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    생체 시료 내 페놀 화합물 동시 분석 방법
    4.
    发明公开
    생체 시료 내 페놀 화합물 동시 분석 방법 有权
    方法同时测定生物材料中酚醛化合物

    公开(公告)号：KR1020140027735A

    公开(公告)日：2014-03-07

    申请号：KR1020120093684

    申请日：2012-08-27

    Applicant: 한국과학기술연구원

    Inventor： 이정애 ,  이수현 ,  정봉철 ,  표희수

    IPC: G01N33/493 ,  G01N30/72 ,  C12Q1/34

    Abstract: The present invention relates to a method for the simultaneous analysis of a phenol compound in a biological material, and more specifically, to a method for the simultaneous analysis of a phenol compound in a biological material, wherein the method includes a step of adjusting the pH of a living body sample and a step of extracting a phenolic compound from the living body sample in a liquid phase. According to one embodiment of the present invention, the pH of the living body sample is adjusted using potassium carbonate (K2CO3).

    Abstract translation: 本发明涉及生物材料中酚类化合物的同时分析方法，更具体地说，涉及生物材料中酚化合物的同时分析方法，其中该方法包括调节pH 的活体样品和从活体样品中以液相萃取酚类化合物的步骤。 根据本发明的一个实施方案，使用碳酸钾（K 2 CO 3）来调节活体样品的pH。

    생체 뇨 시료 내 휘발성 유기 화합물(ＶＯＣ) 대사체 분석 방법
    5.
    发明公开
    생체 뇨 시료 내 휘발성 유기 화합물(ＶＯＣ) 대사체 분석 방법 失效
    用于确定挥发性有机化合物代谢物在尿液中的方法

    公开(公告)号：KR1020100124910A

    公开(公告)日：2010-11-30

    申请号：KR1020090043849

    申请日：2009-05-20

    Applicant: 한국과학기술연구원

    Inventor： 이정애 ,  정봉철 ,  표희수 ,  김민화

    IPC: G01N33/493 ,  G01N30/12 ,  G01N30/72

    Abstract: PURPOSE: A method for analyzing volatile organic compound(VOC) metabolite concentrate in urine sample is provided to accurately analyze VOC metabolites. CONSTITUTION: A method for analyzing VOC metabolite in urine sample comprises: a extracting VOC metabolite from the urine sample; and a step of performing quantitation by gas chromatography-mass spectrometry(GC-MS) of VOC metabolite. The volume of the urine sample is 0.1-1 mL.

    Abstract translation: 目的：提供尿样中挥发性有机化合物（VOC）代谢物浓缩物的分析方法，准确分析VOC代谢产物。 构成：用于分析尿样中VOC代谢物的方法包括：从尿样中提取VOC代谢物; 以及通过VOC代谢物的气相色谱 - 质谱（GC-MS）进行定量的步骤。 尿液体积为0.1-1 mL。

    양이온성 4가 암모늄화합물의 정량분석 방법
    7.
    发明公开
    양이온성 4가 암모늄화합물의 정량분석 방법 有权
    阳离子四价铵化合物的定量分析方法

    公开(公告)号：KR1020180005074A

    公开(公告)日：2018-01-15

    申请号：KR1020160085036

    申请日：2016-07-05

    Applicant: 한국과학기술연구원

    Inventor： 이정애 ,  오지선 ,  표희수 ,  정봉철

    IPC: G01N30/88 ,  G01N30/72

    CPC classification number: G01N30/88 ,  G01N30/7233 ,  G01N2030/884

    Abstract: 본명세서에는피검사체에서양이온성 4가암모늄화합물을정량분석및 검출하는방법이개시된다. 상기방법에따르면피검사체로부터다양한양이온성 4가암모늄화합물을분석할수 있고, 매트릭스영향을줄여검출감도를향상시켜양이온성 4가암모늄화합물을우수한정밀도및 정확도로정량분석할수 있다.

    Abstract translation: 本文是用于定量分析阳离子4和检测在所述测试受试者的铵化合物公开了一种方法。 根据上述方法，并且可以分析来自测试受试者的各种阳离子的四价铵化合物，由通过改进检测灵敏度可以以高的精度和准确度阳离子季铵化合物的进行定量分析降低基体的效果。

    미량 산성농약의 동시 검출법
    10.
    发明公开
    미량 산성농약의 동시 검출법 失效
    共同检测微酸性农药的方法

    公开(公告)号：KR1020030044662A

    公开(公告)日：2003-06-09

    申请号：KR1020010075500

    申请日：2001-11-30

    Applicant: 한국과학기술연구원

    Inventor： 박송자 ,  표희수 ,  신혜승

    IPC: G01N33/00

    Abstract: PURPOSE: A method of concurrent-detecting micro acid pesticides is provided to concurrently extract and detect ten kinds of pesticides from the samples of water or soil in an effective manner. CONSTITUTION: In a method of co-detecting micro acid pesticides, samples are taken from the water or soil, and a strong-base material is added to the samples to make a mixture. The mixture is bathed, and hydrolyzed. The mixture is acidified by a strong acid solution, and the target is extracted from the acidified mixture by using an organic solvent. The extract is derivatized in reaction with trifluoro acetic acid anhydride and trifluoro ethanol. The derivatized extract is directly put in a gas chromatograph, or a gas chromatograph/a mass spectrograph to concurrently detect the micro acid pesticides.

    Abstract translation: 目的：提供同时检测微酸性农药的方法，以有效的方式从水或土壤样品中同时提取和检测十种农药。 构成：在一种共同检测微酸性农药的方法中，将样品从水或土壤中取出，并将强碱材料加入到样品中以形成混合物。 混合物沐浴并水解。 将混合物用强酸溶液酸化，用有机溶剂从酸化混合物中萃取。 提取物与三氟乙酸酐和三氟乙醇反应衍生化。 将衍生的提取物直接放入气相色谱仪或气相色谱仪/质谱仪中，同时检测微酸杀虫剂。

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