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81.发明授权Bis(2,2',6,6'-tetramethyl-4-aminoethyleneamidopiperidyl) polyoxyalkylene 失效聚（2,2'，6,6'-四甲基-4-氨基亚乙基氨基哌啶基）聚氧化烯
公开(公告)号：US5210195A
公开(公告)日：1993-05-11
申请号：US789500
申请日：1991-11-08
Applicant: Jiang-Jen Lin , George P. Speranza
Inventor： Jiang-Jen Lin , George P. Speranza
IPC: C07D211/58 , C08G65/332 , C08G65/333 , C08K5/3435
CPC classification number: C08K5/3435 , C07D211/58 , C08G65/3322 , C08G65/33317
Abstract: Polyoxyalkylene diamines react with excess acrylate to form diesters which react with 2,2',6,6'-tetramethyl-4-aminopiperidines to give a product of formula 1, useful as photostabilizer for photosensitive materials. ##STR1##
Abstract translation: 聚氧化烯二胺与过量的丙烯酸酯反应形成二酯，其与2,2'，6,6'-四甲基-4-氨基哌啶反应，得到式1的产物，其用作感光材料的光稳定剂。 公式1
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公开(公告)号：US5128441A
公开(公告)日：1992-07-07
申请号：US519080
申请日：1990-05-04
Applicant: George P. Speranza , Jiang-Jen Lin
Inventor： George P. Speranza , Jiang-Jen Lin
Abstract: A block polyamido primary amine condensation product prepared by reacting a defined polyoxyalkylene polyamine having terminal primary amine groups with an amount of a defined dicarboxylic acid or an anhydride or a C.sub.1 to C.sub.4 alkyl ester thereof, sufficient to react one mole of the dicarboxylic acid reactant with each primary amine group of the polyoxyalkylene polyamine to thereby prepare an intermediate condensation reaction product containing terminal carboxyl groups, and reacting one mole of a defined organic di-primary amine with each terminal carboxyl group of the said intermediate condensation reaction product to thereby provide, as the principal product of the reaction a block polyamido primary amine condensation product.
Abstract translation: 通过使具有末端伯胺基的规定的聚氧化烯多胺与一定量的二羧酸或其酸酐或其C1-C4烷基酯反应制备的嵌段聚酰氨基伯胺缩合产物，其足以使一摩尔二羧酸反应物与 从而制备含有末端羧基的中间缩合反应产物，并使一摩尔限定的有机二伯胺与所述中间缩合反应产物的每个末端羧基反应，从而提供作为 反应的主要产物是嵌段聚酰胺伯胺缩合产物。
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公开(公告)号：US5120817A
公开(公告)日：1992-06-09
申请号：US661142
申请日：1991-02-27
Applicant: George P. Speranza , Harold G. Waddill , Jiang-Jen Lin
Inventor： George P. Speranza , Harold G. Waddill , Jiang-Jen Lin
Abstract: An epoxy resin composition comprises an vicinal polyepoxide and a Mannich condensation reaction product curing agent. The curing agent is the Mannich condensation reaction product of a phenol, formaldehyde and a polyoxyethylenediamine of the formula:NH.sub.2 (CH.sub.2 CH.sub.2 O).sub.x --CH.sub.2 CH.sub.2 NH.sub.2,and wherein: x ranges from 1 to 3. These epoxy resin compositions are useful in coatings, adhesives, encapsulations and composite matrices.
Abstract translation: 环氧树脂组合物包含邻位聚环氧化物和曼尼希缩合反应产物固化剂。 固化剂是苯酚，甲醛和下列通式为：NH 2（CH 2 CH 2 O）x -CH 2 CH 2 NH 2的聚氧乙烯二胺的曼尼希缩合反应产物，其中：x为1至3.这些环氧树脂组合物可用于涂料，粘合剂， 封装和复合矩阵。
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公开(公告)号：US5101060A
公开(公告)日：1992-03-31
申请号：US615104
申请日：1990-11-19
Applicant: George P. Speranza , Jiang-Jen Lin
Inventor： George P. Speranza , Jiang-Jen Lin
IPC: C07C217/08 , C07C255/24
CPC classification number: C07C217/08 , C07C255/24
Abstract: Normally liquid final Mannich condensates prepared by reacting a para C.sub.1 -C.sub.15 alkyl phenol with formaldehyde and a first polyoxyalkylene diamine to form an intermediate Mannich condensate that is reacted with formaldehyde and a second polyoxyalkylene diamine to form a final Mannich condensate, the first and second polyoxyalkylene diamines having the formula: ##STR1## wherein R represents hydrogen or methyl and R' represents an alkyl group containing 1 to 4 carbon atoms or cyanoethyl group, and n represents positive numbers having a value of 1 to about 6, the final Mannich condensate having the formula: ##STR2## wherein X and Y are polyoxyalkylene amine groups derived from the first and second polyoxyalkylene diamines and formaldehyde.
Abstract translation: 通常将对位C 1 -C 15烷基苯酚与甲醛和第一聚氧化烯二胺反应制备的通常为液体的最终曼尼希缩合物，以形成与甲醛和第二聚氧化烯二胺反应形成最终曼尼希缩合物的中间曼尼希缩合物，第一和第二聚氧化烯 具有下式的二胺：其中R表示氢或甲基，R'表示含有1至4个碳原子的烷基或氰乙基，n表示1至6的正数，最终 具有下式的曼尼希缩合物：其中X和Y是衍生自第一和第二聚氧化烯二胺和甲醛的聚氧化烯胺基团。
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85.发明授权Isocyanate prepolymers and secondary amines from disecondary amines and alkyl diisocyanates 失效异氰酸酯丙烯酸酯和二异丙基胺与二异丙基氨基甲酸酯
公开(公告)号：US5084202A
公开(公告)日：1992-01-28
申请号：US377355
申请日：1989-07-10
Applicant: Jiang-Jen Lin , George P. Speranza
Inventor： Jiang-Jen Lin , George P. Speranza
IPC: C07C273/02 , C07C273/18 , C07C275/18 , C07C275/26 , C07C275/28 , C08G18/32 , C08G18/50 , C08G18/80
CPC classification number: C07C273/1827 , C08G18/3228 , C08G18/5024 , C08G18/8038
Abstract: Disclosed are novel isocyanate prepolymers and novel secondary amines, both prepared from alkyl diisocyanates and secondary isopropyl derivatives of polyoxyalkylene diamines. The molar ratios, reaction procedures (i.e. inverse addition of reactants) and solvent determine the products. Most of the products are light colored and nongelled.The isocyanate prepolymers are useful in the field of polyurethanes and the novel secondary amines are useful in epoxy coatings applications.
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Patent Agency Ranking
公开(公告)号：US5068444A
公开(公告)日：1991-11-26
申请号：US429671
申请日：1989-10-31
Applicant: Michael Cuscurida , David R. McCoy , Jiang-Jen Lin
Inventor： Michael Cuscurida , David R. McCoy , Jiang-Jen Lin
IPC: C07C217/08 , C08G18/50 , C08G18/56 , C08G65/26 , C08G65/325 , C08G65/331 , C08L63/00
CPC classification number: C08G65/331 , C07C217/08 , C08G18/5024 , C08G18/56 , C08G65/2609 , C08G65/3255 , C08L63/00 , C08G2120/00
Abstract: A process in which a dialdehyde is reacted with a polyoxyalkylene glycol to form a dialdehyde glycol condensate which is alkoxylated with propylene oxide, butylene oxide or mixtures thereof and the resulting product is then catalytically aminated to provide, for example, a tetramine is disclosed. These compounds are useful as curing agents for epoxy resins and for reaction with isocyanates to prepare polyurea elastomers and to manufacture articles, such as automotive body panels by reaction injection molding.
Abstract translation: 其中二醛与聚亚氧烷基二醇反应以形成二氧化二醇缩合物，其用环氧丙烷，环氧丁烷或其混合物进行烷氧基化，然后所得产物进行催化胺化以提供例如四胺。 这些化合物可用作环氧树脂的固化剂并用于与异氰酸酯反应以制备聚脲弹性体，并通过反应注射成型制备制品，例如汽车车身面板。
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公开(公告)号：US4990576A
公开(公告)日：1991-02-05
申请号：US429672
申请日：1989-10-31
Applicant: Michael Cuscurida , Jiang-Jen Lin
Inventor： Michael Cuscurida , Jiang-Jen Lin
IPC: C08G65/26 , C08G65/28 , C08G65/325 , C08L63/00
CPC classification number: C08G65/3255 , C08G65/2609 , C08L63/00
Abstract: A process in which a di-trimethylol alkane initiator is oxyalkylated to form an alkylene oxide adduct which is then catalytically aminated to provide, for example, a tetramine. These compounds are useful for preparing polyurethane products and as curing agents for epoxy resins.
Abstract translation: 其中二 - 三羟甲基烷烃引发剂被烷氧基化以形成烯化氧加合物的方法，然后进行催化胺化以提供例如四胺。 这些化合物可用于制备聚氨酯产品和用作环氧树脂的固化剂。
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公开(公告)号：US4940770A
公开(公告)日：1990-07-10
申请号：US270897
申请日：1988-11-14
Applicant: George P. Speranza , Jiang-Jen Lin
Inventor： George P. Speranza , Jiang-Jen Lin
CPC classification number: C08G59/184 , C08L63/00
Abstract: Disclosed are novel compositions useful in mixed epoxy material synthesis, poly(epoxy)-(urea) synthesis and cases where epoxy curing agents require flexibility which are essentially the reaction products of polyoxyalkylene polyamines and epoxides. Specifically the amine reactants comprise polyoxypropylene triamines, amine terminated alkylene glycols and polyoxypropylene diols, such as those represented by Texaco Chemical Company's JEFFAMINE.RTM. T-series, JEFFAMINE.RTM. EDR series and JEFFAMINE.RTM. D-series amines, respectively. The epoxide component prepolymers essentially comprise Bisphenol A diglycidyl ethers. The ratio of JEFFAMINE.RTM. amine to epoxide and the use of acetone are essential to prepare non-gelled products.
Abstract translation: 公开了可用于混合环氧材料合成，聚（环氧） - （尿素）合成和环氧固化剂需要柔性的情况的新型组合物，其基本上是聚氧化烯多胺和环氧化物的反应产物。 具体地，胺反应物分别包括聚氧丙烯三胺，胺封端的亚烷基二醇和聚氧丙烯二醇，例如由Texaco Chemical Company的JEFFAMINE TM T系列，JEFFAMINE TM EDR系列和JEFFAMINE TM D系列胺代表的那些。 环氧化物组分预聚物基本上包含双酚A二缩水甘油醚。 JEFFAMINE TM胺与环氧化物的比例和使用丙酮对于制备非凝胶产品是至关重要的。
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89.发明授权Liquid cleaning compositions containing polyether amide surfactants as thickening agents 失效含有聚醚酰胺表面活性剂作为增稠剂的液体清洗组合物
公开(公告)号：US4828757A
公开(公告)日：1989-05-09
申请号：US168024
申请日：1988-03-14
Applicant: Carter G. Naylor , Jiang-Jen Lin , George P. Speranza
Inventor： Carter G. Naylor , Jiang-Jen Lin , George P. Speranza
IPC: C08G65/332 , C11D1/52 , C11D3/37 , C11D17/00
CPC classification number: C11D1/528 , C08G65/3322 , C11D17/003 , C11D3/3707
Abstract: A method of thickening an aqueous solution containing from 5 to 50 wt% of a surfactant is disclosed comprising the addition of from about 0.1 to 10 wt% to the solution of a polyether amide derivative having the general formula: ##STR1## wherein R=C.sub.9 -C.sub.23 and a=1 to about 5 and b=1 to 500.
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90.发明授权Process for oxidative carbonylation using a catalyst having a novel support 失效使用具有新型载体的催化剂进行氧化羰基化的方法
公开(公告)号：US4667053A
公开(公告)日：1987-05-19
申请号：US880394
申请日：1986-06-30
Applicant: Jiang-Jen Lin
Inventor： Jiang-Jen Lin
IPC: C07C67/38
CPC classification number: C07C67/38
Abstract: This invention relates to the carbonylation of olefins. More particularly it involves the carbonylation of an .alpha.-olefins such as ethylene to form diesters, such as, for example, dimethyl succinate, 3-methoxypropionate and dimethylcarbonate by a process comprising reacting said olefin with carbon monoxide, oxygen and an alkanol in the presence of a heterogeneous palladium/copper catalyst, on a polymer support.
Abstract translation: 本发明涉及烯烃的羰基化。 更具体地，涉及α-烯烃如乙烯的羰基化以形成二酯，例如琥珀酸二甲酯，3-甲氧基丙酸酯和碳酸二甲酯，其包括在存在下使所述烯烃与一氧化碳，氧和链烷醇反应的方法 的非均相钯/铜催化剂。
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