli ,  Jiang Qian ,  Jason Wiggins ,  Michael A. Vail ,  Debkumar Mukhopadhyay

Inventor： Kenneth E. Bertagnolli ,  Jiang Qian ,  Jason Wiggins ,  Michael A. Vail ,  Debkumar Mukhopadhyay

IPC: B24D3/10 ,  B24D3/06 ,  C09K3/14 ,  B01J3/06

CPC classification number: C04B37/001 ,  B21C3/025 ,  B24D18/0009 ,  C04B2237/36 ,  C04B2237/363 ,  C22C26/00 ,  E21B10/567 ,  F16C17/02 ,  F16C17/04 ,  F16C33/043 ,  F16C33/26 ,  F16C2206/04 ,  F16C2206/82 ,  F16C2220/20 ,  F16C2240/40 ,  F16C2240/48 ,  F16C2352/00 ,  G01N27/72 ,  G01N27/80 ,  Y10T428/24058 ,  Y10T428/24997 ,  Y10T428/25 ,  Y10T428/252 ,  Y10T428/30

Abstract: Embodiments of the invention relate to polycrystalline diamond (“PCD”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, PCD includes a plurality of diamond grains defining a plurality of interstitial regions. A metal-solvent catalyst occupies at least a portion of the plurality of interstitial regions. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit a coercivity of about 115 Oersteads or more and a specific magnetic saturation of about 15 Gauss·cm3/grams or less. Other embodiments are directed to polycrystalline diamond compacts (“PDCs”) employing such PCD, methods of forming PCD and PDCs, and various applications for such PCD and PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.

Abstract translation: 本发明的实施方案涉及显示增强的金刚石 - 金刚石键合的多晶金刚石（“PCD”）。 在一个实施例中，PCD包括限定多个间隙区域的多个金刚石晶粒。 金属溶剂催化剂占据多个间隙区域的至少一部分。 多个金刚石晶粒和金属 - 溶剂催化剂共同表现出约115奥斯特德或更高的矫顽磁力和约15高斯·cm 3 /克或更低的特定磁饱和度。 其他实施方案涉及采用这种PCD的多晶金刚石压块（“PDC”），形成PCD和PDC的方法，以及用于旋转钻头，轴承装置和拉丝模具中的这种PCD和PDC的各种应用。

公开(公告)号：US20110088954A1

公开(公告)日：2011-04-21

申请号：US12901253

申请日：2010-10-08

Applicant: Anthony A. DiGiovanni ,  Danny E. Scott

Inventor： Anthony A. DiGiovanni ,  Danny E. Scott

IPC: E21B10/00 ,  E21B10/36 ,  B24D3/04 ,  B24D18/00 ,  B01J3/06

CPC classification number: E21B10/56 ,  B24D18/0009 ,  C01B32/25 ,  C04B35/52 ,  C04B35/6303 ,  C04B35/645 ,  C04B2235/3839 ,  C04B2235/3856 ,  C04B2235/3886 ,  C04B2235/427 ,  C22C26/00 ,  E21B10/36 ,  E21B10/54 ,  E21B10/567 ,  Y10T428/25

Abstract: Polycrystalline compacts include non-catalytic nanoparticles in interstitial spaces between interbonded grains of hard material in a polycrystalline hard material. Cutting elements and earth-boring tools include such polycrystalline compacts. Methods of forming polycrystalline compacts include sintering hard particles and non-catalytic nanoparticles to form a polycrystalline material. Methods of forming cutting elements include infiltrating interstitial spaces between interbonded grains of hard material in a polycrystalline material with a plurality of non-catalytic nanoparticles.

Abstract translation: 多晶压块包括在多晶硬质材料中的硬质材料的键合间的间隙中的非催化纳米颗粒。 切割元件和钻孔工具包括这种多晶压块。 形成多晶压块的方法包括烧结硬颗粒和非催化纳米颗粒以形成多晶材料。 形成切割元件的方法包括在多晶材料中与多种非催化纳米颗粒之间的硬质材料的结合晶粒之间的渗透间隙。

公开(公告)号：US07862792B2

公开(公告)日：2011-01-04

申请号：US12087279

申请日：2005-12-30

Applicant: Valery Yurievich Dolmatov

Inventor： Valery Yurievich Dolmatov

IPC: B01J3/06 ,  B22F3/08

CPC classification number: B01J3/08 ,  C01B32/05

Abstract: The invention relates to carbon chemistry and is embodied in the form of a diamond-carbon material, in which carbon is contained in the form a diamond cubic modification and in a roentgen-amorphous phase at a ratio of (40-80):(60-20) in terms of a carbon mass, respectively, wherein the inventive material comprises 89.1-95.2 mass % carbon, 1.2-5.0 mass % nitrogen, 0.1-4.7 mass % oxygen and 0.1-1.5 mass % fire-resisting impurities. The inventive method for producing said material consisting in detonating, in a closed space of a carbon-inert gas medium, a carbon-containing oxygen-deficient explosive material, which is placed in a condensed phase envelop containing a reducing agent at a quantitative ratio between said reducing agent mass in the condensed phase and the mass of the used carbon-containing explosive material equal to or greater than 0.01:1. A method for processing the samples of diamond-carbon material produced by means of a detonation synthesis for examining the elemental composition thereof is also disclosed.

Abstract translation: 本发明涉及碳化学，并且以金刚石碳材料的形式实施，其中碳以菱形立方体形式包含，并且在（40-80）：60（60-80）的比率的罗恩 - 非晶相中 -20），其中本发明的材料包含89.1-95.2质量％的碳，1.2-5.0质量％的氮，0.1-4.7质量％的氧和0.1-1.5质量％的耐火杂质。 用于生产所述材料的本发明方法包括在碳惰性气体介质的封闭空间内引发含碳缺氧的炸药，其以含有还原剂的冷凝相包裹物的量定为比例 所述冷凝相中的还原剂物质和所使用的含碳爆炸物质的质量等于或大于0.01:1。 还公开了一种用于处理通过用于检查其元素组成的爆炸合成产生的金刚石碳材料的样品的方法。

公开(公告)号：US20100294571A1

公开(公告)日：2010-11-25

申请号：US12784460

申请日：2010-05-20

Applicant: J. Daniel Belnap ,  Georgiy Voronin ,  Feng Yu ,  Peter T. Cariveau ,  Youhe Zhang ,  Yuelin Shen ,  Guodong Zhan

Inventor： J. Daniel Belnap ,  Georgiy Voronin ,  Feng Yu ,  Peter T. Cariveau ,  Youhe Zhang ,  Yuelin Shen ,  Guodong Zhan

IPC: E21B10/46 ,  C09K3/14 ,  B01J3/06

CPC classification number: E21B10/567 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2998/10 ,  B22F2999/00 ,  B24D3/10 ,  C22C26/00 ,  C22C2026/006 ,  E21B10/55 ,  E21B10/5735 ,  B22F7/062 ,  B22F3/14 ,  B22F2003/244 ,  B22F2207/01 ,  B22F2207/13 ,  B22F2207/17

Abstract: The present disclosure relates to cutting elements incorporating polycrystalline diamond bodies used for subterranean drilling applications, and more particularly, to polycrystalline diamond bodies having a high diamond content which are configured to provide improved properties of thermal stability and wear resistance, while maintaining a desired degree of impact resistance, when compared to prior polycrystalline diamond bodies. In various embodiments disclosed herein, a cutting element with high diamond content includes a modified PCD structure and/or a modified interface (between the PCD body and a substrate), to provide superior performance.

Abstract translation: 本发明涉及包含用于地下钻井应用的多晶金刚石体的切割元件，更具体地，涉及具有高金刚石含量的多晶金刚石体，其被配置为提供改善的热稳定性和耐磨性能，同时保持期望程度 与现有的多晶金刚石体相比，具有耐冲击性。 在本文公开的各种实施例中，具有高金刚石含量的切割元件包括改性的PCD结构和/或改性界面（在PCD体和基底之间），以提供优异的性能。

公开(公告)号：US20100005728A1

公开(公告)日：2010-01-14

申请号：US12499679

申请日：2009-07-08

Applicant: FEDERICO BELLIN

Inventor： FEDERICO BELLIN

IPC: C09K3/14 ,  B01J3/06 ,  C01B21/064

CPC classification number: B01J3/062 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0685

Abstract: The present invention relates to polycrystalline ultra hard material cutting elements, and more particularly to a method of forming a polycrystalline ultra hard material cutting element with a thicker ultra hard layer than cutting elements formed by prior art methods. In an exemplary embodiment, such a method includes pre-sintering the ultra hard material powder to form an ultra hard material layer that is partially or fully densified prior to HPHT sintering, so that the ultra hard layer is pre-shrunk. This pre-sintering in an exemplary embodiment is achieved by means of a spark plasma process, or in another exemplary embodiment by a microwave sintering process.

Abstract translation: 本发明涉及多晶超硬材料切割元件，更具体地涉及一种形成具有比通过现有技术形成的切割元件更厚的超硬层的多晶超硬材料切割元件的方法。 在一个示例性实施例中，这种方法包括预烧结超硬材料粉末以形成在HPHT烧结之前部分或完全致密化的超硬材料层，使得超硬层被预收缩。 在示例性实施例中的这种预烧结通过火花等离子体工艺实现，或者在另一示例性实施例中通过微波烧结工艺实现。

公开(公告)号：US07615203B2

公开(公告)日：2009-11-10

申请号：US10584927

申请日：2005-05-26

Applicant: Yoshiyuki Yamamoto ,  Kiichi Meguro ,  Takahiro Imai

Inventor： Yoshiyuki Yamamoto ,  Kiichi Meguro ,  Takahiro Imai

IPC: C30B23/00 ,  C30B17/00 ,  B01J3/06 ,  B32B9/00 ,  D06N7/04 ,  H05H1/24 ,  H01L31/0312

CPC classification number: C30B25/105 ,  C30B25/20 ,  C30B29/04 ,  Y10T428/24355

Abstract: A single crystal diamond grown by vapor phase synthesis, wherein when one main surface is irradiated with a linearly polarized light considered to be the synthesis of two mutually perpendicular linearly polarized light beams, the phase difference between the two mutually perpendicular linearly polarized light beams exiting another main surface on the opposite side is, at a maximum, not more than 50 nm per 100 μm of crystal thickness over the entire crystal. This single crystal diamond is of a large size and high quality unattainable up to now, and has characteristics that are extremely desirable in semiconductor device substrates and are applied to optical components of which low strain is required.

Abstract translation: 通过气相合成生长的单晶金刚石，其中当被认为是两个相互垂直的线偏振光的合成的线偏振光照射一个主表面时，两个相互垂直的线偏振光束离开另一个的相位差 在整个晶体上，相对侧的主表面最大为每100微米的晶体厚度不大于50nm。 这种单晶金刚石迄今为止不具有大尺寸和高质量，并且具有在半导体器件基板中非常需要的特性，并且被应用于需要低应变的光学部件。

公开(公告)号：US20090260895A1

公开(公告)日：2009-10-22

申请号：US12148927

申请日：2008-04-22

Applicant: Michael A. Vail ,  Kenneth E. Bertagnolli ,  Jason Wiggins ,  Jiang Qian ,  David P. Miess

Inventor： Michael A. Vail ,  Kenneth E. Bertagnolli ,  Jason Wiggins ,  Jiang Qian ,  David P. Miess

IPC: E21B10/46 ,  B01J3/06 ,  C09K3/14 ,  B29C43/50

CPC classification number: E21B10/46 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685

Abstract: Embodiments relate to methods of fabricating PCD materials by subjecting a mixture that exhibits a broad diamond particle size distribution to a HPHT process, PCD materials so-formed, and PDCs including a polycrystalline diamond table comprising such PCD materials. In an embodiment, a method includes subjecting a mixture to heat and pressure sufficient to form a PCD material. The mixture comprises a plurality of diamond particles exhibiting a diamond particle size distribution characterized, in part, by a parameter θ that is less than about 1.0, where θ = x 6 · σ , x is the average particle size of the diamond particle size distribution, and σ is the standard deviation of the diamond particle size distribution. In an embodiment, the diamond particle size distribution can be generally modeled by the following equation: CPFT 100 = D n - D S n D L n - D S n , wherein CPFT is the cumulative percent finer than, D is diamond grain size, DL is the largest-sized diamond grain, DS is the smallest-sized diamond grain, and n is a distribution modulus.

Abstract translation: 实施方案涉及通过使表现出宽金刚石粒度分布的混合物经历HPHT方法，所形成的PCD材料以及包括包含这种PCD材料的多晶金刚石台的PDC来制造PCD材料的方法。 在一个实施方案中，一种方法包括使混合物经受足以形成PCD材料的热和压力。 该混合物包括多个金刚石颗粒，其具有金刚石颗粒尺寸分布，其部分表征为参数θ小于约1.0，其中θ= x 6。 sigma，x是金刚石粒度分布的平均粒度，σ是金刚石粒度分布的标准偏差。 在一个实施方案中，金刚石粒度分布通常可以通过以下等式建模：CPFT 100 = D n -DS n DL n-DS n，其中CPFT是比D更精细的累积百分比，D是金刚石晶粒尺寸，DL是 最大尺寸的金刚石颗粒，DS是最小尺寸的金刚石颗粒，n是分布模量。