Invention Grant
- Patent Title: Method of synthesis of CMK-3-type carbon replica
- Patent Title (中): CMK-3型碳复制品的合成方法
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Application No.: US14374566Application Date: 2013-02-08
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Publication No.: US09302252B2Publication Date: 2016-04-05
- Inventor: Piotr Kustrowski , Rafal Janus , Paula Niebrzydowska
- Applicant: UNIWERSYTET JAGIELLONSKI
- Applicant Address: PL Cracow
- Assignee: UNIWERSYTET JAGIELLONSKI
- Current Assignee: UNIWERSYTET JAGIELLONSKI
- Current Assignee Address: PL Cracow
- Agency: Walker & Jocke
- Priority: PL398111 20120214
- International Application: PCT/PL2013/000015 WO 20130208
- International Announcement: WO2013/122488 WO 20130822
- Main IPC: C01B31/02
- IPC: C01B31/02 ; B01J29/03 ; C01B31/00 ; B01J37/03 ; B01J37/06 ; B01J37/08 ; B01J21/18 ; B01J35/00 ; B01J35/10 ; B01J37/00 ; C01B37/00 ; B01J20/20 ; B01J20/30 ; B01J20/28

Abstract:
The method of obtaining the CMK-3-type carbon replica, consisting of the introduction of SBA-15-type molecular sieve to a mixture of furfuryl alcohol and a solvent, the subsequent polycondensation of furfuryl alcohol, carbonization of the prepared, composite and removal of the hard template, according to the invention, is characterized in that the reaction of furfuryl alcohol polycondensation is carried out by the precipitation method in a slurry containing SBA-15 silica sieve, water, furfuryl alcohol and concentrated solution of hydrochloric acid in mass ratios, respectively, in the range from 1.00:32.33:1.00:6.65 to 1.00:30.83:2.50:16.64, whereas the ratio of the total mass of furfuryl alcohol and water to the mass of SBA-15 as well as the mass ratio of the concentrated HCl solution to the mass of furfuryl alcohol are kept at the constant value every time.
Public/Granted literature
- US20150010459A1 METHOD OF SYNTHESIS OF CMK-3-TYPE CARBON REPLICA Public/Granted day:2015-01-08
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