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公开(公告)号:US20170113212A1
公开(公告)日:2017-04-27
申请号:US15127881
申请日:2014-10-15
Applicant: HALDOR TOPSØE A/S
Inventor: Ton V.W. Janssens , Peter N.R. Vennestrøm
CPC classification number: B01J29/85 , B01D53/9418 , B01D2251/2062 , B01D2251/208 , B01D2255/20761 , B01D2255/50 , B01J29/084 , B01J29/84 , B01J37/0018 , B01J37/0036 , B01J37/0238 , B01J37/04 , B01J37/08 , B01J37/30 , B01J38/08 , B01J2229/183 , B01J2229/186 , B01J2229/38 , B01J2229/40 , C01B39/54 , F01N3/208 , F01N2370/02 , F01N2570/14 , F01N2610/02 , F01N2610/03 , F01N2610/10 , Y02P20/584
Abstract: Method for the preparation of a metal exchanged crystalline microporous metalloaluminophosphate or mixtures containing metal exchanged microporous metalloaluminophosphates materials comprising the steps of providing a dry mixture containing a) one or more metalloaluminophosphates starting materials that exhibit ion exchange capacity, and b) one or more metal compounds; heating the mixture in a gaseous atmosphere containing ammonia to a temperature and for a time sufficient to initiate and perform a solid state ion exchange of ions of the metal compound and ions of the crystalline microporous material; and obtaining the metal-exchanged microporous metalloaluminophosphate material or mixtures containing the metal-exchanged microporous metalloaluminophosphate material.
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2.
公开(公告)号:US20170095804A1
公开(公告)日:2017-04-06
申请号:US15126171
申请日:2014-10-15
Applicant: HALDOR TOPSØE A/S
Inventor: Ton V.W. Janssens , Peter N.R. Vennestrøm
CPC classification number: B01J29/46 , B01D53/9418 , B01D2251/2062 , B01D2251/208 , B01D2255/20738 , B01D2255/20746 , B01D2255/20761 , B01D2255/50 , B01D2255/504 , B01J29/061 , B01J29/072 , B01J29/146 , B01J29/24 , B01J29/68 , B01J29/7607 , B01J29/7615 , B01J29/763 , B01J29/83 , B01J29/85 , B01J37/0018 , B01J37/0036 , B01J37/0238 , B01J37/04 , B01J37/08 , B01J37/30 , B01J38/08 , B01J2229/183 , B01J2229/186 , B01J2229/38 , B01J2229/40
Abstract: Method for the preparation of a metal-exchanged zeolites or mixtures of metal-exchanged zeolites, such as Cu-SSZ-13, Cu-ZSM-S, Cu-beta, or Fe-beta, comprising the steps of providing a dry mixture of a) one or more microporous zeotype materials that exhibit ion exchange capacity and b) one or more metal compounds; heating the mixture in a gaseous atmosphere containing ammonia to a temperature lower than 300° C. for a time sufficient to initiate and perform a solid state ion exchange of ions of the metal compound and ions of the zeolite material; and obtaining the metal-exchanged zeolitematerial.
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