公开(公告)号：US20150369727A1

公开(公告)日：2015-12-24

申请号：US14489244

申请日：2014-09-17

Applicant: SHIMADZU CORPORATION

Inventor： Mikio SUGIOKA

IPC: G01N21/31 ,  C12Q1/06 ,  G01N33/06 ,  G01N33/14 ,  G01N21/3577 ,  G01N21/33

CPC classification number: G01N21/31 ,  G01N21/33 ,  G01N21/3577 ,  G01N21/359 ,  G01N33/06 ,  G01N33/14 ,  G01N2201/065

Abstract: A method and an apparatus that make an easy and quick measurement of the concentration of materials in a suspension possible with high precision and without essentially changing the structure of the conventional spectrometer for pre-dispersive spectrometry are provided by nullifying the limitation of a container of a sample as compared to transmission measurement. A spectrometer equipped with an integrating sphere is used to measure the reflection spectrum from a suspension in a container when the suspension is irradiated with measurement light, of which the wavelengths are selected from a wavelength range including near infrared, reflection spectra of a number of types of standard samples, of which the concentrations in the suspension are already known, are used to prepare a measurement model in accordance with an assay technique on the basis of a recursion, and the concentration of a material in the suspension is found using the measurement model.

Abstract translation: 提供了一种方法和装置，其可以以高精度容易且快速地测量悬浮液中材料的浓度，并且基本上不改变用于预分散光谱的常规光谱仪的结构，这是通过以下方式提供的： 样品与传输测量相比。 当使用测量光照射悬浮液时，配备有积分球的光谱仪用于测量来自容器中的悬浮液的反射光谱，其中波长选自包括近红外的波长范围，多种类型的反射光谱 标准样品（其中悬浮液中的浓度已知）用于根据递推法根据测定技术制备测量模型，并且使用测量模型发现悬浮液中的材料的浓度 。