Abstract:
Fine-crystalline cast charges with an unoriented crystal structure of TNT or explosive charges containing TNT are obtained by adding 2,2'',4,4'', 6, 6''-hexanitrostilbene to the melt from which the cast charge is made.
Abstract:
3-ACETAMIDO-5-AMINOBENZOIC ACID IS A VALUABLE INTERMEDIATE FOR THE PREPARATION OF DRUGS ESPECIALLY FOR CERTAIN TYPES OF IODINE COMPOUNDS WHICH ARE USED AS X-ray contrast agents. According to the present invention it is prepared by acetylating of 3,5diaminobenzoic acid in an aqueous solution in the presence of a mineral acid. The 3-acetamido-5-aminobenzoic acid is then obtained in the form of its salt of the mineral acid from which salt the desired free acid may be recovered by adding a base. The free acid is obtained in high yields and of high purity.
WHERE AR AND AR1 ARE PHENYL OR SUBSTITUTED PHENYL ARE COVERTED TO THE CORRESPONDING KETONES WITH NITRIC ACID IN THE PRESENCE OF AN ORGANIC SOLVENT WHICH IS IMMISCIBLE WITH AND RESISTANT TO OXIDATION BY NITRIC ACID.