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公开(公告)号：US20180179067A1
公开(公告)日：2018-06-28
申请号：US15740371
申请日：2016-06-21
Inventor： Ryutaro WADA , Masaya UEDA
CPC classification number: C01B32/26 , B01J2/00 , B01J2/003 , B01J3/08 , B05D1/10 , B05D1/40 , C01B32/10 , C01B32/205 , C08K9/02 , C09C1/00 , C09K3/00 , C23C4/067 , C23C4/18 , C23C18/52 , C23C24/02 , C23C24/04
Abstract: In a coated particle, a surface of a base material particle is coated with a carbon particle. The carbon particle is produced by disposing an explosive substance with a detonation velocity of 6,300 m/sec or higher in a periphery of a raw material substance containing an aromatic compound having two or less nitro groups, and detonating the explosive substance.
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公开(公告)号：US09993796B2
公开(公告)日：2018-06-12
申请号：US14669463
申请日：2015-03-26
Applicant: Honeywell International Inc.
Inventor： Stephen A. Cottrell
IPC: B01J19/00 , B01J19/02 , B01J19/18 , B01J19/26 , B01F7/00 , C07C17/00 , C07C17/25 , C07C17/38 , C07C17/383 , C07C21/00 , C07C21/02 , C07C21/18 , C07C21/185 , B01J3/08 , C07C17/093
CPC classification number: B01J19/02 , B01F7/00033 , B01J3/08 , B01J19/006 , B01J19/0066 , B01J19/0073 , B01J19/18 , B01J19/26 , B01J2219/00006 , B01J2219/0004 , B01J2219/00094 , B01J2219/00123 , B01J2219/00162 , B01J2219/0218 , B01J2219/0263 , B01J2219/0277 , C07C17/093 , C07C17/25 , C07C17/38 , C07C17/383 , C07C21/185 , Y02P20/149 , C07C21/18
Abstract: Disclosed are a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.
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3.发明授权Continuous process for nanomaterial synthesis from simultaneous emulsification and detonation of an emulsion 有权用于纳米材料合成的连续方法，从乳液的同时乳化和引爆公开(公告)号：US09327257B2
公开(公告)日：2016-05-03
申请号：US13880309
申请日：2011-10-18
Applicant: Sílvio Manuel Pratas Da Silva , João Manuel Calado Da Silva
IPC: B01J3/08 , B82Y30/00 , B82Y40/00 , C01B13/32 , C01F7/16 , C01G23/047 , C01G45/12 , C04B35/01 , C04B35/443 , C06B23/00 , C06B47/14
CPC classification number: B01J3/08 , B82Y30/00 , B82Y40/00 , C01B13/328 , C01F7/162 , C01G23/047 , C01G45/1242 , C01P2002/32 , C01P2004/64 , C01P2006/12 , C04B35/016 , C04B35/443 , C04B2235/3203 , C04B2235/3222 , C04B2235/5454 , C06B23/00 , C06B47/145
Abstract: The present invention refers to a continuous process for in secco nanomaterial synthesis from the emulsification and detonation of an emulsion. The said process combines the simultaneous emulsification and detonation operations of the emulsion, thus assuring a production yield superior to 100 kg/h. When guaranteeing that the sensitization of the emulsion occurs mainly upon its feeding into the reactor, it is possible to avoid the accumulation of any class-1 substances along the entire synthesis process, thus turning it into an intrinsically safe process. Afterwards, dry collection of the nanomaterial avoids the production of liquid effluents, which are very difficult to process. Given that there's neither accumulation nor resort to explosive substances along the respective stages, the process of the present invention becomes a safe way of obtaining nanomaterial, thus allowing it to be implemented in areas wherein processes with hazardous substance aid are not allowed.
Abstract translation: 本发明涉及一种从乳液乳化和爆炸引发的secco纳米材料合成中的连续方法。 所述方法结合了乳液的同时乳化和爆炸操作，从而确保了高于100kg / h的生产产率。 当保证乳液的敏化主要发生在其进入反应器时，可以避免整个合成过程中任何1类物质的累积，从而将其转化为本质安全的过程。 之后，纳米材料的干收集避免了液体流出物的生产，这很难处理。 既然既没有积累，也没有诉诸各阶段的爆炸性物质，本发明的方法成为获得纳米材料的一种安全的方式，从而允许其在不允许具有危险物质助剂的过程的区域中实施。
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公开(公告)号：US20150360422A1
公开(公告)日：2015-12-17
申请号：US14729439
申请日：2015-06-03
Applicant: David Charles Nemir , Edward S. Rubio , Jan Bastian Beck
Inventor： David Charles Nemir , Edward S. Rubio , Jan Bastian Beck
IPC: B29C67/04
CPC classification number: B29C67/04 , B01J3/08 , B22F3/02 , B22F3/03 , B22F3/08 , B22F2003/248 , B29C43/52 , B29L2031/34
Abstract: Systems and methods for producing a dense, well bonded solid material from a powder may include consolidating the powder utilizing any suitable consolidation method, such as explosive shockwave consolidation. The systems and methods may also include a post-processing thermal treatment that exploits a mismatch between the coefficients of thermal expansion between the consolidated material and the container. Due to the mismatch in the coefficients, internal pressure on the consolidated material during the heat treatment may be increased.
Abstract translation: 用于从粉末生产致密的，良好结合的固体材料的系统和方法可以包括使用任何合适的固结方法（例如爆炸冲击波固结）来固化粉末。 系统和方法还可以包括利用固结材料和容器之间的热膨胀系数之间的不匹配的后处理热处理。 由于系数不匹配，可以增加热处理期间固结材料的内部压力。
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5.发明授权公开(公告)号：US09115001B2
公开(公告)日：2015-08-25
申请号：US13879579
申请日：2011-10-14
CPC classification number: C01D1/02 , B01J3/08 , B82Y30/00 , C01G23/047 , C01G25/02 , C01G45/1235 , C01P2002/34 , C01P2002/50 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C06B23/00 , C06B47/145 , Y10T428/2982
Abstract: The present invention refers to a nanomaterial synthesis process from the decomposition and subsequent reaction among common and economical insoluble precursors, or precursors which hydrolyze in contact with water, which are incorporated in the internal phase of an emulsion. These insoluble precursors are introduced in the internal phase of an emulsion, then being subject to decomposition and subsequent reaction in the solid state, under shockwave effect during the detonation of the emulsion, the nanomaterial with the intended structure being in the end obtained. The process of the present invention therefore allows obtaining a wide range of nanomaterial as composites or binary, ternary structures or higher structures, with small-sized homogenous primary particles, applicable to several technological fields.
Abstract translation: 本发明涉及在共同和经济的不溶性前体之间的分解和随后反应的纳米材料合成方法，或与水接触的水解的前体，其被并入乳液的内相中。 将这些不溶性前体引入乳液的内相中，然后在乳状液爆炸期间的冲击波效应下在固体状态下分解和随后的反应，具有预期结构的纳米材料得到最终结果。 因此，本发明的方法允许获得宽范围的纳米材料作为复合材料或二元，三元结构或更高结构，具有适用于若干技术领域的小尺寸均匀初级颗粒。
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Patent Agency Ranking
6.发明申请公开(公告)号：US20130224488A1
公开(公告)日：2013-08-29
申请号：US13879579
申请日：2011-10-14
IPC: C01D1/02 , C01G25/02 , C01G23/047
CPC classification number: C01D1/02 , B01J3/08 , B82Y30/00 , C01G23/047 , C01G25/02 , C01G45/1235 , C01P2002/34 , C01P2002/50 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C06B23/00 , C06B47/145 , Y10T428/2982
Abstract: The present invention refers to a nanomaterial synthesis process from the decomposition and subsequent reaction among common and economical insoluble precursors, or precursors which hydrolyze in contact with water, which are incorporated in the internal phase of an emulsion. These insoluble precursors are introduced in the internal phase of an emulsion, then being subject to decomposition and subsequent reaction in the solid state, under shockwave effect during the detonation of the emulsion, the nanomaterial with the intended structure being in the end obtained. The process of the present invention therefore allows obtaining a wide range of nanomaterial as composites or binary, ternary structures or higher structures, with small-sized homogenous primary particles, applicable to several technological fields.
Abstract translation: 本发明涉及在共同和经济的不溶性前体之间的分解和随后反应的纳米材料合成方法，或与水接触的水解的前体，其被并入乳液的内相中。 将这些不溶性前体引入乳液的内相中，然后在乳状液爆炸期间的冲击波效应下在固体状态下分解和随后的反应，具有预期结构的纳米材料得到最终结果。 因此，本发明的方法允许获得宽范围的纳米材料作为复合材料或二元，三元结构或更高结构，具有适用于若干技术领域的小尺寸均匀初级颗粒。
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公开(公告)号：US20130221141A1
公开(公告)日：2013-08-29
申请号：US13852730
申请日：2013-03-28
Applicant: Xiaoding Zhang , Chuanzhong Zhang
Inventor： Xiaoding Zhang , Chuanzhong Zhang
IPC: B01J19/26
CPC classification number: B02C19/06 , B01F5/0256 , B01J3/08 , B01J4/002 , B01J19/2405 , B01J19/26 , B01J2219/00162 , B01J2219/00164 , B01J2219/1942 , B02C19/063 , B02C19/065 , C01G25/02 , C01G39/06 , C01P2004/62 , C09C1/00 , C09C1/0003 , C09C3/043
Abstract: The present invention relates to a fluid shockwave reactor. The fluid shockwave reactor introduces laser resonance theory into the field of fluid physics. It consists of a shockwave resonance energy concentration device and at least one set of jet collision device. The shockwave resonance energy concentration device can enhance the shockwave strength produced during jet collisions; strengthen the ultrahigh pressure and cavitation effect of the shockwave field; it can also intensify physical and chemical effects on the processed materials. The fluid shockwave reactor can achieve ultrafine crushing on the fluid materials with lower energy consumption. Under certain technological conditions, the fluid shockwave reactor may also effectively catalytize the chemical reaction process on fluid materials.
Abstract translation: 本发明涉及一种流体冲击波反应器。 流体冲击波反应器将激光共振理论引入流体物理学领域。 它由冲击波共振能量集中装置和至少一组喷射冲击装置组成。 冲击波共振能量集中装置可以提高射流冲击时产生的冲击波强度; 加强冲击波场的超高压和气蚀效应; 也会加剧对加工材料的物理化学作用。 流体冲击波反应器能够以较低的能量消耗对液体材料实现超细粉碎。 在某些技术条件下，流体冲击波反应器也可以有效地催化流体材料上的化学反应过程。
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公开(公告)号：US20120207641A1
公开(公告)日：2012-08-16
申请号：US13441267
申请日：2012-04-06
Applicant: Edward Rubio , David Charles Nemir
Inventor： Edward Rubio , David Charles Nemir
IPC: H01L35/34
Abstract: The explosive consolidation of semiconductor powders results in thermoelectric materials having reduced thermal conductivity without a concurrent reduction in electrical conductivity and thereby allows the construction of thermoelectric generators having improved conversion efficiencies of heat energy to electrical energy.
Abstract translation: 半导体粉末的爆炸性固结导致热电材料具有降低的导热性，而不会导致电导率的同时降低，从而允许构建具有提高的热能转换效率至电能的热电发电机。
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公开(公告)号：US20110226609A1
公开(公告)日：2011-09-22
申请号：US12659808
申请日：2010-03-22
Abstract: This system and method for producing nanomaterials allows for the production of relatively high concentrations of nanoparticles with a minimum of expense, time and energy. Ultrasonic waves, produced at a power of approximately 50 W with a frequency of 26.23 kHz, are projected on a material sample while, simultaneously, a fluid stream jet is projected on the material sample. The ultrasonic waves, in the presence of the fluid jet, create cavities that explode at the surface of the solid material, leading to creation of cracks in the material surface. With the increase in the number of cracks in the material, the solid material erodes. The eroded material, which is on the nanometer scale, is collected on a suitable substrate, such as silicon. This method allows for the preparation of nanoparticles from any solid material, in particular very hard materials, such as diamond, silicon carbide and the like.
Abstract translation: 用于生产纳米材料的该系统和方法允许以最小的费用，时间和能量生产相对高浓度的纳米颗粒。 以大约50瓦的功率产生的频率为26.23kHz的超声波被投射在材料样品上，同时流体流射流投射在材料样品上。 在存在流体射流的情况下，超声波产生在固体材料的表面上爆炸的空腔，导致材料表面产生裂纹。 随着材料中裂纹数量的增加，固体材料的腐蚀程度降低。 在纳米尺度上的被侵蚀的材料被收集在合适的衬底如硅上。 该方法允许从任何固体材料制备纳米颗粒，特别是非常硬的材料，例如金刚石，碳化硅等。
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公开(公告)号：US07867467B2
公开(公告)日：2011-01-11
申请号：US12087280
申请日：2005-12-30
Applicant: Valery Yurievich Dolmatov
Inventor： Valery Yurievich Dolmatov
Abstract: The invention relates to carbon chemistry and is embodied in the form of a nanodiamond comprising 90.0-98.0 mass % carbon, 0.1-5.0 mass % hydrogen, 1.5-3.0 mass % nitrogen and 0.1-4.5 mass % oxygen, wherein the carbon is contained in the form a diamond cubic modification and in a roentgen-amorphous phase at a ratio of (82-95):(18-5) in terms of a carbon mass, respectively. The inventive method for producing said material consisting in detonating in a closed space of a carbon-inert gas medium a carbon-containing oxygen-deficient explosive material which is placed in a condensed phase envelop containing a reducing agent at a quantitative ratio between said reducing agent mass in the condensed envelop and the mass of the used carbon-containing explosive material equal to or greater than 0.01:1 and in chemically purifying by treating detonation products with a 2-40% aqua nitric acid jointly with a compressed air oxygen at a temperature ranging from 200 to 280° C. and a pressure of 5-15 MPa.
Abstract translation: 本发明涉及碳化学，并且以纳米金刚石的形式实施，其包含90.0-98.0质量％的碳，0.1-5.0质量％的氢，1.5-3.0质量％的氮和0.1-4.5质量％的氧，其中， 形式为菱形立方体改性，在碳质量方面分别以（82-95）：（18-5）的比例在罗恩非晶相中。 本发明的制造所述材料的方法包括在碳惰性气体介质的封闭空间内引发含碳缺氧的炸药，所述含碳缺氧的炸药在所述还原剂的定量比例下放置在含有还原剂的冷凝相包络中 冷凝包层中的质量和所用含碳的爆炸性物质的质量等于或大于0.01:1，并通过用2-40％的硝酸与压缩空气氧在温度下联合处理爆炸产物进行化学纯化 范围为200至280℃，压力为5-15MPa。
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