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公开(公告)号：US08911878B2
公开(公告)日：2014-12-16
申请号：US13755415
申请日：2013-01-31
Applicant: Integran Technologies, Inc.
Inventor： Klaus Tomantschger , Jonathan McCrea , Nandakumar Nagarajan , Francisco Gonzalez , Gino Palumbo , Konstantinos Panagiotopoulos , Herath Katugaha
IPC: B32B1/08 , B32B7/04 , B32B15/04 , B32B15/08 , C25D7/00 , C23C18/16 , C08J7/12 , B32B7/12 , B32B37/24 , B32B37/12
CPC classification number: B32B7/04 , B32B1/08 , B32B7/12 , B32B15/043 , B32B15/08 , B32B37/1284 , B32B2037/246 , B32B2307/202 , B32B2311/00 , C08J7/123 , C23C18/1641 , C23C18/165 , C25D7/00 , Y10T156/10 , Y10T428/12028 , Y10T428/12049 , Y10T428/12389 , Y10T428/12451 , Y10T428/12472 , Y10T428/12569 , Y10T428/12632 , Y10T428/12896 , Y10T428/12944 , Y10T428/131 , Y10T428/1352 , Y10T428/1355 , Y10T428/1359 , Y10T428/24545 , Y10T428/24612 , Y10T428/2495 , Y10T428/26 , Y10T428/263 , Y10T428/269 , Y10T428/31678
Abstract: Metal-clad polymer articles containing structural fine-grained and/or amorphous metallic coatings/layers optionally containing solid particulates dispersed therein. The fine-grained and/or amorphous metallic coatings are particularly suited for strong and lightweight articles, precision molds, sporting goods, automotive parts and components exposed to thermal cycling although the CLTE of the metallic layer and the one of the substrate is mismatched. The interface between the metallic layer and the polymer is suitably pretreated to withstand thermal cycling without failure.
Abstract translation: 包含结构细晶粒和/或非晶金属涂层/层的金属包层聚合物制品任选地含有分散在其中的固体颗粒。 细晶粒和/或非晶金属涂层特别适用于强而轻的制品，精密模具，运动用品，暴露于热循环的汽车部件和部件，尽管金属层的CLTE和基板之一不匹配。 金属层和聚合物之间的界面适当地经过预处理以承受热循环而不失败。
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公开(公告)号：US20150111673A1
公开(公告)日：2015-04-23
申请号：US14513267
申请日：2014-10-14
Applicant: Integran Technologies Inc.
Inventor： Klaus Tomantschger , Jonathan McCrea , Nandakumar Nasarajan , Francisco Gonzalez , Gino Palumbo , Konstantinos Panagiotopoulos , Herath Katugaha , Diana Facchini , Jared Victor , Uwe Erb
IPC: C23C18/16 , C09J163/00 , A63B59/14
CPC classification number: C23C18/1641 , A63B59/70 , A63B2102/24 , B32B1/08 , B32B3/30 , B32B7/02 , B32B15/08 , B32B15/18 , B32B15/20 , B32B27/08 , B32B27/16 , B32B27/18 , B32B27/20 , B32B27/281 , B32B27/285 , B32B27/288 , B32B27/302 , B32B27/304 , B32B27/308 , B32B27/32 , B32B27/322 , B32B27/34 , B32B27/36 , B32B27/365 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2255/06 , B32B2255/10 , B32B2255/20 , B32B2255/205 , B32B2262/101 , B32B2262/106 , B32B2264/02 , B32B2264/10 , B32B2264/12 , B32B2270/00 , B32B2307/202 , B32B2307/212 , B32B2307/30 , B32B2307/51 , B32B2307/538 , B32B2307/54 , B32B2307/718 , B32B2457/00 , B32B2509/00 , B32B2535/00 , B32B2597/00 , B32B2605/00 , C09J163/00 , C23C14/021 , C23C14/024 , C23C14/028 , C23C16/0227 , C23C16/0254 , C23C16/0272 , C23C18/1855 , C23C18/1893 , C23C18/1896 , C25D5/54 , Y10T428/12111 , Y10T428/12389 , Y10T428/12451 , Y10T428/12472 , Y10T428/12569 , Y10T428/12944 , Y10T428/1355 , Y10T428/24355 , Y10T428/24545 , Y10T428/24612 , Y10T428/26 , Y10T428/269
Abstract: The fine-grained and/or amorphous metallic coatings are particularly suited for strong and lightweight sporting goods exposed to thermal cycling although the coefficient of linear thermal expansion (CLTE) of the metallic layer and the substrate are mismatched.
Abstract translation: 细晶粒和/或非晶金属涂层特别适用于暴露于热循环的强和轻的运动用品，尽管金属层和基材的线性热膨胀系数（CLTE）不匹配。
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公开(公告)号：US08691397B2
公开(公告)日：2014-04-08
申请号：US13665052
申请日：2012-10-31
Applicant: Integran Technologies, Inc.
Inventor： Diana Facchini , Francisco Gonzalez , Jonathan McCrea , Mike Uetz , Gino Palumbo , Klaus Tomantschger
CPC classification number: C25D3/562 , C25D3/12 , C25D3/26 , C25D5/18 , C25D5/50 , C25D15/00 , Y10T428/12049 , Y10T428/12493 , Y10T428/12861 , Y10T428/12937 , Y10T428/12993 , Y10T428/13 , Y10T428/24942 , Y10T428/24967 , Y10T428/26 , Y10T428/263 , Y10T428/264 , Y10T428/265
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基底的强度，磨损和/或润滑性，而不降低疲劳性能。 包含Co的细粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其它应力和/或需要抗微生物性能的应用中的制品。
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公开(公告)号：US10060016B2
公开(公告)日：2018-08-28
申请号：US15003259
申请日：2016-01-21
Applicant: INTEGRAN TECHNOLOGIES INC.
Inventor： Gino Palumbo , Iain Brooks , Klaus Tomantschger , Peter Lin , Karl Aust , Nandakumar Nagarajan , Francisco Gonzalez
Abstract: Polycrystalline materials are prepared by electrodeposition of a precursor material that is subsequently heat-treated to induce at least a threefold increase in the grain size of the material to yield a relatively high fraction of ‘special’ low Σ grain boundaries and a randomized crystallographic texture. The precursor metallic material has sufficient purity and a fine-grained microstructure (e.g., an average grain size of 4 nm to 5 μm). The resulting metallic material is suited to the fabrication of articles requiring high mechanical or physical isotropy and/or resistance to grain boundary-mediated deformation or degradation mechanisms.
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Patent Agency Ranking
5.发明授权Electrodeposited metallic coatings comprising cobalt with enhanced fatigue properties 有权包含钴的电沉积金属涂层具有增强的疲劳性能公开(公告)号：US08663819B2
公开(公告)日：2014-03-04
申请号：US13673017
申请日：2012-11-09
Applicant: Integran Technologies, Inc.
Inventor： Francisco Gonzalez , Diana Facchini , Jonathan McCrea , Mike Uetz , Gino Palumbo , Klaus Tomantschger
CPC classification number: C25D7/00 , B32B15/01 , B32B15/013 , B32B15/017 , C22C19/07 , C23C30/00 , C25D3/12 , C25D3/562 , C25D5/18 , C25D5/50 , C25D7/04 , C25D15/00 , Y10T428/12458 , Y10T428/12493 , Y10T428/12625 , Y10T428/12729 , Y10T428/1275 , Y10T428/12778 , Y10T428/12861 , Y10T428/12882 , Y10T428/1291 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/12972 , Y10T428/12979 , Y10T428/13 , Y10T428/24942 , Y10T428/24967 , Y10T428/26 , Y10T428/263 , Y10T428/264 , Y10T428/265
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness chromium coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基材的强度，磨损和/或润滑性，而不降低与未涂覆或等效厚度的铬涂覆的基材相比的疲劳性能。 包含Co的细粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其它应力和/或需要抗微生物性能的应用中的制品。
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公开(公告)号：US09970120B2
公开(公告)日：2018-05-15
申请号：US14997636
申请日：2016-01-18
Applicant: Integran Technologies Inc.
Inventor： Klaus Tomantschger , Diana Facchini , Francisco Gonzalez , Jonathan McCrea , John Kratochwil , Dan Woloshyn , Yusuf Bismilla , Nandakumar Nagarajan , Mioara Neacsu
Abstract: A method for electrodepositing a coating/free-standing layer on a workpiece in an electrolytic cell includes moving the workpiece and an anode applicator tool having a consumable anode insert relative to each other; anodically dissolving a metal from the insert and cathodically depositing the metal on the workpiece; providing flow of electrolyte solution through the insert to ensure that greater than 90% of the anodic reaction is represented by dissolution of the metal; recirculating collected electrolyte solution exiting the electrolytic cell through the insert; applying an electric current to the electrolytic cell; maintaining a concentration of the anodically dissolved metal within ±25% of each Ampere-hour per liter of electroplating solution; and creating a cathodic electrodeposit on the workpiece which includes the anodically dissolved metal, the chemical composition of the deposit varying by less than 25% in the deposition direction over a selected thickness of up to 25 microns of the deposit.
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公开(公告)号：US08916248B2
公开(公告)日：2014-12-23
申请号：US13756755
申请日：2013-02-01
Applicant: Integran Technologies, Inc.
Inventor： Jonathan McCrea , Francisco Gonzalez , Gino Palumbo , Klaus Tomantschger , Rich Emrich , Konstantinos Panagiotopoulos , Mary Pasquantonio , John Kratochwil , Herath Katugaha
IPC: B32B1/00 , B32B1/02 , B32B1/08 , B32B15/04 , B32B15/08 , B32B27/14 , B32B27/20 , F16L9/02 , F16L9/147 , B32B15/16 , C23C18/20 , C23C18/16 , C08J7/12 , C08J7/04 , B32B5/16 , C23C18/30 , C25D7/00
CPC classification number: B32B15/08 , B32B5/16 , B32B15/043 , B32B15/16 , B32B27/14 , C08J7/04 , C08J7/045 , C08J7/123 , C08J2323/06 , C23C18/1601 , C23C18/165 , C23C18/20 , C23C18/2006 , C23C18/2013 , C23C18/2086 , C23C18/2093 , C23C18/22 , C23C18/30 , C23C24/04 , C23C28/00 , C23C28/021 , C23C28/023 , C25D7/00 , Y10T428/12049 , Y10T428/12479 , Y10T428/12882 , Y10T428/13 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1355 , Y10T428/1359 , Y10T428/1372 , Y10T428/1376 , Y10T428/1379 , Y10T428/1386 , Y10T428/1393 , Y10T428/24997 , Y10T428/25 , Y10T428/256 , Y10T428/257 , Y10T428/259 , Y10T428/269 , Y10T428/31678
Abstract: Metal-coated polymer articles containing structural substantially porosity-free, fine-grained and/or amorphous metallic coatings/layers optionally containing solid particulates dispersed therein on polymer substrates, are disclosed. The substantially porosity-free metallic coatings/layers/patches are applied to polymer or polymer composite substrates to provide, enhance or restore vacuum/pressure integrity and fluid sealing functions. Due to the excellent adhesion between the metallic coating and the polymer article satisfactory thermal cycling performance is achieved. The fine-grained and/or amorphous metallic coatings are particularly suited for strong and lightweight articles, precision molds, sporting goods, aerospace and automotive parts and other components exposed to thermal cycling and stress created by erosion and impact damage.
Abstract translation: 公开了包含基本上无孔隙结构，细粒度和/或无定形金属涂层/层的金属涂覆的聚合物制品，其任选地包含分散在聚合物基材上的固体颗粒。 将基本上无孔隙的金属涂层/层/贴片施加到聚合物或聚合物复合基材上以提供，增强或恢复真空/压力完整性和流体密封功能。 由于金属涂层和聚合物制品之间优异的粘合性，可实现令人满意的热循环性能。 细粒度和/或无定形金属涂层特别适用于强而轻的制品，精密模具，运动用品，航空航天和汽车零件以及暴露于热循环和受冲击和冲击损坏产生的应力的其他部件。
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公开(公告)号：US20130337288A1
公开(公告)日：2013-12-19
申请号：US13975696
申请日：2013-08-26
Applicant: Integran Technologies Inc.
Inventor： Diana Facchini , Francisco Gonzalez , Jonathan McCrea , Mike Uetz , Gino Palumbo , Klaus Tomantschger , Nandakumar Nagarajan , Jared J. Victor , Uwe Erb
IPC: B32B15/01
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness Cr coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial and hydrophobic properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基材的强度，磨损和/或润滑性，而不降低与未涂覆或等效厚度的Cr涂覆的基材相比的疲劳性能。 包含Co的细晶粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其他应力的物品和/或需要抗微生物和疏水性质的应用中。
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9.发明申请公开(公告)号：US20160130713A1
公开(公告)日：2016-05-12
申请号：US14997636
申请日：2016-01-18
Applicant: Integran Technologies Inc.
Inventor： Klaus Tomantschger , Diana Facchini , Francisco Gonzalez , Jonathan McCrea , John Kratochwil , Dan Woloshyn , Yusuf Bismilla , Nandakumar Nagarajan , Mioara Neacsu
Abstract: A method for electrodepositing a coating/free-standing layer on a workpiece in an electrolytic cell includes moving the workpiece and an anode applicator tool having a consumable anode insert relative to each other; anodically dissolving a metal from the insert and cathodically depositing the metal on the workpiece; providing flow of electrolyte solution through the insert to ensure that greater than 90% of the anodic reaction is represented by dissolution of the metal; recirculating collected electrolyte solution exiting the electrolytic cell through the insert; applying an electric current to the electrolytic cell; maintaining a concentration of the anodically dissolved metal within ±25% of each Ampere-hour per liter of electroplating solution; and creating a cathodic electrodeposit on the workpiece which includes the anodically dissolved metal, the chemical composition of the deposit varying by less than 25% in the deposition direction over a selected thickness of up to 25 microns of the deposit.
Abstract translation: 一种用于在电解池中将工件上的涂层/独立层电沉积的方法包括相对于彼此移动工件和具有可消耗阳极插入件的阳极施用工具; 将金属从插入物阳极溶解并将金属阴极沉积在工件上; 提供电解质溶液通过插入物的流动，以确保大于90％的阳极反应由金属的溶解表示; 通过插入物再循环离开电解池的收集的电解质溶液; 向电解槽施加电流; 将阳极溶解的金属的浓度保持在每升电镀溶液的每安培小时的±25％内; 并且在包括阳极溶解的金属的工件上产生阴极电沉积物，沉积物的沉积方向上的沉积物的化学成分在沉积方向上选择厚度高达25微米的选定厚度变化小于25％。
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