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公开(公告)号：US5079309A
公开(公告)日：1992-01-07
申请号：US378784
申请日：1989-07-12
Applicant: James E. Harris , Lloyd M. Robeson , Michael D. Cliffton , Bernard H. Eckstein , Markus Matzner
Inventor： James E. Harris , Lloyd M. Robeson , Michael D. Cliffton , Bernard H. Eckstein , Markus Matzner
Abstract: Described herein are miscible blends of a poly(aryl ether ketone) and an imide-containing polymer which are useful in the manufacture of extruded film, continuous fiber composites and injection molded articles.
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2.发明授权Miscible blends of a poly(aryl ether ketone) and an imide containing polymer 失效聚（芳基醚酮）和含酰亚胺的聚合物的混溶混合物
公开(公告)号：US5171796A
公开(公告)日：1992-12-15
申请号：US231532
申请日：1988-08-12
Applicant: James E. Harris , Lloyd M. Robeson , Michael D. Cliffton , Bernard H. Eckstein , Markus Matzner
Inventor： James E. Harris , Lloyd M. Robeson , Michael D. Cliffton , Bernard H. Eckstein , Markus Matzner
Abstract: Described herein are miscible blends of a poly(aryl ether ketone) and an imide-containing polymer which are useful in the manufacture of extruded film, continuous fiber composites and injection molded articles.
Abstract translation: 本文描述了可用于制造挤出薄膜，连续纤维复合材料和注塑制品的聚（芳基醚酮）和含酰亚胺聚合物的混溶混合物。
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公开(公告)号：US5071944A
公开(公告)日：1991-12-10
申请号：US315997
申请日：1989-02-27
Applicant: Michael D. Cliffton , Jon F. Geibel
Inventor： Michael D. Cliffton , Jon F. Geibel
CPC classification number: C08G75/00 , C08G75/024
Abstract: A polymerization process is provided for the production of high molecular weight aromatic sulfide/ketone polymer from at least one dihaloaromatic ketone, at least one alkali metal sulfide, at least one polar organic compound and water wherein the polymerization reaction is conducted in two distinct steps separated by an intermediate step of removal of at least a portion of the water.
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公开(公告)号：US5089596A
公开(公告)日：1992-02-18
申请号：US527233
申请日：1990-05-22
Applicant: Michael D. Cliffton , Jerry O. Reed , Rex L. Bobsein , Jon F. Geibel
Inventor： Michael D. Cliffton , Jerry O. Reed , Rex L. Bobsein , Jon F. Geibel
IPC: C08G75/02
CPC classification number: C08G75/0254 , C08G75/024 , C08G75/0281
Abstract: Aromatic sulfide/ketone polymer is prepared from dihaloaromatic ketone, alkali metal sulfide, water and a polar organic compound. The polymerization reaction mixture comprising the aromatic sulfide/ketone polymer is subjected to a heat soak at elevated temperature then a separation agent (non-solvent) is added under controlled conditions and subsequently cooled to provide a mixture comprising particulate aromatic sulfide/ketone polymer.Biaxially-oriented film is made from recovered particles of aromatic sulfide/ketone polymer prepared as described by (1) washing the polymer particles with an aqueous calcium salt, (2) heating said washed particles to remove water, wherein the resulting heated particles are at least partially crystalline, (3) molding said heating particles to form a sheet of polymer, (4) biaxially stretching said sheet above the glass transition temperature of the polymer to form a film, and (5) heat-setting said biazially-oriented film under stretching tension for a time and at a temperature to increase strength properties and density.
Abstract translation: 芳族硫化物/酮聚合物由二卤代芳族酮，碱金属硫化物，水和极性有机化合物制备。 将包含芳族硫化物/酮聚合物的聚合反应混合物在高温下进行热浸，然后在受控条件下加入分离剂（非溶剂），随后冷却以提供包含颗粒状芳族硫化物/酮聚合物的混合物。 双轴取向薄膜由（1）用钙盐水洗涤聚合物颗粒制备的芳族硫化物/酮聚合物的回收颗粒制成，（2）加热所洗涤的颗粒以除去水，其中所得的加热颗粒在 （3）模制所述加热颗粒以形成聚合物片材，（4）将所述片材双轴拉伸高于聚合物的玻璃化转变温度以形成膜，和（5）将所述双重取向的膜热定型 在拉伸张力下一段时间，并在一定温度下增加强度性能和密度。
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公开(公告)号：US4892929A
公开(公告)日：1990-01-09
申请号：US272620
申请日：1988-11-16
Applicant: Jon F. Geibel , Roger G. Gaughan , Michael D. Cliffton
Inventor： Jon F. Geibel , Roger G. Gaughan , Michael D. Cliffton
IPC: C08G75/02
CPC classification number: C08G75/0295 , C08G75/024
Abstract: Melt stable polymeric resins are provided by process which comprises heating a first particulate resin selected from the group consisting of poly(arylene sulfide ketone) and poly(arylene sulfide diketone), while in the presence of a gaseous oxidizing atmosphere, to a temperature at least about 150.degree. C. (302.degree. F.) but below the melting point of the first particulate resins, for time sufficient to produce a second particulate resin. The thermal stability of the second particulate resin is superior to that of its respective first particulate resin is superior to that of its respective first particulate resin. Moreover, the molecular weight of the second particulate resin is greater than that of its respective first particulate resin.
Abstract translation: 熔融稳定的聚合物树脂通过以下方法提供，该方法包括在气态氧化气氛存在下将选自聚（亚芳基硫醚酮）和聚（亚芳基硫醚二酮）的第一颗粒树脂加热到至少 约130℃（302°F）但低于第一颗粒树脂的熔点，足以产生第二颗粒树脂。 第二颗粒树脂的热稳定性优于其第一颗粒树脂的热稳定性优于其相应的第一颗粒树脂的热稳定性。 此外，第二颗粒树脂的分子量大于其第一颗粒树脂的分子量。
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Patent Agency Ranking
公开(公告)号：US4698411A
公开(公告)日：1987-10-06
申请号：US857271
申请日：1986-04-30
Applicant: H. Wayne Hill, Jr. , Michael D. Cliffton
Inventor： H. Wayne Hill, Jr. , Michael D. Cliffton
CPC classification number: C08G63/52
Abstract: An unsaturated polyester resin syrup containing styrene monomer in which styrene volatilization is suppressed using a substituted succinic acid or substituted succinic anhydride.
Abstract translation: 使用取代的琥珀酸或取代的琥珀酸酐抑制苯乙烯挥发的含苯乙烯单体的不饱和聚酯树脂糖浆。
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7.发明授权
公开(公告)号：US5264176A
公开(公告)日：1993-11-23
申请号：US800905
申请日：1991-11-26
Applicant: Michael D. Cliffton , Jerry O. Reed , Rex L. Bobsein , Jon F. Geibel
Inventor： Michael D. Cliffton , Jerry O. Reed , Rex L. Bobsein , Jon F. Geibel
CPC classification number: C08G75/0254 , C08G75/024 , C08G75/0281
Abstract: An aromatic sulfide/ketone polymer is prepared from a dihaloaromatic ketone, alkali metal sulfide, water and a polar organic compound. The polymerization reaction mixture is subjected to a heat soak at an elevated temperature, then a separation agent is added under controlled conditions and the mixture is subsequently cooled to provide a mixture comprising particulate aromatic sulfide/ketone polymer. Biaxially-oriented film is made from the recovered particles of aromatic sulfide/ketone polymer by (1) washing the polymer particles with an aqueous calcium salt, (2) heating the washed particles to remove water, (3) molding the heated particles to form a sheet of polymer, (4) biaxially stretching the sheet above the glass transition temperature of the polymer to form a film, and (5) heat-setting the biaxially-oriented film under stretching tension for a time and at a temperature to increase strength properties and density.
Abstract translation: 由二卤代芳族酮，碱金属硫化物，水和极性有机化合物制备芳族硫化物/酮聚合物。 将聚合反应混合物在升高的温度下进行热浸，然后在受控条件下加入分离剂，随后将混合物冷却以提供包含颗粒状芳族硫化物/酮聚合物的混合物。 通过（1）用钙盐水洗涤聚合物颗粒，（2）加热洗涤的颗粒以除去水，（3）将加热的颗粒成型形成，由回收的芳族硫化物/酮聚合物颗粒制成双轴取向膜 （4）将聚合物的玻璃化转变温度以上的双轴拉伸形成薄膜，（5）将拉伸张力下的双轴拉伸薄膜热固化一段时间，并使温度升高， 性质和密度。
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公开(公告)号：US5003033A
公开(公告)日：1991-03-26
申请号：US505877
申请日：1990-04-06
Applicant: Jon F. Geibel , Lacey E. Scoggins , Michael D. Cliffton
Inventor： Jon F. Geibel , Lacey E. Scoggins , Michael D. Cliffton
IPC: C08G75/02
CPC classification number: C08G75/0231 , C08G75/024
Abstract: A process for preparing a branched, high molecular weight poly(arylene sulfide ketone) by the addition of a polyhaloaromatic compound to a reaction mixture containing a dihaloaromatic ketone, an organic amide, an alkali metal sulfide, and water, and the product produced therefrom.
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公开(公告)号：US4988796A
公开(公告)日：1991-01-29
申请号：US481529
申请日：1990-02-20
Applicant: Michael D. Cliffton , Jon F. Geibel
Inventor： Michael D. Cliffton , Jon F. Geibel
CPC classification number: C08G75/0236 , C08G75/20
Abstract: A process for preparing poly(arylene sulfide sulfone) by contacting a dihaloaromatic sulfone, an organic amide, a sulfur-containing compound selected from the group consisting of alkali metal bisulfides, hydrogen sulfide and N-methyl-2-pyrrolidinethione, water, and an alkali metal carboxylate.
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10.发明授权Production of copper amine salt complexes for catalysts for the oxidative coupling of alkylphenols 失效生产用于烷基酚氧化偶合的催化剂的铜胺盐络合物
公开(公告)号：US4965384A
公开(公告)日：1990-10-23
申请号：US348058
申请日：1989-05-05
Applicant: Michael D. Cliffton , Stephen J. Carter
Inventor： Michael D. Cliffton , Stephen J. Carter
Abstract: This invention relates to the production of copper catalysts for the oxidative coupling of 2,6-dialkylphenols to produce mixtures of 3,3',5,5'-tetra-alkyl-4,4'-dihydroxybiphenyls and corresponding diphenoquinones.
Abstract translation: 本发明涉及用于氧化偶联2,6-二烷基酚以制备3,3'，5,5'-四烷基-4,4'-二羟基联苯和相应的二苯醌的混合物的铜催化剂的生产。
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