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    HYDROBROMINATION METHOD
    4.
    发明申请
    HYDROBROMINATION METHOD 审中-公开
    液相色谱法

    公开(公告)号：US20160185705A1

    公开(公告)日：2016-06-30

    申请号：US14909775

    申请日：2014-08-07

    Applicant: ARKEMA FRANCE

    Inventor： Bernard BERTHE ,  Bernard PEES ,  Philippe ANNOOT ,  Jean-Luc DUBOIS ,  Ornella ZOVI

    IPC: C07C51/363 ,  C08G69/08 ,  C07C227/08

    Abstract: A process for synthesizing a product of formula Br—(CH2)n—R by hydrobromination, by reacting: a reagent of formula (I) R1-CH═CH—R2 in which R1 and R2, identical or different, are chosen from H or an alkyl radical comprising 1 to 30 carbon atoms, which is saturated or unsaturated, linear or branched, functionalized or non-functionalized, with a molar excess of HBr relative to the reagent of formula (I), in the presence of a radical initiator, and optionally in the presence of at least one solvent, said process including a step A of mixing at least reagent I and the HBr, each of the latter arriving in the form of a flow of liquid into a mixing device dA.

    Abstract translation: 通过氢溴酸合成式Br-（CH2）n-R的产物的方法，通过使式（I）的试剂R1-CH = CH-R2反应，其中R1和R2相同或不同，选自H 或包含1至30个碳原子的烷基，其在自由基引发剂存在下是饱和或不饱和的，官能化或非官能化的，具有相对于式（I）的试剂的摩尔过量的HBr ，并且任选地在至少一种溶剂的存在下，所述方法包括将至少试剂I和HBr混合的步骤A，后者各自以液体流的形式进入混合装置dA。

    CROSS METATHESIS PROCESS
    5.
    发明申请
    CROSS METATHESIS PROCESS 有权
    交叉过程

    公开(公告)号：US20150344416A1

    公开(公告)日：2015-12-03

    申请号：US14654663

    申请日：2014-01-07

    Applicant: ARKEMA FRANCE

    Inventor： Jean-Luc DUBOIS ,  Jean-Luc COUTURIER

    IPC: C07C253/30 ,  C07C227/04

    CPC classification number: C07C6/04 ,  C07C227/04 ,  C07C253/30 ,  C07C255/23

    Abstract: A process for the synthesis of an unsaturated product by cross metathesis between a first unsaturated compound having at least 8 carbon atoms and a second unsaturated compound having less than 8 carbon atoms, the first unsaturated compound being capable of producing an unsaturated coproduct comprising more than 14 carbon atoms, by homometathesis, said process including at least one production phase which includes: feeding a reactor with the first unsaturated compound; feeding the reactor with the second unsaturated compound; feeding the reactor with at least a first metathesis catalysts, then feeding the reactor with at least a second metathesis catalyst; withdrawing a product stream arising from the reactor; the turnover number of the first catalyst being higher than the turnover number of the second catalyst so as to achieve the same target degree of conversion of the first unsaturated compound.

    Abstract translation: 一种通过具有至少8个碳原子的第一不饱和化合物与具有少于8个碳原子的第二不饱和化合物之间的交叉复分解合成不饱和产物的方法，所述第一不饱和化合物能够产生包含超过14个碳原子的不饱和共聚物 碳原子，所述方法包括至少一个生产阶段，其包括：向第一不饱和化合物进料反应器; 向第二不饱和化合物进料反应器; 向所述反应器中加入至少第一复分解催化剂，然后向所述反应器供入至少第二复分解催化剂; 取出反应堆产生的产物流; 所述第一催化剂的周转数高于所述第二催化剂的周转数，以达到与所述第一不饱和化合物相同的目标转化率。

    HYDROGEN STORAGE BY MEANS OF DERIVATIVES OF COMPOUNDS OF RENEWABLE ORIGIN
    7.
    发明公开
    HYDROGEN STORAGE BY MEANS OF DERIVATIVES OF COMPOUNDS OF RENEWABLE ORIGIN 审中-公开

    公开(公告)号：US20230227306A1

    公开(公告)日：2023-07-20

    申请号：US17999063

    申请日：2021-10-07

    Applicant: ARKEMA FRANCE

    Inventor： Jean-Luc DUBOIS ,  Bernard MONGUILLON

    IPC: C01B3/00

    CPC classification number: C01B3/0015

    Abstract: The present invention relates to the use of a formulation which is liquid at ambient temperature comprising at least one terpene derivative for the fixing and the release of hydrogen in at least one hydrogenation/dehydrogenation cycle of said formulation.
    The invention also relates to the use of said formulation for the transportation and the handling of hydrogen resulting from the steam cracking of petroleum products, of inevitable hydrogen resulting from chemical reactions, such as the electrolysis of salt, or of hydrogen resulting from the electrolysis of water.

    PROCESS FOR THE SYNTHESIS OF OMEGA-UNSATURATED NITRILE-ACID/ESTER IN WHICH TWO TYPES OF CROSS METATHESIS ARE ALTERNATED CONSECUTIVELY, SWING PROCESS
    10.
    发明申请
    PROCESS FOR THE SYNTHESIS OF OMEGA-UNSATURATED NITRILE-ACID/ESTER IN WHICH TWO TYPES OF CROSS METATHESIS ARE ALTERNATED CONSECUTIVELY, SWING PROCESS 审中-公开
    合成不饱和硝酸酯/酯的方法，其中两种类型的交联物质被相互交替排列，挥发过程

    公开(公告)号：US20150336879A1

    公开(公告)日：2015-11-26

    申请号：US14759573

    申请日：2013-01-07

    Applicant: ARKEMA FRANCE

    Inventor： Jean-Luc DUBOIS ,  Jean-Luc COUTURIER

    IPC: C07C253/30 ,  C08G69/00 ,  C07C227/04

    CPC classification number: C07C227/04 ,  C07C253/30 ,  C07C2531/28 ,  C08G69/00 ,  C08G69/04 ,  C08G69/08 ,  C07C255/23 ,  C07C229/08

    Abstract: A process for the synthesis of a monounsaturated nitrile-ester (acid) by cross metathesis starting from an unsaturated compound I including at least one trivalent nitrile, acid or ester functional group, wherein the process includes a stage in which two types of cross metathesis are alternated consecutively: — a first type of cross metathesis cm1 with an acrylic compound II chosen from acrylonitrile, acrylic acid or an acrylic ester, one of the compounds I or II including a nitrile functional group and the other of these compounds II or I including an acid or ester functional group, and—a second type of cross metathesis cm2 with a light C2 to C4 alkene compound III. Also, a process for the synthesis of an α,ω-amino ester (acid) obtained by a process including a stage in which the two types of cross metathesis defined above are alternated consecutively, followed by a hydrogenation stage.

    Abstract translation: 通过包含至少一种三价腈，酸或酯官能团的不饱和化合物I从交叉复分解合成单不饱和腈 - 酯（酸）的方法，其中该方法包括两种类型的交叉复分解为 交替连续： - 第一种类型的交叉复分解cm1，丙烯酸化合物II选自丙烯腈，丙烯酸或丙烯酸酯，化合物I或II之一包括腈官能团，而这些化合物II或I中的另一种包括 酸或酯官能团，和具有轻的C2至C4烯烃化合物III的第二类型的交叉复分解cm2。 此外，合成通过包括上述定义的两种类型的交叉复分解的阶段的方法获得的α，ω-氨基酯（酸）的方法连续交替，随后是氢化阶段。

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