Continuous process of preparing bromopicrin
    2.
    发明授权
    Continuous process of preparing bromopicrin 有权
    制备溴氰菊酯的连续工艺

    公开(公告)号:US08415513B2

    公开(公告)日:2013-04-09

    申请号:US12601547

    申请日:2008-05-26

    CPC classification number: C07C201/12 C07C205/08

    Abstract: A continuous process of preparing bromopicrin is disclosed. The process is effected by transferring a continuous flow of a first mixture and a continuous flow of a second mixture into a first reactor, the first mixture containing nitromethane and bromine and the second mixture containing an aqueous solution of an alkaline substance, to thereby obtain a reaction mixture which comprises bromopicrin in said first reactor; and collecting the bromopicrin from the reaction mixture. Highly pure bromopicrin obtained by this process is also disclosed.

    Abstract translation: 公开了制备溴氰菊酯的连续方法。 该方法通过将第一混合物的连续流和第二混合物的连续流转移到第一反应器中,第一混合物含有硝基甲烷和溴,第二混合物含有碱性物质的水溶液,从而获得 在所述第一反应器中包含溴化苦素的反应混合物; 并从反应混合物中收集溴氰菊酯。 还公开了通过该方法获得的高纯度溴氰菊酯。

    CONTINUOUS PROCESS OF PREPARING BROMOPICRIN
    4.
    发明申请
    CONTINUOUS PROCESS OF PREPARING BROMOPICRIN 有权
    连续制备BROMOPICRIN的方法

    公开(公告)号:US20100204528A1

    公开(公告)日:2010-08-12

    申请号:US12601547

    申请日:2008-05-26

    CPC classification number: C07C201/12 C07C205/08

    Abstract: A continuous process of preparing bromopicrin is disclosed. The process is effected by transferring a continuous flow of a first mixture and a continuous flow of a second mixture into a first reactor, the first mixture containing nitromethane and bromine and the second mixture containing an aqueous solution of an alkaline substance, to thereby obtain a reaction mixture which comprises bromopicrin in said first reactor; and collecting the bromopicrin from the reaction mixture. Highly pure bromopicrin obtained by this process is also disclosed.

    Abstract translation: 公开了制备溴氰菊酯的连续方法。 该方法通过将第一混合物的连续流和第二混合物的连续流转移到第一反应器中,第一混合物含有硝基甲烷和溴,第二混合物含有碱性物质的水溶液,从而获得 在所述第一反应器中包含溴化苦素的反应混合物; 并从反应混合物中收集溴氰菊酯。 还公开了通过该方法获得的高纯度溴氰菊酯。

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