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    Incorporation of bulk metal foils to increase toughness of polycrystalline diamond
    1.
    发明授权
    Incorporation of bulk metal foils to increase toughness of polycrystalline diamond 有权
    加入大块金属箔以增加多晶金刚石的韧性

    公开(公告)号：US09555519B2

    公开(公告)日：2017-01-31

    申请号：US14547867

    申请日：2014-11-19

    Applicant: DIAMOND INNOVATIONS, INC.

    Inventor： Abhijit Prabhakar Suryavanshi

    IPC: B22F7/06 ,  E21B10/567 ,  B24D3/06 ,  B22F5/00 ,  B24D99/00 ,  C22C26/00 ,  E21B10/573 ,  B01J3/06 ,  B24D18/00

    CPC classification number: B24D3/06 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0655 ,  B01J2203/0685 ,  B22F5/00 ,  B22F7/06 ,  B24D18/0009 ,  B24D99/005 ,  C22C26/00 ,  E21B10/567 ,  E21B10/573

    Abstract: A cutting element include a substrate and a diamond compact including at least two polycrystalline diamond portions separated by at least one metal carbide foil portion. The cutting element is made by placing diamond powder in a reaction container, placing a thin metal layer in the reaction container above or around the diamond powder and binder, placing additional diamond powder in the reaction container above or around the thin metal layer, and placing a pre-sintered substrate containing binder into the reaction container above all diamond powder and thin metal layer components. The assembled reaction container is put into a reactor and is subjected to a high-temperature high-pressure sintering process. The binder in the pre-sintered substrate sweeps through to sinter the first diamond portion, and then reacts with the thin metal layer to form a metal carbide, and then the binder continues to sweep through to sinter the second diamond portion.

    Abstract translation: 切割元件包括基底和金刚石致密体，其包括由至少一个金属碳化物箔部分分开的至少两个多晶金刚石部分。 切割元件通过将金刚石粉末放置在反应容器中，将金属薄层放置在金刚石粉末和粘合剂上方或周围的反应容器中，在金属层上方或周围将反应容器中的另外的金刚石粉末放置在反应容器中， 将包含粘合剂的预烧结基材置于反应容器中，高于所有金刚石粉末和薄金属层组分。 将组装的反应容器放入反应器中并进行高温高压烧结工艺。 预烧结衬底中的粘合剂扫过以烧结第一金刚石部分，然后与薄金属层反应形成金属碳化物，然后粘合剂继续扫过以烧结第二金刚石部分。

    INCORPORATION OF BULK METAL FOILS TO INCREASE TOUGHNESS OF POLYCRYSTALLINE DIAMOND
    2.
    发明申请
    INCORPORATION OF BULK METAL FOILS TO INCREASE TOUGHNESS OF POLYCRYSTALLINE DIAMOND 审中-公开
    膨胀金属箔增加多晶金刚石的韧度

    公开(公告)号：US20150202741A1

    公开(公告)日：2015-07-23

    申请号：US14547867

    申请日：2014-11-19

    Applicant: DIAMOND INNOVATIONS, INC.

    Inventor： Abhijit Prabhakar Suryavanshi

    IPC: B24D3/06 ,  B24D18/00

    CPC classification number: B24D3/06 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0655 ,  B01J2203/0685 ,  B22F5/00 ,  B22F7/06 ,  B24D18/0009 ,  B24D99/005 ,  C22C26/00 ,  E21B10/567 ,  E21B10/573

    Abstract: A cutting element include a substrate and a diamond compact including at least two polycrystalline diamond portions separated by at least one metal carbide foil portion. The cutting element is made by placing diamond powder in a reaction container, placing a thin metal layer in the reaction container above or around the diamond powder and binder, placing additional diamond powder in the reaction container above or around the thin metal layer, and placing a pre-sintered substrate containing binder into the reaction container above all diamond powder and thin metal layer components. The assembled reaction container is put into a reactor and is subjected to a high-temperature high-pressure sintering process. The binder in the pre-sintered substrate sweeps through to sinter the first diamond portion, and then reacts with the thin metal layer to form a metal carbide, and then the binder continues to sweep through to sinter the second diamond portion.

    Abstract translation: 切割元件包括基底和金刚石致密体，其包括由至少一个金属碳化物箔部分分开的至少两个多晶金刚石部分。 切割元件通过将金刚石粉末放置在反应容器中，将金属薄层放置在金刚石粉末和粘合剂上方或周围的反应容器中，在金属层上方或周围将反应容器中的另外的金刚石粉末放置在反应容器中， 将包含粘合剂的预烧结基材置于反应容器中，高于所有金刚石粉末和薄金属层组分。 将组装的反应容器放入反应器中并进行高温高压烧结工艺。 预烧结衬底中的粘合剂扫过以烧结第一金刚石部分，然后与薄金属层反应形成金属碳化物，然后粘合剂继续扫过以烧结第二金刚石部分。

    POLYCRYSTALLINE COMPACTS, EARTH-BORING TOOLS INCLUDING SUCH COMPACTS, AND METHODS OF FABRICATING POLYCRYSTALLINE COMPACTS
    3.
    发明申请
    POLYCRYSTALLINE COMPACTS, EARTH-BORING TOOLS INCLUDING SUCH COMPACTS, AND METHODS OF FABRICATING POLYCRYSTALLINE COMPACTS 有权
    聚合物复合材料，包括这种复合材料的接地工具以及制备聚合物复合材料的方法

    公开(公告)号：US20150144407A1

    公开(公告)日：2015-05-28

    申请号：US14090018

    申请日：2013-11-26

    Applicant: Baker Hughes Incorporated

    Inventor： Valery N. Khabashesku ,  Vladimir P. Filonenko

    IPC: E21B10/56 ,  B24D18/00 ,  E21B10/55 ,  B24D3/06

    CPC classification number: E21B10/567 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/0685 ,  B24D3/06 ,  B24D18/0009

    Abstract: A polycrystalline compact includes diamond grains, cubic boron nitride grains, and grains of an additional nitride, carbide, or boride. The additional nitride, carbide, or boride may be aluminum nitride, gallium nitride, silicon nitride, titanium nitride, silicon carbide, titanium carbide, titanium boride, titanium diboride, and/or aluminum boride. The diamond grains, the cubic boron nitride grains, and the grains of the additional nitride, carbide, or boride are intermixed and interbonded to form a polycrystalline material. An earth-boring tool includes a bit body and such a polycrystalline diamond compact secured to the bit body. Methods of fabricating polycrystalline compacts include forming a mixture comprising diamond grains, non-cubic boron nitride grains, and a metal or semimetal; encapsulating the mixture in a container; and subjecting the encapsulated mixture to high-pressure and high-temperature conditions to form a polycrystalline material.

    Abstract translation: 多晶压块包括金刚石晶粒，立方氮化硼晶粒和另外的氮化物，碳化物或硼化物的晶粒。 另外的氮化物，碳化物或硼化物可以是氮化铝，氮化镓，氮化硅，氮化钛，碳化硅，碳化钛，硼化钛，二硼化钛和/或硼化铝。 金刚石晶粒，立方氮化硼晶粒和附加氮化物，碳化物或硼化物的晶粒混合并键合以形成多晶材料。 钻孔工具包括钻头体和固定在钻头体上的这种多晶金刚石砂块。 制造多晶压块的方法包括形成包含金刚石晶粒，非立方氮化硼晶粒和金属或半金属的混合物; 将混合物包封在容器中; 并将包封的混合物经受高压和高温条件以形成多晶材料。

    Polycrystalline diamond compacts including at least one transition layer and methods for stress management in polycrsystalline diamond compacts
    4.
    发明授权
    Polycrystalline diamond compacts including at least one transition layer and methods for stress management in polycrsystalline diamond compacts 有权
    包括至少一个过渡层的多晶金刚石压块和多晶金刚石压块中的应力管理方法

    公开(公告)号：US08727046B2

    公开(公告)日：2014-05-20

    申请号：US13087775

    申请日：2011-04-15

    Applicant: David P. Miess ,  Kenneth E. Bertagnolli ,  Damon B. Crockett ,  Arnold D. Cooper

    Inventor： David P. Miess ,  Kenneth E. Bertagnolli ,  Damon B. Crockett ,  Arnold D. Cooper

    IPC: E21B10/36 ,  E21B10/567

    CPC classification number: B24D3/007 ,  B01J3/062 ,  B01J2203/063 ,  B01J2203/0655 ,  B22F2005/001 ,  B24D18/0009 ,  C22C26/00 ,  E21B10/567 ,  E21B10/5735 ,  F16C33/043 ,  F16C2206/04 ,  F16C2352/00

    Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) that are less susceptible to liquid metal embrittlement damage due to the use of at least one transition layer between a polycrystalline diamond (“PCD”) layer and a substrate. In an embodiment, a PDC includes a PCD layer, a cemented carbide substrate, and at least one transition layer bonded to the substrate and the PCD layer. The at least one transition layer is formulated with a coefficient of thermal expansion (“CTE”) that is less than a CTE of the substrate and greater than a CTE of the PCD layer. At least a portion of the PCD layer includes diamond grains defining interstitial regions and a metal-solvent catalyst occupying at least a portion of the interstitial regions. The diamond grains and the catalyst collectively exhibit a coercivity of about 115 Oersteds or more and a specific magnetic saturation of about 15 Gauss·cm3/grams or less.

    Abstract translation: 实施例涉及由于在多晶金刚石（“PCD”）层和基底之间使用至少一个过渡层而对液态金属脆化损伤较不敏感的多晶金刚石压块（“PDC”）。 在一个实施例中，PDC包括PCD层，硬质合金基底和结合到基底和PCD层的至少一个过渡层。 所述至少一个过渡层被配制成具有小于衬底的CTE且大于PCD层的CTE的热膨胀系数（“CTE”）。 PCD层的至少一部分包括限定间隙区域的金刚石颗粒和占据间隙区域的至少一部分的金属溶剂催化剂。 金刚石颗粒和催化剂共同表现出约115奥斯特或更高的矫顽磁力和约15高斯·厘米3 /克或更低的特定磁饱和度。

    Method for producing a PCD compact
    5.
    发明授权
    Method for producing a PCD compact 有权
    生产PCD压块的方法

    公开(公告)号：US08485284B2

    公开(公告)日：2013-07-16

    申请号：US12995370

    申请日：2009-06-03

    Applicant: Humphrey Samkelo Lungisani Sithebe

    Inventor： Humphrey Samkelo Lungisani Sithebe

    IPC: E21B10/46 ,  E21B10/567

    CPC classification number: B01J3/065 ,  B01J2203/063 ,  B01J2203/0655 ,  B22F7/062 ,  C22C26/00 ,  C22C2204/00

    Abstract: A method of producing a composite diamond compact comprising a polycrystalline diamond (PCD) compact bonded to a cemented carbide substrate is provided. The method includes the steps of: providing a PCD table, preferably a PCD table with diamond-to-diamond bonding and a porous microstructure in which the pores are empty of second phase material bringing together the PCD table and a cemented carbide substrate in the presence of a bonding agent to form an unbonded assembly; subjecting the unbonded assembly to an initial compaction at a pressure of at least 4.5 GPa and a temperature below the melting point of the bonding agent for a period of at least 150 seconds; and thereafter subjecting the unbonded assembly to a temperature above the melting point of the bonding agent and a pressure of at least 4.5 GPa for a time sufficient for the bonding agent to become molten and bond the PCD table to the substrate to form a composite diamond compact.

    Abstract translation: 提供了一种制造复合金刚石复合体的方法，其包括结合到硬质合金基底的多晶金刚石（PCD）紧固件。 该方法包括以下步骤：提供PCD表，优选具有金刚石 - 金刚石结合的PCD表和多孔微结构，其中孔隙为空的第二相材料，在存在的情况下将PCD台和硬质合金基底聚集在一起 的粘合剂以形成未结合的组件; 使未结合的组件在至少4.5GPa的压力和低于粘合剂的熔点的温度下进行至少150秒的初始压实; 然后使未结合的组件经受高于粘合剂熔点的温度和至少4.5GPa的压力，持续一段时间足以使粘合剂熔融并将PCD工作台结合到衬底上以形成复合金刚石致密体 。

    FISCHER-TROPSCH CATALYSTS CONTAINING IRON OR COBALT SELECTIVE TOWARDS HIGHER HYDROCARBONS
    7.
    发明申请
    FISCHER-TROPSCH CATALYSTS CONTAINING IRON OR COBALT SELECTIVE TOWARDS HIGHER HYDROCARBONS 有权
    含有铁或钴的选择性催化剂选择性更高的碳氢化合物

    公开(公告)号：US20120245236A1

    公开(公告)日：2012-09-27

    申请号：US13072683

    申请日：2011-03-26

    Applicant: Steven L. Suib ,  Boxun Hu ,  Eric Rolland Kreidler ,  Christopher James Brooks

    Inventor： Steven L. Suib ,  Boxun Hu ,  Eric Rolland Kreidler ,  Christopher James Brooks

    IPC: B01J23/32 ,  C07C1/04 ,  C07C1/12 ,  B01J27/22

    CPC classification number: B01J35/002 ,  B01J23/34 ,  B01J23/8892 ,  B01J27/22 ,  B01J37/0201 ,  B01J37/16 ,  B01J37/18 ,  B01J2203/063 ,  B01J2229/183 ,  B01J2229/186 ,  C07C51/367 ,  C10G2/33 ,  C10G2/332 ,  C10G2/334 ,  C07C59/245

    Abstract: Cryptomelane-type manganese oxide octahedral molecular sieves (OMS-2) supported Fe and Co catalysts are utilized in a method for producing hydrocarbons by a Fischer-Tropsch mechanism. The hydrocarbon producing method includes providing a catalyst of a manganese oxide-based octahedral molecular sieve nanofibers with an active catalyst component of at least one of iron, cobalt, nickel, copper, manganese, vanadium, zinc, and mixtures thereof, and further containing an alkali metal. The formation of iron carbides and cobalt carbides by exposing the catalyst to conditions sufficient to form those carbides is also taught. After the catalyst has been appropriately treated, a carbon source and a hydrogen source are provided and contacted with the catalyst to thereby form a hydrocarbon containing product. The catalyst have high catalytic activity and selectivity (75%) for C2+ hydrocarbons in both CO hydrogenation and CO2 hydrogenation. Highly selective syntheses of high value jet fuel, C2-C6 alkenes, C2-C6 carboxylic acids; α-hydroxylic acids and their derivatives have been realized by tuning the oxidation ability of OMS-2 supports and by doping with Cu2+ ions.

    Abstract translation: 在通过费 - 托机制生产烃的方法中，使用了Cryportelane型锰氧化物八面体分子筛（OMS-2）负载的Fe和Co催化剂。 烃生产方法包括提供一种氧化锰基八面体分子筛纳米纤维的催化剂，其具有铁，钴，镍，铜，锰，钒，锌及其混合物中的至少一种的活性催化剂组分，并且还含有 碱金属。 还教导了通过将催化剂暴露于足以形成这些碳化物的条件来形成碳化铁和碳化钴。 在催化剂被适当处理之后，提供碳源和氢源并与催化剂接触，从而形成含烃产品。 该催化剂在CO氢化和二氧化碳加氢过程中对于C2 +烃具有较高的催化活性和选择性（75％）。 高选择性合成高价值喷气燃料，C2-C6烯烃，C2-C6羧酸; 通过调节OMS-2载体的氧化能力和掺杂Cu2 +离子已经实现了α-羟基酸及其衍生物。

    POLYCRYSTALLINE COMPACTS, EARTH-BORING TOOLS INCLUDING SUCH COMPACTS, AND METHODS OF FABRICATING POLYCRYSTALLINE COMPACTS
    9.
    发明申请
    POLYCRYSTALLINE COMPACTS, EARTH-BORING TOOLS INCLUDING SUCH COMPACTS, AND METHODS OF FABRICATING POLYCRYSTALLINE COMPACTS 审中-公开
    聚合物复合材料，包括这种复合材料的接地工具以及制备聚合物复合材料的方法

    公开(公告)号：US20170037688A1

    公开(公告)日：2017-02-09

    申请号：US15297882

    申请日：2016-10-19

    Applicant: Baker Hughes Incorporated

    Inventor： Valery N. Khabashesku ,  Vladimir P. Filonenko

    IPC: E21B10/567 ,  B24D3/06 ,  B24D18/00

    CPC classification number: E21B10/567 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/0685 ,  B24D3/06 ,  B24D18/0009

    Abstract: A polycrystalline compact includes diamond, cubic boron nitride, and at least one hard material, which may be aluminum nitride, gallium nitride, silicon nitride, titanium nitride, silicon carbide, titanium carbide, titanium boride, titanium diboride, and/or aluminum boride. The diamond, the cubic boron nitride, and the hard material are intermixed and interbonded to form a polycrystalline material. An earth-boring tool includes a bit body and a polycrystalline diamond compact secured to the bit body. Methods of fabricating polycrystalline compacts include forming a mixture comprising diamond, non-cubic boron nitride, and a metal or semimetal; encapsulating the mixture in a container; and subjecting the encapsulated mixture to high-pressure and high-temperature conditions to form a polycrystalline material.

    Abstract translation: 多晶结构体包括金刚石，立方氮化硼和至少一种硬质材料，其可以是氮化铝，氮化镓，氮化硅，氮化钛，碳化硅，碳化钛，硼化钛，二硼化钛和/或硼化铝。 将金刚石，立方氮化硼和硬质材料混合并键合以形成多晶材料。 钻孔工具包括固定在钻头体上的钻头体和多晶金刚石块。 制造多晶压块的方法包括形成包含金刚石，非立方氮化硼和金属或半金属的混合物; 将混合物包封在容器中; 并将包封的混合物经受高压和高温条件以形成多晶材料。

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