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    PROCESS AND APPARATUS FOR THE PRODUCTION OF HIGHER ALCOHOLS
    1.
    发明申请
    PROCESS AND APPARATUS FOR THE PRODUCTION OF HIGHER ALCOHOLS 有权
    用于生产高级酒精的方法和装置

    公开(公告)号：US20150315109A1

    公开(公告)日：2015-11-05

    申请号：US14651083

    申请日：2013-12-18

    Applicant: HALDOR TOPSØE A/S

    Inventor： Hassan Modarresi ,  Christian Wix

    IPC: C07C29/152 ,  C07C29/32

    CPC classification number: C07C29/152 ,  C07C29/32 ,  C07C31/04 ,  C07C31/08 ,  C07C31/12

    Abstract: In a process for the production of higher alcohols, i.e. C4+ alcohols, from syngas, the syngas is first reacted in a heterogeneous alcohol pre-converter (A) using an alcohol synthesis catalyst, whereby methanol as the main product in a concentration corresponding to or close to the equilibrium A concentration is produced. Then the effluent from the pre-converter is mixed with unconverted wet recycle gas and reacted in a heterogeneous reactor for higher alcohols synthesis (B) containing a higher alcohols synthesis catalyst, and finally the effluent from the reactor for higher alcohols synthesis is separated into (i) unconverted syngas, which is recycled to the higher alcohols synthesis reactor, (ii) methanol and light alcohols, which are recycled to the higher alcohols synthesis reactor, and (iii) the final product consisting of higher alcohols.

    Abstract translation: 在从合成气生产高级醇（即C4 +醇）的方法中，合成气首先在异构醇转化器（A）中使用醇合成催化剂进行反应，其中甲醇作为主要产物，浓度对应于或 接近平衡产生浓度。 然后将来自预转化器的流出物与未转化的湿循环气体混合，并在含有较高级醇合成催化剂的高级醇合成（B）的非均相反应器中反应，最后来自用于高级醇合成的反应器的流出物被分离成 i）未转化的合成气，其被再循环到高级醇合成反应器中，（ii）再循环到高级醇合成反应器中的甲醇和轻质醇，和（iii）由高级醇组成的最终产物。

    Methanol synthesis process layout for large production capacity
    2.
    发明授权
    Methanol synthesis process layout for large production capacity 有权

    公开(公告)号：US10478798B2

    公开(公告)日：2019-11-19

    申请号：US16083549

    申请日：2017-03-23

    Applicant: Haldor Topsøe A/S

    Inventor： Hassan Modarresi

    IPC: B01J8/06 ,  B01J19/24 ,  C07C29/152 ,  B01J8/02

    Abstract: A process layout for large scale methanol synthesis comprises one or more boiling water reactors and one or more radial flow reactors in series, the boiling water reactor(s) being fed with approximately fresh make-up syngas. The methanol synthesis loop comprises a make-up gas compressor K1, a recycle gas compressor K2, two or more boiling water converters for methanol synthesis (A1, A2, . . . ), a radial flow converter (B) for methanol synthesis, a steam drum (V1), a high pressure separator (V2), a low pressure separator (V3), feed effluent heat exchangers (E1 and E2), a wash column (C), an air cooler (E3) and a water cooler (E4).

    PROCESS FOR THE PREPARATION OF METHANOL IN PARALLEL REACTORS
    3.
    发明申请
    PROCESS FOR THE PREPARATION OF METHANOL IN PARALLEL REACTORS 有权
    在平行反应器中制备甲醇的方法

    公开(公告)号：US20160107961A1

    公开(公告)日：2016-04-21

    申请号：US14892124

    申请日：2014-05-15

    Applicant: HALDOR TOPSØE A/S

    Inventor： Hassan Modarresi ,  Christian Wix

    IPC: C07C29/152 ,  B01J19/18 ,  B01J8/02

    CPC classification number: C07C29/152 ,  B01J8/0292 ,  B01J8/0453 ,  B01J19/1856 ,  B01J2208/00274 ,  B01J2208/027 ,  C07C31/04

    Abstract: In a process for the preparation of methanolin parallel reactors, comprising the steps of (a) reacting carbon oxides and hydrogen in the presence of a methanol catalyst in a first methanol reactor to obtain a first methanol-containing effluent, (b) introducing and reacting unconverted synthesis gas in a second methanol reactor in the presence of a methanol catalyst to obtain a second methanol-containing effluent, the first methanol reactor and the second methanol reactor being connected in parallel, (c) combining the first and second effluent, and (d) cooling and separating the combined and cooled effluent into a methanol-containing liquid phase and unconverted synthesis gas, the methanol catalyst in the first methanol reactor is indirectly cooled by boiling water and the methanol catalyst in the second methanol reactor is either directly or indirectly cooled by the unconverted synthesis gas prior to conversion into the second effluent.

    Abstract translation: 在制备甲醇并行反应器的方法中，包括以下步骤：（a）在甲醇催化剂存在下，在第一甲醇反应器中使碳氧化物和氢气反应，得到第一含甲醇的流出物，（b）引入和反应 未转化的合成气在第二甲醇反应器中在甲醇催化剂存在下得到第二含甲醇的流出物，第一甲醇反应器和第二甲醇反应器并联连接，（c）将第一和第二流出物与（ d）冷却并将合并后的流出物分离成含甲醇的液相和未转化的合成气，第一甲醇反应器中的甲醇催化剂由沸水间接冷却，第二甲醇反应器中的甲醇催化剂直接或间接地 在转化成第二流出物之前由未转化的合成气冷却。

    Process for the preparation of methanol in parallel reactors
    7.
    发明授权
    Process for the preparation of methanol in parallel reactors 有权
    在并联反应器中制备甲醇的方法

    公开(公告)号：US09464014B2

    公开(公告)日：2016-10-11

    申请号：US14892124

    申请日：2014-05-15

    Applicant: Haldor Topsøe A/S

    Inventor： Hassan Modarresi ,  Christian Wix

    IPC: C07C27/00 ,  C07C29/152 ,  B01J8/04 ,  B01J8/02 ,  B01J19/18

    CPC classification number: C07C29/152 ,  B01J8/0292 ,  B01J8/0453 ,  B01J19/1856 ,  B01J2208/00274 ,  B01J2208/027 ,  C07C31/04

    Abstract: In a process for the preparation of methanolin parallel reactors, comprising the steps of (a) reacting carbon oxides and hydrogen in the presence of a methanol catalyst in a first methanol reactor to obtain a first methanol-containing effluent, (b) introducing and reacting unconverted synthesis gas in a second methanol reactor in the presence of a methanol catalyst to obtain a second methanol-containing effluent, the first methanol reactor and the second methanol reactor being connected in parallel, (c) combining the first and second effluent, and (d) cooling and separating the combined and cooled effluent into a methanol-containing liquid phase and unconverted synthesis gas, the methanol catalyst in the first methanol reactor is indirectly cooled by boiling water and the methanol catalyst in the second methanol reactor is either directly or indirectly cooled by the unconverted synthesis gas prior to conversion into the second effluent.

    Abstract translation: 在制备甲醇并行反应器的方法中，包括以下步骤：（a）在甲醇催化剂存在下，在第一甲醇反应器中使碳氧化物和氢气反应，得到第一含甲醇的流出物，（b）引入和反应 未转化的合成气在第二甲醇反应器中在甲醇催化剂存在下得到第二含甲醇的流出物，第一甲醇反应器和第二甲醇反应器并联连接，（c）将第一和第二流出物与（ d）冷却并将合并后的流出物分离成含甲醇的液相和未转化的合成气，第一甲醇反应器中的甲醇催化剂由沸水间接冷却，第二甲醇反应器中的甲醇催化剂直接或间接地 在转化成第二流出物之前由未转化的合成气冷却。

    Method for methanol synthesis
    8.
    发明授权
    Method for methanol synthesis 有权

    公开(公告)号：US10308576B2

    公开(公告)日：2019-06-04

    申请号：US15569527

    申请日：2016-05-10

    Applicant: Haldor Topsøe A/S

    Inventor： Per Juul Dahl ,  Hassan Modarresi ,  Max Thorhauge

    IPC: C07C29/151 ,  C07C31/04 ,  B01D3/06 ,  B01L3/06 ,  C01B3/12

    Abstract: In a process for methanol production from synthesis gas, which comprises the steps of providing a make-up gas containing hydrogen and carbon monoxide, in which the content of carbon dioxide is less than 0.1 mole %, mixing the make-up gas with a hydrogen-rich recycle gas and passing the gas mixture to a methanol synthesis reactor, optionally via a sulfur guard, and subjecting the effluent from the synthesis reactor to a separation step, thereby providing crude methanol and the hydrogen-rich recycle gas, the customary addition of carbon dioxide to the make-up gas is replaced by addition of water in an amount of 0.1 to 5 mole %. This way, a CO2 compressor is saved, and the amount of poisonous sulfur in the make-up gas is markedly reduced.

    A NOVEL METHOD FOR METHANOL SYNTHESIS
    9.
    发明申请
    A NOVEL METHOD FOR METHANOL SYNTHESIS 审中-公开

    公开(公告)号：US20180305281A1

    公开(公告)日：2018-10-25

    申请号：US15569527

    申请日：2016-05-10

    Applicant: Haldor Topsøe A/S

    Inventor： Per Juul Dahl ,  Hassan Modarresi ,  Max Thorhauge

    IPC: C07C29/151 ,  C07C31/04 ,  B01D3/06

    CPC classification number: C07C29/1518 ,  B01D3/06 ,  B01D2257/70 ,  C01B3/12 ,  C01B2203/061 ,  C01B2203/1223 ,  C07C31/04

    Abstract: In a process for methanol production from synthesis gas, which comprises the steps of providing a make-up gas containing hydrogen and carbon monoxide, in which the content of carbon dioxide is less than 0.1 mole %, mixing the make-up gas with a hydrogen-rich recycle gas and passing the gas mixture to a methanol synthesis reactor, optionally via a sulfur guard, and subjecting the effluent from the synthesis reactor to a separation step, thereby providing crude methanol and the hydrogen-rich recycle gas, the customary addition of carbon dioxide to the make-up gas is replaced by addition of water in an amount of 0.1 to 5 mole %. This way, a CO2 compressor is saved, and the amount of poisonous sulfur in the make-up gas is markedly reduced.

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