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    High alkalinity additives for lubricating oil compositions
    81.
    发明授权
    High alkalinity additives for lubricating oil compositions 失效
    用于润滑油组合物的高碱性添加剂

    公开(公告)号：US3671430A

    公开(公告)日：1972-06-20

    申请号：US3671430D

    申请日：1971-01-19

    Applicant: EXXON RESEARCH ENGINEERING CO

    Inventor： CORRINGER JEAN

    IPC: C10M159/24 ,  C10M1/40 ,  C10M1/48

    CPC classification number: C10M159/24 ,  C10M2201/062 ,  C10M2201/08 ,  C10M2201/081 ,  C10M2201/082 ,  C10M2201/084 ,  C10M2203/10 ,  C10M2203/102 ,  C10M2203/104 ,  C10M2203/106 ,  C10M2203/108 ,  C10M2207/023 ,  C10M2207/027 ,  C10M2207/123 ,  C10M2207/125 ,  C10M2207/129 ,  C10M2207/22 ,  C10M2219/02 ,  C10M2219/044 ,  C10M2219/046 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089 ,  C10M2223/00 ,  C10M2223/045 ,  C10M2223/047 ,  C10M2223/08 ,  C10M2223/12 ,  C10M2225/04 ,  C10M2225/041 ,  C10N2210/00 ,  C10N2210/02 ,  C10N2240/102 ,  C10N2240/103 ,  C10N2270/02

    Abstract: An alkaline earth metal sulfonate of high alkalinity is prepared by reacting an alkaline earth metal base, e.g. calcium hydroxide, with carbon dioxide in the presence of the metal sulfonate and an alkaline earth metal phenate, there also being present a polar solvent such as benzyl alcohol or tetrahydrofurfuryl alcohol, as well as free phenol in an amount over and above the stoichiometric quantity necessary to form metal phenate by reaction with the metal base. At the end of the reaction the solvent and free phenol are removed from the product by distillation. Preformed metal phenate can be used at the beginning of the reaction or the metal phenate can be formed in situ, starting with free phenol. Also, in place of metal sulfonate, free sulfonic acid can be used initially, with sufficient metal base to convert it to metal sulfonate. The attainment of total base numbers of 400 or more is possible by use of a second dispersant along with the metal sulfonate. This second dispersant, which is used with the sulfonate in the proportion of 0.1 to 1 part per part of sulfonate, can be a thioacid of phosphorus, or metal salt thereof, obtained by reaction of a sulfide of phosphorus on a hydrocarbon; an alkyl phenol or alkyl phenol sulfide, or metal salt thereof; or a monocarboxylic or polycarboxylic acid or anhydride, or metal salt thereof, characterized by a long chain hydrocarbon group of from about 20 to 200 carbon atoms, as for example, a polyisobutenyl succinic acid.

    Abstract translation: 高碱度的碱土金属磺酸盐是通过使碱土金属碱如 氢氧化钙与金属磺酸盐和碱土金属酚盐存在下的二氧化碳，还存在极性溶剂如苄醇或四氢糠醇，以及游离酚的量超过所需化学计量的量 通过与金属基体反应形成金属酚盐。 在反应结束时，通过蒸馏从产物中除去溶剂和游离酚。 可以在反应开始时使用预成型的金属酚盐，或者可以从游离酚开始原位形成金属酚盐。 另外，代替金属磺酸盐，最初可以使用游离的磺酸，具有足够的金属碱将其转化为金属磺酸盐。 通过使用第二分散剂与金属磺酸盐可以实现总碱值为400以上。 与磺酸盐以0.1〜1份/份磺酸盐的比例使用的第二种分散剂可以是通过在烃上的磷的硫化物反应获得的磷或其金属盐的硫酸， 烷基酚或烷基酚硫醚，或其金属盐; 或单羧酸或多羧酸或酸酐或其金属盐，其特征在于约20至200个碳原子的长链烃基，例如聚异丁烯基琥珀酸。

    Increasing viscosity of normally liquid hydrocarbons and gels produced
    82.
    发明授权
    Increasing viscosity of normally liquid hydrocarbons and gels produced 失效
    增加生产的正常液体碳氢化合物和凝胶的粘度

    公开(公告)号：US3658491A

    公开(公告)日：1972-04-25

    申请号：US51678055

    申请日：1955-06-20

    Applicant: PHILLIPS PETROLEUM CO

    Inventor： CANTERINO PETER J

    IPC: C08J3/02 ,  C10L7/02

    CPC classification number: C10M5/00 ,  C10L7/02 ,  C10M2201/00 ,  C10M2201/061 ,  C10M2201/08 ,  C10M2201/081 ,  C10M2201/082 ,  C10M2201/084 ,  C10M2201/085 ,  C10M2201/16 ,  C10M2201/18 ,  C10M2207/121 ,  C10M2207/122 ,  C10M2207/123 ,  C10M2207/129 ,  C10M2207/22 ,  C10M2217/022 ,  C10M2217/028 ,  C10M2217/06 ,  C10N2250/10

    Abstract: 1. The production of a gel which comprises incorporating into a normally liquid hydrocarbon a small proportion effective to form a gel of at least one liquid hydrocarbon dispersible copolymer selected from the group consisting of rubbery and solid copolymers compound represented by the formula WHEREIN R is selected from the group consisting of hydrogen, alkyl and alkoxy; and R'' is selected from the group consisting of WHEREIN X is selected from the group consisting of hydrogen, alkyl and a halogen, Y is selected from the group consisting of hydrogen, alkyl and aryl; wherein R'''' is selected from the group consisting of alkyl, cycloalkyl, aryl, alkaryl, and aralkyl; the total of the carbon atoms in R and R'' when R'' does not contain R'''' is two to eight; and wherein when R'''' is present the total of the carbon atoms in R and R'' is two to thirteen and a copolymerizable compound containing a basic tertiary amine group selected from the group consisting of vinylpyridines, vinylquinolines and their nuclear-alkyl-substituted derivatives containing not more than a total of 12 carbon atoms in the nuclear-substituted groups, said copolymerizable compound containing not more than a total of 12 carbon atoms in the hydrocarbon groups attached to the nitrogen atom, said copolymer having been prepared using 0.25-8 parts per 100 by weight of total monomeric material.

    Abstract translation: 1.制备凝胶，其包括将有效形成至少一种选自由式WHEREIN R表示的橡胶状和固体共聚物化合物的至少一种液体烃分散性共聚物的凝胶的常规液体烃引入 由氢，烷基和烷氧基组成的组; 并且R'选自WHEREIN X选自氢，烷基和卤素，Y选自氢，烷基和芳基; 其中R“选自烷基，环烷基，芳基，烷芳基和芳烷基; 当R'不含R“时R和R'中的碳原子总数为2至8; 并且当R“存在时，R和R'中的碳原子总数为2至13，并且含有选自乙烯基吡啶，乙烯基喹啉及其核 - 烷基取代的衍生物的碱性叔胺基团的可共聚化合物 在核取代基中含有不超过总共12个碳原子，所述可共聚化合物在与氮原子连接的烃基中不超过总共12个碳原子，所述共聚物使用0.25-8份 每100重量份的总单体材料。

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