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    Olefin metathesis catalyst compositions comprising at least two metal carbene olefin metathesis catalysts
    4.
    发明授权
    Olefin metathesis catalyst compositions comprising at least two metal carbene olefin metathesis catalysts 有权

    公开(公告)号：US09598531B2

    公开(公告)日：2017-03-21

    申请号：US14843448

    申请日：2015-09-02

    Applicant: MATERIA, INC.

    Inventor： Anthony R. Stephen ,  Christopher J. Cruce ,  Michael A. Giardello

    IPC: C08F4/80 ,  B01J31/28 ,  C08G61/08 ,  C08F132/08 ,  C08F32/00

    CPC classification number: C08G61/08 ,  B01J31/28 ,  B01J2231/14 ,  B01J2231/54 ,  B01J2531/821 ,  C08F4/80 ,  C08F32/00 ,  C08F132/08 ,  C08G2261/11 ,  C08G2261/135 ,  C08G2261/3325 ,  C08G2261/418 ,  C08G2261/76

    Abstract: This invention relates to olefin metathesis catalysts and methods for controlling olefin metathesis reactions. More particularly, the present invention relates to methods and compositions for catalyzing and controlling ring opening metathesis polymerization (ROMP) reactions and the manufacture of polymer articles via ROMP. This invention also relates to olefin metathesis catalyst compositions comprising at least two metal carbene olefin metathesis catalysts, wherein the at least two metal carbene olefin metathesis catalysts are structurally different, are chemically different, are distinct compounds, are not isomers, are not structural isomers, are not diastereoisomers, are not stereoisomers, are not enantiomers, or are not cis/trans isomers of each other, or any combinations thereof. This invention also relates to a ROMP composition comprising a resin composition comprising at least one cyclic olefin, and an olefin metathesis catalyst composition comprising at least two metal carbene olefin metathesis catalysts, wherein the at least two metal carbene olefin metathesis catalysts are structurally different, are chemically different, are distinct compounds, are not isomers, are not structural isomers, are not diastereoisomers, are not stereoisomers, are not enantiomers, or are not cis/trans isomers of each other, or any combinations thereof. This invention also relates to a method of making an article comprising combining an olefin metathesis catalyst composition comprising at least two metal carbene olefin metathesis catalysts with a resin composition comprising at least one cyclic olefin, thereby forming a ROMP composition, and subjecting the ROMP composition to conditions effective to polymerize the ROMP composition, wherein the at least two metal carbene olefin metathesis catalysts are structurally different, are chemically different, are distinct compounds, are not isomers, are not structural isomers, are not diastereoisomers, are not stereoisomers, are not enantiomers, or are not cis/trans isomers of each other, or any combinations thereof. Polymer products produced via the metathesis reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.

    ADHESION PROMOTERS AND GEL-MODIFIERS FOR OLEFIN METATHESIS COMPOSITIONS
    5.
    发明申请
    ADHESION PROMOTERS AND GEL-MODIFIERS FOR OLEFIN METATHESIS COMPOSITIONS 有权

    公开(公告)号：US20220089481A1

    公开(公告)日：2022-03-24

    申请号：US17365433

    申请日：2021-07-01

    Applicant: MATERIA, INC.

    Inventor： Li-Sheng Wang ,  Anthony R. Stephen ,  Paul W. Boothe ,  Tessa Schulze ,  Michael A. Giardello ,  Mark S. Trimmer ,  Christopher J. Cruce ,  Farshad J. Motamedi ,  Brian Edgecombe

    IPC: C03C25/30 ,  C08F32/02 ,  C08K5/00 ,  C08K5/14 ,  C08K5/29

    Abstract: This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyanate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.

    Thermal insulation
    8.
    发明授权
    Thermal insulation 有权

    公开(公告)号：US10711090B2

    公开(公告)日：2020-07-14

    申请号：US15122860

    申请日：2014-12-23

    Applicant: MATERIA, INC.

    Inventor： Christopher J. Cruce ,  Michael A. Giardello ,  Brian L. Conley ,  Anthony R. Stephen

    IPC: C08G61/02 ,  F16L59/20 ,  C08G61/08 ,  C08L65/00 ,  F16L58/10 ,  C09D165/00 ,  B05D7/22 ,  F16L59/14 ,  F16L59/02 ,  F16L58/18

    Abstract: The present invention is directed to addressing one or more of the aforementioned concerns and relates to thermal insulation materials and thermal insulation material compositions and methods for thermally insulating pipelines and associated equipment, structures, and objects used in offshore drilling. The present invention is directed to articles of manufacture comprising the thermal insulation materials and/or thermal insulation material compositions of the invention. More particularly the present invention relates to the use of ring opening metathesis polymerization polymers (ROMP polymers) and/or ROMP polymer composites for thermally insulating pipelines and associated equipment, structures, and objects used in offshore oil drilling.

    Method and composition for improving adhesion of metathesis compositions to substrates
    9.
    发明授权
    Method and composition for improving adhesion of metathesis compositions to substrates 有权

    公开(公告)号：US10059857B2

    公开(公告)日：2018-08-28

    申请号：US15413703

    申请日：2017-01-24

    Applicant: MATERIA, INC.

    Inventor： Anthony R. Stephen ,  Christopher J. Cruce ,  Mark S. Trimmer ,  Michael A. Giardello

    IPC: C09D145/00 ,  C09D143/00

    CPC classification number: C09D143/00 ,  C09D143/04

    Abstract: A method of improving the adhesion of metathesis compositions, such as ring-opening metathesis polymerization (ROMP) compositions, to a substrate is disclosed, in which an adhesion promoter is added to a polymerizable resin composition in order to improve the adhesion of the polymerizing resin to a substrate material. The addition of the adhesion promoter has been found to provide beneficial improvements in the adhesion of metathesis, especially ROMP, compositions to substrates, particularly glass surfaces, leading to improved characteristics in ROMP materials formed therefrom. The adhesion promoter generally comprises a functionalized silane compound and a peroxide compound. A ROMP composition is further disclosed comprising a cyclic olefin, a ROMP metathesis catalyst, and the adhesion promoter. Polymer products produced via metathesis (ROMP) reactions of the invention may be utilized to provide a wide range of materials and in a variety of composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.

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