Abstract:
The present invention concerns a device for measuring the pressure and temperature in at least one pressure-tight analysis vessel, that has been sealed by means of a lid, whereby heat is supplied to the analysis vessel by means of a microwave oven. The device comprises a measurement device that is connected to a unit for controlling the microwave oven. In this regard, the measurement device is arranged in a microwave-tight housing inside the microwave field that is produced by the microwave oven. The housing is constructed in such a way that it forms a shield that is impermeable for the microwave field. A microwave-free zone is produced inside the housing. Electronic, current-carrying components can be arranged in the microwave-tight housing without, as a result, generating interference in the microwave field.
Abstract:
A device for high-pressure treatment, in particular of liquid substances which contain components with a consistency different from that of the liquid. The device comprises a cylinder member (1), two end members (2, 3), a high-pressure piston (4), two high-pressure seals (8, 9) and connection means comprising channels and valve members to conduct the substance to and from the cylinder member (1). When the substance is pressurized, the cylinder member (1), at least one of the end members (3), the high-pressure piston (4) and the two high-pressure seals (8, 9) delimit a high-pressure chamber (10). The connection means are arranged outside the high-pressure chamber and preferably in respective end members (2, 3).
Abstract:
A process for hydrothermal oxidation of combustible materials in which, during at least a part of the oxidation, corrosive material is present and makes contact with at least a portion of the apparatus over a contact area on the apparatus. At least a portion of the contact surface area comprises iridium, iridium oxide, an iridium alloy, or a base metal overlaid with an iridium coating. Iridium has been found to be highly resistant to environments encountered in the process of hydrothermal oxidation. Such environments typically contain greater than 50 mole percent water, together with oxygen, carbon dioxide, and a wide range of acids, bases and salts. Pressures are typically about 27.5 to about 1000 bar while temperatures range as high as 800.degree. C.
Abstract:
Process and device for the treatment of lumpy products using process media, the treatment including a predetermined sequence of process steps. A chain of treatment units is moved in a stepwise manner. The product to be treated remains within the same treatment unit for the duration of the sequence of the process steps. A supply unit supplies and removes process media in a stopping-station specific manner so that the process steps can proceed simultaneously in the treatment units.
Abstract:
Sealable container assemblies include containers for materials which are to be microwave heated, such as in digesting or extracting operations, made of thermoplastic material, such as fluoropolymer, that is strengthened by reinforcing means that may be a fiber reinforced thermoplastic of high tensile strength, such as polyetherimide, with reinforcing continuous fibers in a matrix of such thermoplastic, which fibers are very preferably in the shape of a sleeve or sleeves and are of glass or other heat resistant and microwave transmissive material. The containers may be strengthened by incorporating the fiber reinforced thermoplastic in a wall or walls of the container or preferably by inserting the container into a reinforcement, which is a sleeve or collar of the reinforced thermoplastic. In both such constructions the reinforcing means protects the container against radial failure due to pressure that is generated by the microwave heating of the container contents. However, it has been found that in those cases wherein the internal pressure of the container rises even higher than that against which the reinforcement is protective, failure of the side wall and the reinforcement may be explosive, so the containers of this invention are of a structure that causes them to fail at an unreinforced location before the reinforcement, which failure is less explosive and less damaging to equipment employed and to any surroundings. Also described are the container construction, which preferably includes a central bottom depression and a skirt, and procedures for utilizing the containers in heatings of materials.
Abstract:
High temperature reactions are conducted within a high pressure reaction vessel. The interior surfaces of the high pressure containment vessel are protected from the high temperature and corrosive effects of the reaction by causing the reactants to converge in a vortex which contains the highest reaction temperature within the central portions of the reactor. A toroidal reaction vessel is disclosed in which the reactants are directed into a vortex at the axis of origin of the torus by flow guides.
Abstract:
A sterilization system attachable to an autoclave or in the form of a free-standing auxiliary unit adapted to receive cassette sterilization containers for causing a high volume of air heated to an effective drying temperature to flow into said chamber at a high air flow rate. A control effective to open a valve when the unit for supplying heated air is operating and to close the valve when the unit is not operating. A device for supporting medical or dental instruments during sterilization is also disclosed.
Abstract:
A safety apparatus has been found for controlling the release of flashing hydrogen fluoride in a hydrocarbon alkylation process. The safety apparatus comprises containment baffles enclosing major process vessels. The safety apparatus may be used in combination with a liquid onium polyhydrogen fluoride complex to substantially reduce the vapor cloud produced from a leaking process vessel.
Abstract:
An apparatus for sterilizing objects comprising a tubular container part which is removably arranged on an electric supply and control unit. The container part has a chamber-defining inner wall which is also an electrical resistance heating element. Accordingly, the container part may be made with low heat capacity and a correspondingly short heat-up period.
Abstract:
A high temperature high pressure furnace has a hybrid partially externally heated construction. A metallic vessel fabricated from an alloy having a composition of at least 45% nickel, 15% chrome, and 10% tungsten is utilized (the preferred alloy including 55% nickel, 22% chrome, 14% tungsten, 2% molybdenum, 3% iron (maximum) and 5% cobalt (maximum). The disclosed alloy is fabricated into 11/4 or 2 inch, 32 mm or 50 mm bar stock and has a length of about 22 inches, 56 cm. This bar stock has an aperture formed therein to define a closed high temperature, high pressure oxygen chamber. The opposite and closed end of the vessel is provided with a small blind aperture into which a thermocouple can be inserted. The closed end of the vessel is inserted into an oven, preferably heated by standard nickel chrome electrical elements and having a heavily insulated exterior.