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公开(公告)号:DE502005010287D1
公开(公告)日:2010-11-04
申请号:DE502005010287
申请日:2005-01-26
Applicant: BASF SE
Inventor: JUNGKAMP TIM , POLKA HANS-MARTIN , BAUMANN ROBERT , BARTSCH MICHAEL , HADERLEIN GERD , LUYKEN HERMANN , SCHEIDEL JENS
IPC: C07C253/34 , C07C255/04 , C07C255/07
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公开(公告)号:PL1713760T3
公开(公告)日:2008-12-31
申请号:PL05701204
申请日:2005-01-27
Applicant: BASF SE
Inventor: JUNGKAMP TIM , BAUMANN ROBERT , BARTSCH MICHAEL , HADERLEIN GERD , LUYKEN HERMANN , SCHEIDEL JENS
IPC: C07C253/10 , C07C255/04
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公开(公告)号:AT399761T
公开(公告)日:2008-07-15
申请号:AT05701204
申请日:2005-01-27
Applicant: BASF SE
Inventor: JUNGKAMP TIM , BAUMANN ROBERT , BARTSCH MICHAEL , HADERLEIN GERD , LUYKEN HERMANN , SCHEIDEL JENS
IPC: C07C253/10 , C07C255/04
Abstract: An adiponitrile/methylglutaronitrile preparation process includes distilling a reaction stream to obtain stream 3 depleted in pentenenitriles (bottom product) and stream 4 enriched in pentenenitriles (top product); extracting stream 3 obtaining stream 6 enriched with extractant (top product) and stream 7 depleted in extractant (bottom product); distilling stream 6 obtaining stream 8 comprising the catalyst (bottom product) and stream 9 comprising the extractant (top product); distilling stream 7 obtaining stream 10 (bottom product) and stream 11 comprising the extractant (top product); distilling stream 10 obtaining stream 12 comprising catalyst degradation products, at least one promotor, adiponitrile and methylglutaronitrile (bottom product) and stream 13 comprising pentenenitriles (top product); distilling stream 12 obtaining stream 14 comprising catalyst degradation products and the promotor(s) (bottom product) and stream 15 comprising adiponitrile and methylglutaronitrile (top product); distilling stream 15 obtaining stream 16 comprising adiponitrile (bottom product) and stream 17 comprising methylglutaronitrile (top product).
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