Invention Patent
- Patent Title: PRODUCTION OF QUINACRIDONE PIGMENT
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Application No.: JP8286297Application Date: 1997-04-01
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Publication No.: JPH1036699APublication Date: 1998-02-10
- Inventor: URBAN MANFRED , SCHNAITMANN DIETER DR , BOEHMER MARTIN
- Applicant: HOECHST AG
- Assignee: HOECHST AG
- Current Assignee: HOECHST AG
- Priority: DE19613186 1996-04-02
- Main IPC: C09B67/20
- IPC: C09B67/20 ; C09B48/00 ; C09B67/10 ; C09B67/22 ; C09B67/52
Abstract:
PROBLEM TO BE SOLVED: To obtain a quinacridone pigment economically profitably without causing environmental disruption by hydrolyzing a reaction mixture obtained by cyclizing a specified dianilinoterephthalic acid with a polyphosphoric acid or a polyphosphate. SOLUTION: A dianilinoterephthalic acid represented by formula I (R to R are each H, Cl, Br, F, a 1-4C alkyl, a 1-4C alkoxyl, a carboxamido, or a phenoxy or 6-18C aryl ring which may be fused with an aromatic, aliphatic or heterocyclic ring) is cyclized with 3-10 pts.wt., per pt.wt. the above terephathlic acid, polyphosphoric acid or polyphosphate at 80-150 deg.C for 0.5-24hr to obtain a reaction mixture. A pre-pigment obtained by hydrolyzing this mixture with water or an aqueous mineral acid solution at 110 deg.C or above under elevated pressure is heat-treated at 50-200 deg.C for 1-24hr to obtain a coarse crystalline crude pigment. The crude pigment is ground in an aqueous medium, an aqueous/organic medium or an organic solvent to obtain a quinacridone pigment represented by formula II.
Public/Granted literature
- JP3923132B2 Method of manufacturing a quinacridone pigment Public/Granted day:2007-05-30
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