公开(公告)号：DE1568180A1

公开(公告)日：1970-07-23

申请号：DE1568180

申请日：1966-09-17

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  SCHULZ DR ALFRED

IPC: C07C5/11

公开(公告)号：DE1570314A1

公开(公告)日：1970-03-05

申请号：DE1570314

申请日：1965-11-04

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  FUERST DR ERNST ,  NOTTES DR-ING GUENTHER

IPC: C07G99/00 ,  C08G14/04 ,  C08G14/12

公开(公告)号：DE1568079A1

公开(公告)日：1970-01-02

申请号：DE1568079

申请日：1966-02-17

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  FUERST DR ERNST ,  WEITZ DR HANS-MARTIN

IPC: C10G21/20

公开(公告)号：DE1259846B

公开(公告)日：1968-02-01

申请号：DEB0081008

申请日：1965-03-17

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  FUERST DR ERNST ,  BUDDENBERG DR OTTO ,  SCHMID DR DIETER

IPC: B01D53/52 ,  C01B32/50 ,  C10K1/16

公开(公告)号：DE1244150B

公开(公告)日：1967-07-13

申请号：DEB0073041

申请日：1963-08-08

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  MERKEL DR KARL

IPC: C08K5/315

公开(公告)号：DE1239467B

公开(公告)日：1967-04-27

申请号：DEB0083787

申请日：1965-09-18

Applicant: BASF AG

Inventor： MERKEL DR KARL ,  HAARER DR ERICH

IPC: C08G18/22 ,  C08G18/76

公开(公告)号：DE1229064B

公开(公告)日：1966-11-24

申请号：DEB0069478

申请日：1962-11-03

Applicant: BASF AG

Inventor： SCHOLZ DR HEINRICH ,  STROHMEYER DR MAX ,  HAARER DR ERICH

IPC: C07C231/02 ,  C07C233/02 ,  C07D213/72

Abstract: In a continuous process for preparing amides by reaction of esters with primary or secondary amines, the reactants are introduced into a column in which there is, both above and below the point of introduction, a countercurrent flow of ascending vaporous products and descending liquid products (the amide being withdrawn from a point below the supply point), and a temperature gradient increasing from top to bottom. The esters are derived from C1- 4 acids and C1- 4 alcohols and the amines have 1-12 C atoms and may contain 1 or 2 OH groups or ether bridges; the column temperatures are not more than 260 DEG C. at the bottom and at least 20 DEG C. at the top. A part only of the top product is removed at a minimum reflux ratio of 2: 1. Exemplified products are HCONMe2, HCONHEt, HCONEt2, HCONBu2, HCONH (cyclohexyl) and AcNHEt.

公开(公告)号：DE1159423B

公开(公告)日：1963-12-19

申请号：DEB0065383

申请日：1961-12-30

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  PLASS DR REINHOLD ,  HORNBERGER DR PAUL

IPC: C07C51/31

公开(公告)号：DE1108508B

公开(公告)日：1961-06-08

申请号：DEB0054075

申请日：1959-07-18

Applicant: BASF AG

Inventor： HAARER DR ERICH ,  NOTTES DR GUENTHER ,  WOLF DR-ING WILLY

IPC: C10L1/14 ,  C10L1/18 ,  C10L1/22

公开(公告)号：DE1568087A1

公开(公告)日：1970-02-05

申请号：DE1568087

申请日：1966-03-09

Applicant: BASF AG

Inventor： ADAM DR KARL ,  HAARER DR ERICH ,  MERKEL DR KARL ,  PILCH DR KURT