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    1,2-DIAMINOCYCLOHEXANE AND CHEMICAL PROCESS
    162.
    发明申请
    1,2-DIAMINOCYCLOHEXANE AND CHEMICAL PROCESS 审中-公开
    1,2-二氨基辛醇和化学工艺

    公开(公告)号：WO2010059420A1

    公开(公告)日：2010-05-27

    申请号：PCT/US2009/063227

    申请日：2009-11-04

    Applicant: INVISTA TECHNOLOGIES S.A.R.L. ,  AMEY, Ronald, L.

    Inventor： AMEY, Ronald, L.

    IPC: C07C209/72 ,  C07C209/70 ,  C07C211/51

    CPC classification number: C07C209/72 ,  C07C2601/14 ,  C07C211/36

    Abstract: Disclosed is a process for the preparation of 1,2-cycloaliphatic diamines from 1,2-aromatic diamines. In one embodiment, the process provides a method for making 1,2-diaminocyclohexane by the reaction of 1,2-phenylenediamine contained in a polar, protic solvent with hydrogen in the presence of a supported rhodium catalyst, ammonia, and a trialkylamine, and having enhanced overall conversion and selectivity.

    Abstract translation: 公开了从1,2-芳族二胺制备1,2-环脂族二胺的方法。 在一个实施方案中，该方法提供了在负载的铑催化剂，氨和三烷基胺的存在下，通过极性质子溶剂中的1,2-苯二胺与氢反应制备1,2-二氨基环己烷的方法，以及 具有增强的整体转化率和选择性。

    BULKED CONTINUOUS FILAMENTS WITH HEXALOBAL CROSS-SECTION AND THEREE VOIDS AND SPINNERET PLATES FOR PRODUCING THE FILAMENT
    165.
    发明申请
    BULKED CONTINUOUS FILAMENTS WITH HEXALOBAL CROSS-SECTION AND THEREE VOIDS AND SPINNERET PLATES FOR PRODUCING THE FILAMENT 审中-公开
    具有十字交叉部分的稠密连续薄膜和用于生产薄膜的THEEEE VOIDS和SpinNERET板

    公开(公告)号：WO2010021931A2

    公开(公告)日：2010-02-25

    申请号：PCT/US2009/053868

    申请日：2009-08-14

    Applicant: INVISTA TECHNOLOGIES S.A.R.L. ,  WAE-HAI, Tung

    Inventor： WAE-HAI, Tung

    IPC: D01D5/253 ,  D01D5/24

    CPC classification number: D01D5/253 ,  D01D5/24 ,  Y10T428/2975

    Abstract: Briefly described, embodiments of this disclosure include hexalobal bulked continuous filaments with three axial voids, spinneret plates with a capillary design for producing the hexalobal, tri-void bulked continuous filaments (BCFs) of the present disclosure, articles made from the hexalobal filaments of the present disclosure, methods of making the hexalobal, tri-void filaments of the present disclosure, and the like.

    Abstract translation: 简要描述，本公开的实施方案包括具有三个轴向空隙的六边形膨胀连续长丝，具有毛细管设计的喷丝板，用于制备本公开的六角形三孔膨体连续长丝（BCF），由六角形细丝制成的制品 本公开的内容，制备本公开的六价，三孔丝的方法等。

    IMPROVED PROCESS FOR MAKING TRIPHENYLBORON-PYRIDINE COMPOUND
    167.
    发明申请
    IMPROVED PROCESS FOR MAKING TRIPHENYLBORON-PYRIDINE COMPOUND 审中-公开
    改进的制备三苯基吡啶 - 化合物的方法

    公开(公告)号：WO2009100261A2

    公开(公告)日：2009-08-13

    申请号：PCT/US2009/033286

    申请日：2009-02-06

    Applicant: INVISTA TECHNOLOGIES S.A.R.L. ,  OSTERMAIER, John, J.

    Inventor： OSTERMAIER, John, J.

    IPC: C07D241/06

    CPC classification number: C07F5/027

    Abstract: A process for improving the recovery of solid triphenylboron-pyridine compound (TPBP), while retaining desirable particle characteristics comprises the addition of an acid to neutralize at least a portion of the alkali contained in the aqueous mother liquor. By adjusting the pH of the product slurry to between about 8.5 and about 12, it is possible to increase product recovery by more than 10 %, while maintaining desirable particle characteristics.

    Abstract translation: 改善固体三苯基硼 - 吡啶化合物（TPBP）的回收率同时保持所需颗粒特征的方法包括加入酸以中和含于所述含水母液中的至少一部分碱 。 通过将产物浆料的pH调节到约8.5和约12之间，可以将产品回收率提高10％以上，同时保持理想的颗粒特性。

    HYDROCYANATION OF PENTENENITRILES
    168.
    发明申请
    HYDROCYANATION OF PENTENENITRILES 审中-公开
    苯胺的水解

    公开(公告)号：WO2009091790A1

    公开(公告)日：2009-07-23

    申请号：PCT/US2009/030943

    申请日：2009-01-14

    Applicant: INVISTA TECHNOLOGIES S.A.R.L. ,  FOO, Thomas ,  GARNER, James, Michael ,  OZER, Ron ,  PEARLMAN, Paul, S.

    Inventor： FOO, Thomas ,  GARNER, James, Michael ,  OZER, Ron ,  PEARLMAN, Paul, S.

    IPC: C07C253/10 ,  B01J27/16 ,  B01J23/75

    CPC classification number: C07C253/10 ,  C07C255/04

    Abstract: The invention provides a hydrocyanation process to produce adiponitrile and other dinitriles having six carbon atoms, the process comprising: a) forming a reaction mixture in the presence of at least one Lewis acid, said reaction mixture comprising ethylenically unsaturated nitriles having five carbon atoms, hydrogen cyanide, and at least one catalyst composition, by continuously feeding the ethylenically unsaturated nitriles, the hydrogen cyanide, and the catalyst composition; wherein the catalyst composition comprises a zero-valent nickel and at least one bidentate phosphorus-containing ligand; the bidentate phosphorus-containing ligand is selected from the group consisting of a phosphite, a phosphonite, a phosphinite, a phosphine, and a mixed phosphorus-containing ligand or a combination of such members; and the bidentate phosphorus-containing ligand gives acceptable results according to at least one protocol of the 2-Pentenenitrile Hydrocyanation Test Method; b) controlling X and Z, wherein X is the overall feed molar ratio of 2- pentenenitriles to all unsaturated nitriles; and Z is the overall feed molar ratio of hydrogen cyanide to all unsaturated nitriles; by selecting a value for X in the range of about 0.001 to about 0.5; and a value for Z in the range of about 0.5 to about 0.99; such that the value of quotient Q, wherein Formula (I), is in the range from about 0.2 to about 10, wherein 3PN is 3-pentenenitriles and 4PN is 4-pentenenitrile; c) withdrawing a reaction product mixture comprising adiponitrile, 2- methylglutaronitrile, ethylenically unsaturated nitriles, the catalyst composition, and catalyst composition degradation products; and wherein the ratio of the concentration of 2-pentenenitriles to the concentration of 3-pentenenitriles in the reaction mixture is in the range from about 0.2/1 to about 10/1; d) extracting at least a portion of the reaction product mixture with an extraction agent selected from the group consisting of aliphatic hydrocarbons, cycloaliphatic hydrocarbons, and mixtures thereof to obtain an extract phase comprising the extraction agent and the catalyst composition and a raffinate phase comprising adiponitrile, 2-methylglutaronitrile, ethylenically unsaturated nitriles, catalyst composition degradation products, and the extraction agent; and e) distilling the extract phase to obtain a first stream comprising the extraction agent and a second stream comprising the catalyst composition.

    Abstract translation: 本发明提供了一种氢氰化方法，用于生产具有六个碳原子的己二腈和其它二腈，该方法包括：a）在至少一种路易斯酸存在下形成反应混合物，所述反应混合物包含具有五个碳原子的烯属不饱和腈，氢 氰化物和至少一种催化剂组合物，通过连续进料烯属不饱和腈，氰化氢和催化剂组合物; 其中所述催化剂组合物包含零价镍和至少一种二齿含磷配体; 二齿含磷配体选自亚磷酸盐，亚膦酸盐，膦酸盐，膦和混合的含磷配体或这些成员的组合; 并且根据2-戊烯腈氢氰化测试方法的至少一个方案，二齿含磷配体可得到可接受的结果; b）控制X和Z，其中X是2-戊烯腈与所有不饱和腈的总进料摩尔比; Z是氰化氢与所有不饱和腈的总进料摩尔比; 通过选择约0.001至约0.5范围内的X的值; 并且Z的值在约0.5至约0.99的范围内; 使得其中式（I）的范围在约0.2至约10的范围内的商Q的值，其中3PN是3-戊烯腈，4PN是4-戊烯腈; c）取出包含己二腈，2-甲基戊二腈，烯属不饱和腈，催化剂组合物和催化剂组合物降解产物的反应产物混合物; 并且其中所述2-戊烯腈的浓度与所述反应混合物中3-戊烯腈的浓度的比率在约0.2 / 1至约10/1的范围内; d）用选自脂族烃，脂环族烃及其混合物的萃取剂萃取反应产物混合物的至少一部分，以获得包含萃取剂和催化剂组合物的提取相，以及含有己二腈的萃余相 ，2-甲基戊二腈，烯键式不饱和腈，催化剂组合物降解产物和提取剂; 和e）蒸馏提取相以获得包含萃取剂的第一流和包含催化剂组合物的第二料流。

    PREPARATION OF VERY HIGH MOLECULAR WEIGHT POLYAMIDE FILAMENTS
    169.
    发明申请
    PREPARATION OF VERY HIGH MOLECULAR WEIGHT POLYAMIDE FILAMENTS 审中-公开
    非常高分子量聚酰胺纤维的制备

    公开(公告)号：WO2009052049A1

    公开(公告)日：2009-04-23

    申请号：PCT/US2008/079716

    申请日：2008-10-13

    Applicant: INVISTA TECHNOLOGIES S.A.R.L. ,  SCHWINN, Glenn, Alan ,  WEST, Gary, Raymond

    Inventor： SCHWINN, Glenn, Alan ,  WEST, Gary, Raymond

    IPC: D01F6/60 ,  D01F6/80 ,  D01F6/90 ,  D01D5/38

    CPC classification number: D01F6/60 ,  D01D5/38 ,  Y10T428/2904

    Abstract: Disclosed is the preparation of very high molecular weight polyamide, e.g., nylon, filaments., as indicated by such filaments exhibiting a very high Relative Viscosity (RV) value. Such filaments can be used to prepare polyamide staple fibers which are especially useful for industrial applications such as in papermachine felts. The filament preparation process involves a melt phase polymerization (MPP) procedure, optionally carried out in combination with a solid phase polymerization (SPP) procedure. Both of these procedures serve to increase the molecular weight and hence the RV of the polyamide filaments produced. These procedures are conducted under selected controlled conditions which permit realization of polyamide filaments of about 2 to 100 denier and which have RV values of greater than about 190. Such filaments also exhibit excellent tenacity and tenacity resistance properties.

    Abstract translation: 公开了非常高分子量的聚酰胺（例如尼龙，长丝）的制备，如由显示非常高的相对粘度（RV）值的长丝所示。 这种长丝可用于制备聚酰胺短纤维，其特别适用于诸如造纸机毛毡的工业应用。 细丝制备方法涉及熔融相聚合（MPP）方法，任选地与固相聚合（SPP）方法组合进行。 这两个方法都用于提高所生产的聚酰胺长丝的分子量，因此增加RV。 这些方法在选择的控制条件下进行，其允许实现约2至100旦尼尔的聚酰胺长丝，并且RV值大于约190.这种长丝还表现出优异的韧性和耐韧性。

    VARIABLE STRETCH NONWOVEN FABRIC COMPOSITES
    170.
    发明申请
    VARIABLE STRETCH NONWOVEN FABRIC COMPOSITES 审中-公开
    可变拉伸非织造布复合材料

    公开(公告)号：WO2009032867A1

    公开(公告)日：2009-03-12

    申请号：PCT/US2008/075167

    申请日：2008-09-04

    Applicant: INVISTA TECHNOLOGIES S.A.R.L. ,  PASCAVAGE, Peter, W.

    Inventor： PASCAVAGE, Peter, W.

    IPC: B32B5/04 ,  B32B5/08 ,  B32B5/26 ,  B32B5/10 ,  D04H3/04 ,  D04H13/00

    CPC classification number: B32B5/08 ,  B32B5/12 ,  B32B5/26 ,  B32B2262/0261 ,  B32B2262/0276 ,  B32B2262/0292 ,  Y10T428/2481 ,  Y10T428/24942 ,  Y10T442/637 ,  Y10T442/641 ,  Y10T442/66

    Abstract: Disclosed herein are nonwoven fabric composites comprising layers of spunbond and meltblown nonwoven webs. Such composites are prepared by forming or assembling the layers of the composite such that there are two outer layers of spunbond fibers disposed on opposite sides of eh at least one inner meltblown layer. At least one of the outer layers comprises substantially parallel lanes of spunbond, continuous filament fibers with at least two different lanes having a higher and a lower basis weight. The higher and lower basis weight lanes of fibers within the spunbond layer(s) are also predominately oriented in the machine direction of the nonwoven fabric composite. All layers of the fabric composites herein are bonded together via thermal, adhesive, ultra-sonic or mechanical bonding means. Such composites can be fashioned to vary the ratio of cross direction stretch to machine direction stretch.

    Abstract translation: 本文公开了包括纺粘和熔喷非织造纤维网层的非织造织物复合材料。 通过形成或组装复合材料层来制备这种复合材料，使得在eh至少一个内部熔喷层的相对侧上有两层纺粘纤维外层。 外层中的至少一个包括具有至少两个具有较高和较低基重的不同通道的基本平行的纺粘连续长丝纤维。 纺粘层中的纤维的较高和较低的基重通道也主要在无纺织物复合材料的纵向取向。 这里的织物复合材料的所有层通过热粘合剂，超声波或机械粘合手段粘合在一起。 这种复合材料可以被形成以改变横向拉伸与机器方向拉伸的比例。

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