Method and apparatus for sampling
    1.
    发明授权
    Method and apparatus for sampling 失效
    采样方法和装置

    公开(公告)号:US3668936A

    公开(公告)日:1972-06-13

    申请号:US3668936D

    申请日:1970-12-15

    Inventor: HERRON RAND E

    CPC classification number: G01N35/1095 G01N1/38 G01N35/08

    Abstract: There is provided a method and apparatus for sampling a viscous liquid by aspiration of such liquid from a container in an offtake tube of a probe insertable in the container. A reagent having the characteristic of a solvent is added to the sample to dilute it within the probe after a relatively short distance of travel of the sample within the probe. The reagent is fed into the probe at a first predetermined flow rate and the admixture is aspirated at a second predetermined flow rate which is faster so that the sample is aspirated at a rate determined by the difference between the first and second flow rates.

    Abstract translation: 提供了一种用于通过从可插入容器中的探针的取出管中的容器中抽吸这种液体来对粘性液体进行取样的方法和装置。 将具有溶剂特性的试剂加入到样品中,以在样品在探针内的相对较短距离的行程之后在探针内稀释。 试剂以第一预定流速进料到探针中,并且混合物以更快的第二预定流速抽吸,以便以由第一和第二流速之间的差确定的速率抽吸样品。

    Burner construction for flame spectrophotometer and system therefor
    2.
    发明授权
    Burner construction for flame spectrophotometer and system therefor 失效
    燃烧器结构用于火焰分光光度计及其系统

    公开(公告)号:US3695812A

    公开(公告)日:1972-10-03

    申请号:US3695812D

    申请日:1970-10-30

    CPC classification number: G01N21/72 F23D91/02 F23D2206/0094

    Abstract: There is provided a spectral flame burner of the preatomizer type having a sample tube the outlet of which is disposed within a carrier gas conduit terminating in a nozzle. The spacing between the outlet of the sample tube and the outlet of the nozzle is adjustable during the normal operation of the analyzer system, including the burner. Improved means is provided to withdraw the outlet of the sample tube to a position in which sufficient gas pressure is developed in the sample tube to blow out any obstruction in the latter, including a lead screw mechanism operatively associated with the sample tube. The burner has an improved cap construction and a control system is provided for the burner to safely shut down the burner when a defect is detected in the burner system.

    Abstract translation: 提供了预分解器类型的光谱火焰燃烧器,其具有样品管,样品管的出口设置在终止于喷嘴中的载体气体导管内。 在分析仪系统(包括燃烧器)的正常操作期间,样品管的出口与喷嘴出口之间的间距是可调节的。 提供改进的装置以将样品管的出口抽出到样品管中产生足够的气体压力的位置,以吹出后者中的任何障碍物,包括与样品管可操作地相关联的丝杠机构。 燃烧器具有改进的盖结构,并且当在燃烧器系统中检测到缺陷时,为燃烧器提供控制系统以安全地关闭燃烧器。

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