公开(公告)号：DE1149338B

公开(公告)日：1963-05-30

申请号：DEB0063544

申请日：1961-08-05

Applicant: BASF AG

Inventor： HAAS DR HANS ,  SCHMIDT DIPL-ING HANS ,  GROSSE DIPL-ING HANS-JOACHIM

IPC: C01C3/10

公开(公告)号：DE1168884B

公开(公告)日：1964-04-30

申请号：DEB0055450

申请日：1959-11-07

Applicant: BASF AG

Inventor： ADAM DR KARL ,  AREND DR WOLFGANG ,  FRICK DR REINHOLD ,  HAAS DR HANS

IPC: C07C253/34 ,  C07C255/45

Abstract: Aliphatic dinitriles containing 4-22 carbon atoms, having at least 2 carbon atoms between the nitrile groups, and having, apart from the nitrile groups, a hydrocarbon structure, are purified by bringing them in the presence of water into contact with an alkali metal bisulphate, ammonium bisulphate, an ammonium bisulphate N-substituted by 1-3 alkyl groups having 1-4 carbon atoms, or a bisulphate of a divalent metal which does not form a sulphate which is difficulty soluble in water, e.g. iron, manganese, zinc, cobalt and nickel. The amount of water is preferably 3-8% by weight of dinitrile, and the amount of bisulphate preferably 0.01-10% by weight of dinitrile. Specified dinitriles are adipodinitrile, suberodinitrile, sebacodinitrile and the mixture of 1.9- and 1,10-dicyanoheptadecane known as heptadecane dicarboxylic acid dinitrile. The temperature may be from the solidification point of the dinitrile to 200 DEG C. or more. The purified dinitriles may be reduced to the corresponding diamines.

公开(公告)号：DE1275046B

公开(公告)日：1968-08-14

申请号：DEB0086110

申请日：1966-03-09

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  HAAS DR HANS ,  HIMMELHAN DIPL-ING EMIL

IPC: C07C51/08

公开(公告)号：DE911263C

公开(公告)日：1954-05-13

申请号：DEB0019530

申请日：1952-03-16

Applicant: BASF AG

Inventor： REPPE DR WALTER ,  FRIEDRICH DR HERBERT ,  HAAS DR HANS

IPC: C07D471/22

公开(公告)号：DE1269348B

公开(公告)日：1968-05-30

申请号：DE1269348

申请日：1964-10-16

Applicant: BASF AG

Inventor： VOLLMERT DR BRUNO ,  HAAS DR HANS

IPC: C08F20/34 ,  C08F22/22

公开(公告)号：DE1156777B

公开(公告)日：1963-11-07

申请号：DEB0063688

申请日：1961-08-17

Applicant: BASF AG

Inventor： HAAS DR HANS ,  OSTERMAYER DR HANS ,  ZINKE-ALLMANG DR HELMUT

公开(公告)号：DE1116646B

公开(公告)日：1961-11-09

申请号：DEB0055919

申请日：1959-12-15

Applicant: BASF AG

Inventor： ADAM DR KARL ,  AREND DR WOLFGANG ,  FRICK DR REINHOLD ,  HAAS DR HANS

公开(公告)号：DE1105159B

公开(公告)日：1961-04-20

申请号：DEB0040552

申请日：1956-06-07

Applicant: BASF AG

Inventor： HANUSCH DR FRITZ ,  HAAS DR HANS ,  RETTIG AUGUST

IPC: C08J3/22 ,  C08L21/00 ,  C08L25/06