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    VERFAHREN ZUR AUFARBEITUNG EINES BUTEN- UND/ODER BUTADIEN ENTHALTENDEN STOFFSTROMS
    96.
    发明公开
    VERFAHREN ZUR AUFARBEITUNG EINES BUTEN- UND/ODER BUTADIEN ENTHALTENDEN STOFFSTROMS 有权
    VERFAHREN ZUR AUFARBEITUNG EINES BUTEN - UND / ODER BUTADIEN ENTHALTENDEN STOFFSTROMS

    公开(公告)号：EP2681178A1

    公开(公告)日：2014-01-08

    申请号：EP12706605.8

    申请日：2012-03-02

    Applicant: BASF SE

    Inventor： KOSTOVA, Albena ,  BENFER, Regina ,  GÖTZ, Jochen ,  REZAI, Alireza ,  MORILLO, Aristides ,  OLBERT, Gerhard ,  PFAB, Peter ,  KOLIOS, Grigorios ,  WEBER, Markus ,  WECK, Alexander

    IPC: C07C7/04 ,  C07C7/08 ,  C07C7/11 ,  C07C11/08 ,  C07C11/167 ,  C07C9/10

    CPC classification number: B01D3/40 ,  C07C7/04 ,  C07C7/08 ,  C07C7/11 ,  C07C11/16 ,  C07C11/167

    Abstract: The invention relates to a process for workup of a stream (1) comprising butene and/or butadiene, butane, hydrogen and/or nitrogen and carbon dioxide, comprising the following steps: (a) absorption of the stream (1) comprising butene and/or butadiene, butane, hydrogen and/or nitrogen, with or without carbon dioxide, with a mixture (5) comprising 80 to 97% by weight of N-methylpyrrolidone and 3 to 20% by weight of water to obtain a stream (9) comprising N-methylpyrrolidone, water, butene and/or butadiene, and butane, with or without carbon dioxide, and a stream (7) comprising hydrogen and/or nitrogen and butane, (b) extractive distillation of the stream (9) comprising N-methylpyrrolidone, water, butene and/or butadiene, and butane, with or without carbon dioxide, with a stream (13) comprising 80 to 97% by weight of N-methylpyrrolidone and 3 to 20% by weight of water to separate the stream (9) comprising N-methylpyrrolidone, water, butene and/or butadiene, and butane, with or without carbon dioxide, into a stream (17) comprising N-methylpyrrolidone, water, butene and/or butadiene, and a stream (15) comprising essentially butane, with or without carbon dioxide, (c) distillation of the stream (17) comprising N-methylpyrrolidone, water, butene and/or butadiene into a stream (23) comprising essentially N-methylpyrrolidone and water, and a stream (21) comprising butene and/or butadiene.

    Abstract translation: 本发明涉及包含丁烯和/或丁二烯，丁烷，氢气和/或氮气和二氧化碳的物流（1）的处理方法，其包括以下步骤：（a）将包含丁烯和 （5）包含80-97重量％的N-甲基吡咯烷酮和3-20重量％的水以获得流（9），所述混合物（5）包含具有或不具有二氧化碳的丁二烯，丁烷，氢和/ ）包含N-甲基吡咯烷酮，水，丁烯和/或丁二烯和丁烷（含有或不含二氧化碳）以及包含氢和/或氮和丁烷的物流（7），（b）物流（9）的萃取蒸馏包含 （13）包含80-97重量％的N-甲基吡咯烷酮和3-20重量％的水以分离含有或不含二氧化碳的N-甲基吡咯烷酮，水，丁烯和/或丁二烯和丁烷， 包含N-甲基吡咯烷酮，水，丁烯和/或丁二烯和丁烷的物流（9），有或没有汽车 （17），包含N-甲基吡咯烷酮，水，丁烯和/或丁二烯，以及基本上包含丁烷的物流（15），其中含有或不含有二氧化碳，（c）蒸馏包含N （23）和包含丁烯和/或丁二烯的物流（21），所述物流（23）基本上包含N-甲基吡咯烷酮和水。

    VERFAHREN ZUR HERSTELLUNG VON ISOCYANATEN
    97.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON ISOCYANATEN 审中-公开

    公开(公告)号：EP2627629A1

    公开(公告)日：2013-08-21

    申请号：EP11767258.4

    申请日：2011-10-11

    Applicant: BASF SE

    Inventor： MATTKE, Torsten ,  OLBERT, Gerhard

    IPC: C07C263/10

    CPC classification number: B01J19/1856 ,  B01J19/1862 ,  B01J2219/00162 ,  C07C263/10 ,  C07C265/14

    Abstract: The invention relates to a method for producing isocyanates by reacting the corresponding amines with phosgene, comprising the following steps: (a) providing at least one amine-containing reactant flow and at least one phosgene-containing reactant flow, (b) mixing the reactant flows to form at least one reaction mixture in a mixing zone, (c) reacting the at least one reaction mixture in a reaction zone, and (d) processing the at least one product mixture obtained from (c), wherein (i) the mixing zone is composed of at least two strands which are connected in parallel and can be controlled separately from each other and which each comprise at least one mixing unit, or (ii) the reaction zone is composed of at least two strands which are connected in parallel and can be controlled separately from each other and which each comprise at least one reaction unit, or (iii) the mixing zone and the reaction zone are composed of at least two strands which are connected in parallel and can be controlled separately from each other and each comprise at least one mixing unit and at least one reaction unit.

    Abstract translation: 该方法包括以下步骤：（a）提供至少一种含胺反应物流和至少一种含光气反应物流，（b）将反应物 （c）使所述至少一种反应混合物在反应区中反应，和（d）处理由（c）获得的所述至少一种产物混合物，其中（i）所述至少一种反应混合物在所述混合区中流动以形成至少一种反应混合物， 混合区由至少两条并列连接并且可以彼此分开控制并且每个都包含至少一个混合单元的链组成，或者（ii）反应区由至少两条链 平行并且可以彼此分开地控制并且每个都包括至少一个反应单元，或者（iii）混合区域和反应区域由至少两个并联连接并且可以控制 它们彼此分开并且各自包含至少一个混合单元和至少一个反应单元。

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