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公开(公告)号：US4316857A
公开(公告)日：1982-02-23
申请号：US86035
申请日：1979-10-18
Applicant: Arthur H. Gilbert
Inventor： Arthur H. Gilbert
IPC: C07B61/00 , B01J31/00 , B01J31/02 , B01J31/12 , C07C67/00 , C07C253/00 , C07C255/04 , C07C255/09 , C07C120/00 , C07C121/20
CPC classification number: C07C255/00 , B01J31/0259 , B01J31/0261
Abstract: A process for the dimerization of acrylonitrile to dicyanobutene and methylene-glutaronitrile under the influence of a phosphinite or phosphonite catalyst uses as solvent a mixture of proton-donating organic solvent, an aromatic hydrocarbon solvent and an aliphatic hydrocarbon solvent in a specified ratio so facilitating product isolation by phase separation or liquid/liquid extraction.
Abstract translation: 在亚磷酸盐或亚膦酸盐催化剂的影响下，将丙烯腈二聚成二氰丁烯和亚甲基 - 戊二腈的方法以特定的比例用作质子供体的有机溶剂，芳族烃溶剂和脂族烃溶剂的溶剂作为溶剂，从而便于产物 通过相分离或液/液萃取分离。
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公开(公告)号：US4147883A
公开(公告)日：1979-04-03
申请号：US708737
申请日：1976-07-26
Applicant: Arthur H. Gilbert
Inventor： Arthur H. Gilbert
CPC classification number: C07C51/316
Abstract: A cycloalkylhydroperoxide is converted to an alkane-dicarboxylic acid of the same number of carbon atoms, e.g. cyclohexylhydroperoxide to adipic acid, by reaction with nitrogen dioxide.
Abstract translation: 将环烷基氢过氧化物转化为相同数目碳原子的烷 - 二羧酸，例如 环己基氢过氧化物与己二酸反应，与二氧化氮反应。
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公开(公告)号：US5051495A
公开(公告)日：1991-09-24
申请号：US195610
申请日：1988-05-18
Applicant: Philip Staniland , Arthur H. Gilbert , Ian R. M. Henderson
Inventor： Philip Staniland , Arthur H. Gilbert , Ian R. M. Henderson
CPC classification number: C08G75/0209 , C08G65/46
Abstract: In making polyarylethersulphones or polyaryletherketones or their thioanalogues by reaction of phenols with aromatic halogen compounds, raw polycondensation product is freed of alkali halide by adjusting its composition and/or temperature so that it dissolves at least 0.5% w/w of water and holds the polymer in solution, and then contacting it in liquid form with hot water, preferably under pressure.
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