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1.发明授权公开(公告)号：US11535703B2
公开(公告)日：2022-12-27
申请号：US17161067
申请日：2021-01-28
Applicant: The Texas A&M University System
Inventor： Lei Fang , Zi-Hao Guo , Chenxu Wang , Qiang Zhang , Hong-Cai Zhou
IPC: C08G61/10 , B01J20/26 , B01J20/20 , B01J20/28 , B01J20/30 , B01D15/16 , B01D67/00 , C08G61/12 , B01D71/06 , B01D71/44 , C08G61/02 , C08J9/28 , B01D61/02 , B01D61/14
Abstract: The present disclosure relates to synthesis of porous polymer networks and applications of such materials. The present disclosure relates to a method of fabricating of a porous polymer network comprising: (a) providing: (i) a first reactant comprising a plurality of compounds comprising at least one acetyl group, said plurality of compounds comprising at least one compound type, and (ii) a second reactant comprising an alkylsulfonic acid, and (b) creating a solution of said reactants, (c) casting said solution in a form, and (d) treating said solution under such conditions so as to produce a porous polymer network. In one embodiment, the invention relates to a porous polymer network which has a basic structure selected from the group consisting of
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公开(公告)号：US09409116B2
公开(公告)日：2016-08-09
申请号：US14405653
申请日：2012-12-13
Applicant: THE TEXAS A&M UNIVERSITY SYSTEM
Inventor： Hong-Cai Zhou , Julian Sculley , Weigang Lu
CPC classification number: B01D53/04 , B01D53/02 , B01D2253/202 , B01D2256/10 , B01D2257/504 , B01D2257/7025 , B01D2259/4525 , B01J20/265 , B01J20/267 , B01J20/28066 , C08J9/00 , C08J2365/00 , C08J2383/00 , C08J2385/00 , F17C11/007 , Y02C10/08 , Y02C20/20 , Y02P20/152 , Y02P20/156
Abstract: Functionalized Porous Polymer Networks (PPNs) exhibiting favourable characteristics such as high surface area′ and gas uptake properties are disclosed, including methods of making such networks. A method of preparing a porous polymer network, comprising: (a) a step of homo-coupling a monomer in the presence of 2,2′-bipyridyl, 1,5-cycloocta-1,5-diene, a mixed solvent of DMF/THF and a compound or mixture selected from the group consisting of bis(1,5-cydoocta-1,5-diene)nickel(0), Ni(PPH3) 4, and Zn/NiCI2/NaBr/PPH3 at a temperature in the range of 20 to 40° C. These stable PPNs may be useful in the context of carbon capture, gas storage and separation, and as supports for catalysts.
Abstract translation: 公开了表现出有利特征如高表面积和气体吸收性能的功能化多孔聚合物网络（PPN），包括制备这种网络的方法。 一种制备多孔聚合物网络的方法，包括：（a）在2,2'-联吡啶，1,5-环辛-1,5-二烯，DMF的混合溶剂存在下使单体均相偶联的步骤 / THF和选自双（1,5-环己基-1,5-二烯）镍（0），Ni（PPH 3）4和Zn / NiCl 2 / NaBr / PPH 3的化合物或混合物，温度为 范围为20至40℃。这些稳定的PPN可用于碳捕获，气体储存和分离以及作为催化剂的载体。
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3.发明申请公开(公告)号：US20210230359A1
公开(公告)日：2021-07-29
申请号：US17161067
申请日：2021-01-28
Applicant: The Texas A&M University System
Inventor： Lei Fang , Zi-Hao Guo , Chenxu Wang , Qiang Zhang , Hong-Cai Zhou
IPC: C08G61/10 , B01J20/26 , B01J20/20 , B01J20/28 , B01J20/30 , B01D15/16 , B01D67/00 , C08J9/28 , C08G61/12 , B01D71/06 , B01D71/44 , C08G61/02
Abstract: The present disclosure relates to synthesis of porous polymer networks and applications of such materials. The present disclosure relates to a method of fabricating of a porous polymer network comprising: (a) providing: (i) a first reactant comprising a plurality of compounds comprising at least one acetyl group, said plurality of compounds comprising at least one compound type, and (ii) a second reactant comprising an alkylsulfonic acid, and (b) creating a solution of said reactants, (c) casting said solution in a form, and (d) treating said solution under such conditions so as to produce a porous polymer network. In one embodiment, the invention relates to a porous polymer network which has a basic structure selected from the group consisting of
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4.发明授权公开(公告)号：US10934389B2
公开(公告)日：2021-03-02
申请号：US16744736
申请日：2020-01-16
Applicant: The Texas A&M University System
Inventor： Lei Fang , Zi-Hao Guo , Chenxu Wang , Qiang Zhang , Hong-Cai Zhou
IPC: C08G61/10 , B01J20/26 , B01J20/20 , B01J20/28 , B01J20/30 , B01D15/16 , B01D67/00 , C08J9/28 , C08G61/12 , B01D71/06 , B01D71/44 , C08G61/02 , B01D61/02 , B01D61/14
Abstract: The present disclosure relates to synthesis of porous polymer networks and applications of such materials. The present disclosure relates to a method of fabricating of a porous polymer network comprising: (a) providing: (i) a first reactant comprising a plurality of compounds comprising at least one acetyl group, said plurality of compounds comprising at least one compound type, and (ii) a second reactant comprising an alkylsulfonic acid, and (b) creating a solution of said reactants, (c) casting said solution in a form, and (d) treating said solution under such conditions so as to produce a porous polymer network. In one embodiment, the invention relates to a porous polymer network which has a basic structure selected from the group consisting of
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公开(公告)号：US20150182903A1
公开(公告)日：2015-07-02
申请号：US14405653
申请日：2012-12-13
Applicant: THE TEXAS A&M UNIVERSITY SYSTEM
Inventor： Hong-Cai Zhou , Julian Sculley , Weigang Lu
CPC classification number: B01D53/04 , B01D53/02 , B01D2253/202 , B01D2256/10 , B01D2257/504 , B01D2257/7025 , B01D2259/4525 , B01J20/265 , B01J20/267 , B01J20/28066 , C08J9/00 , C08J2365/00 , C08J2383/00 , C08J2385/00 , F17C11/007 , Y02C10/08 , Y02C20/20 , Y02P20/152 , Y02P20/156
Abstract: Functionalized Porous Polymer Networks (PPNs) exhibiting favourable characteristics such as high surface area′ and gas uptake properties are disclosed, including methods of making such networks. A method of preparing a porous polymer network, comprising: (a) a step of homo-coupling a monomer in the presence of 2,2′-bipyridyl, 1,5-cycloocta-1,5-diene, a mixed solvent of DMF/THF and a compound or mixture selected from the group consisting of bis(1,5-cydoocta-1,5-diene)nickel(o), Ni(PPH3) 4, and Zn/NiCI2/NaBr/PPH3 at a temperature in the range of 20 to 40° C. These stable PPNs may be useful in the context of carbon capture, gas storage and separation, and as supports for catalysts.
Abstract translation: 公开了表现出有利特征如高表面积和气体吸收性能的功能化多孔聚合物网络（PPN），包括制备这种网络的方法。 一种制备多孔聚合物网络的方法，包括：（a）在2,2'-联吡啶，1,5-环辛-1,5-二烯，DMF的混合溶剂存在下使单体均相偶联的步骤 / THF和选自双（1,5-环己基-1,5-二烯）镍（o），Ni（PPH 3）4和Zn / NiCl 2 / NaBr / PPH 3的化合物或混合物，温度为 范围为20至40℃。这些稳定的PPN可用于碳捕获，气体储存和分离以及作为催化剂的载体。
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Patent Agency Ranking
6.发明申请公开(公告)号：US20200148812A1
公开(公告)日：2020-05-14
申请号：US16744736
申请日：2020-01-16
Applicant: The Texas A&M University System
Inventor： Lei Fang , Zi-Hao Guo , Chenxu Wang , Qiang Zhang , Hong-Cai Zhou
IPC: C08G61/10 , B01D67/00 , C08G61/02 , B01D71/44 , B01D71/06 , C08G61/12 , C08J9/28 , B01D15/16 , B01J20/30 , B01J20/28 , B01J20/20 , B01J20/26
Abstract: The present disclosure relates to synthesis of porous polymer networks and applications of such materials. The present disclosure relates to a method of fabricating of a porous polymer network comprising: (a) providing: (i) a first reactant comprising a plurality of compounds comprising at least one acetyl group, said plurality of compounds comprising at least one compound type, and (ii) a second reactant comprising an alkylsulfonic acid, and (b) creating a solution of said reactants, (c) casting said solution in a form, and (d) treating said solution under such conditions so as to produce a porous polymer network. In one embodiment, the invention relates to a porous polymer network which has a basic structure selected from the group consisting of
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7.发明申请公开(公告)号：US20180194891A1
公开(公告)日：2018-07-12
申请号：US15863095
申请日：2018-01-05
Applicant: The Texas A&M University System
Inventor： Lei Fang , Zi-Hao Guo , Chenxu Wang , Qiang Zhang , Hong-Cai Zhou
IPC: C08G61/10 , C08J9/28 , B01J20/26 , B01J20/20 , B01J20/28 , B01J20/30 , C08G61/12 , B01D15/16 , B01D67/00
Abstract: The present disclosure relates to synthesis of porous polymer networks and applications of such materials.
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8.发明授权公开(公告)号：US10584201B2
公开(公告)日：2020-03-10
申请号：US15863095
申请日：2018-01-05
Applicant: The Texas A&M University System
Inventor： Lei Fang , Zi-Hao Guo , Chenxu Wang , Qiang Zhang , Hong-Cai Zhou
IPC: C08G61/10 , B01J20/26 , B01J20/20 , B01J20/28 , B01D15/16 , B01D67/00 , C08J9/28 , C08G61/12 , B01D71/06 , B01D71/44 , C08G61/02 , B01J20/30 , B01D61/02 , B01D61/14
Abstract: The present disclosure relates to synthesis of porous polymer networks and applications of such materials. The present disclosure relates to a method of fabricating of a porous polymer network comprising: (a) providing: (i) a first reactant comprising a plurality of compounds comprising at least one acetyl group, said plurality of compounds comprising at least one compound type, and (ii) a second reactant comprising an alkylsulfonic acid, and (b) creating a solution of said reactants, (c) casting said solution in a form, and (d) treating said solution under such conditions so as to produce a porous polymer network. In one embodiment, the invention relates to a porous polymer network which has a basic structure selected from the group consisting of
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公开(公告)号：US09951095B2
公开(公告)日：2018-04-24
申请号：US15307267
申请日：2015-05-11
Applicant: The Texas A&M University System
Inventor： Hong-Cai Zhou , Tian-Fu Liu , Xizhen Lian , Lanfang Zou , Dawei Feng
CPC classification number: C07F11/005 , C07F7/28 , C07F15/025
Abstract: The present invention relates to monocrystalline metal organic frameworks comprising chromium ions and carboxylate ligands and the use of the same, for example their use for storing a gas. The invention also relates to methods for preparing metal organic frameworks comprising chromium, titanium or iron ions and carboxylate ligands. The methods of the invention allow such metal organic frameworks to be prepared in monocrystalline or polycrystalline forms.
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公开(公告)号：US09724668B2
公开(公告)日：2017-08-08
申请号：US15165247
申请日：2016-05-26
Applicant: The Texas A&M University System
Inventor： Hong-Cai Zhou , Dawei Feng , Kecheng Wang
IPC: C07C29/147 , B01J20/22 , C07F15/02 , C07F15/04 , C07F15/06 , C07F5/06 , C07F7/00 , B01J20/28 , C01B3/00 , C01B3/50 , C01B21/04 , C01B31/20 , C07C7/13 , C07F7/28
CPC classification number: B01J20/226 , B01J20/28057 , B01J20/28061 , B01J20/28066 , B01J20/28069 , B01J20/28071 , B01J20/28073 , B01J20/28076 , C01B3/0015 , C01B3/508 , C01B21/0455 , C01B32/50 , C01B32/914 , C01B2210/0015 , C07C7/13 , C07F5/06 , C07F5/069 , C07F7/003 , C07F7/28 , C07F15/02 , C07F15/025 , C07F15/04 , C07F15/045 , C07F15/06 , C07F15/065 , Y02E60/324
Abstract: The invention relates to an improved process for preparing metal-organic framework materials, metal-organic frameworks obtainable by such processes, methods using the same, and the use thereof. The process of the invention provides an improved process for preparing metal-organic frameworks in particular monocrystalline metal-organic frameworks having large crystal sizes. The invention also relates to metal organic frameworks comprising iron or titanium, and their uses.
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