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公开(公告)号:AT524435T
公开(公告)日:2011-09-15
申请号:AT05701206
申请日:2005-01-27
Applicant: BASF SE
Inventor: SCHEIDEL JENS , JUNGKAMP TIM , BARTSCH MICHAEL , HADERLEIN GERD , BAUMANN ROBERT , LUYKEN HERMANN
IPC: C07C253/30 , C07C255/07
Abstract: A process is described for isomerizing pentenenitrile in a reactant stream, wherein the isomerization is effected over a heterogeneous catalyst in a distillation column in such a way that, during the isomerization of the isomerization reactant, it is distillatively depleted in relation to the isomerization product in the reaction column of the distillation column.
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公开(公告)号:DE502005011240D1
公开(公告)日:2011-05-26
申请号:DE502005011240
申请日:2005-01-27
Applicant: BASF SE
Inventor: JUNGKAMP TIM , BAUMANN ROBERT , BARTSCH MICHAEL , HADERLEIN GERD , LUYKEN HERMANN , SCHEIDEL JENS
IPC: C07C253/10 , C07C255/07
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公开(公告)号:AT501114T
公开(公告)日:2011-03-15
申请号:AT05707030
申请日:2005-01-27
Applicant: BASF SE
Inventor: SCHEIDEL JENS , JUNGKAMP TIM , BARTSCH MICHAEL , HADERLEIN GERD , BAUMANN ROBERT , LUYKEN HERMANN
IPC: C07C253/10 , C07C255/07
Abstract: A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene, wherein 1,3-butadiene is reacted with hydrogen cyanide in the presence of at least one catalyst and the stream resulting therefrom is purified distillatively, the bottom temperature during the distillation not exceeding 140° C.
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公开(公告)号:DE502005010038D1
公开(公告)日:2010-09-16
申请号:DE502005010038
申请日:2005-01-27
Applicant: BASF SE
Inventor: SCHEIDEL JENS , JUNGKAMP TIM , BARTSCH MICHAEL , HADERLEIN GERD , BAUMANN ROBERT , LUYKEN HERMANN
IPC: C07C253/10 , C07C253/34 , C07C255/07
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公开(公告)号:DE502005004577D1
公开(公告)日:2008-08-14
申请号:DE502005004577
申请日:2005-01-27
Applicant: BASF SE
Inventor: JUNGKAMP TIM , BAUMANN ROBERT , BARTSCH MICHAEL , HADERLEIN GERD , LUYKEN HERMANN , SCHEIDEL JENS
IPC: C07C253/10 , C07C255/04
Abstract: An adiponitrile/methylglutaronitrile preparation process includes distilling a reaction stream to obtain stream 3 depleted in pentenenitriles (bottom product) and stream 4 enriched in pentenenitriles (top product); extracting stream 3 obtaining stream 6 enriched with extractant (top product) and stream 7 depleted in extractant (bottom product); distilling stream 6 obtaining stream 8 comprising the catalyst (bottom product) and stream 9 comprising the extractant (top product); distilling stream 7 obtaining stream 10 (bottom product) and stream 11 comprising the extractant (top product); distilling stream 10 obtaining stream 12 comprising catalyst degradation products, at least one promotor, adiponitrile and methylglutaronitrile (bottom product) and stream 13 comprising pentenenitriles (top product); distilling stream 12 obtaining stream 14 comprising catalyst degradation products and the promotor(s) (bottom product) and stream 15 comprising adiponitrile and methylglutaronitrile (top product); distilling stream 15 obtaining stream 16 comprising adiponitrile (bottom product) and stream 17 comprising methylglutaronitrile (top product).
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公开(公告)号:SI3102562T1
公开(公告)日:2018-05-31
申请号:SI201530208
申请日:2015-02-03
Applicant: BASF SE
Inventor: LUYKEN HERMANN , PFAB PETER , JUNGKAMP TIM
IPC: C07C253/00 , C07C209/00 , C07C211/00 , C07C255/00
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公开(公告)号:ES2667122T3
公开(公告)日:2018-05-09
申请号:ES15703554
申请日:2015-02-03
Applicant: BASF SE
Inventor: LUYKEN HERMANN , PFAB PETER , JUNGKAMP TIM
IPC: C07C253/34 , C07C209/48 , C07C211/12 , C07C253/10 , C07C255/04
Abstract: Procedimiento para la purificación de adipodinitrilo (ADN) que comprende las siguientes etapas a) a c) a) alimentación de una corriente (S1) que contiene adipodinitrilo crudo (ADN crudo) a un dispositivo (R1) de rectificación, b) separación de una corriente (S2) gaseosa mediante una primera salida lateral de (R1), en la que la primera salida lateral de (R1) se encuentra debajo de la posición de alimentación de la corriente (S1) hacia (R1) y en la que la corriente (S2) gaseosa contiene ADN, y c) alimentación de la corriente (S2) gaseosa a un segundo dispositivo (R2) de rectificación, en la que de (R2) en la cabeza se retira una corriente (S7) de ADN empobrecida en productos de alto punto de ebullición (HS) y en el fondo se retira una corriente (S6) líquida enriquecida en productos de alto punto de ebullición (HS).
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公开(公告)号:AT505453T
公开(公告)日:2011-04-15
申请号:AT05707028
申请日:2005-01-27
Applicant: BASF SE
Inventor: JUNGKAMP TIM , BAUMANN ROBERT , BARTSCH MICHAEL , HADERLEIN GERD , LUYKEN HERMANN , SCHEIDEL JENS
IPC: C07C253/10 , C07C255/07
Abstract: A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene in the presence of at least one catalyst, wherein the reaction is carried out in a loop reactor having external pumped circulation and jet nozzle for driving the internal circulation.
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公开(公告)号:AT476411T
公开(公告)日:2010-08-15
申请号:AT05701203
申请日:2005-01-27
Applicant: BASF SE
Inventor: SCHEIDEL JENS , JUNGKAMP TIM , BARTSCH MICHAEL , HADERLEIN GERD , BAUMANN ROBERT , LUYKEN HERMANN
IPC: C07C253/10 , C07C253/34 , C07C255/07
Abstract: A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) reacting 1,3-butadiene with hydrogen cyanide over at least one catalyst to obtain a stream 1 which comprises 3-pentenenitrile, 2-methyl-3-butenenitrile, the at least one catalyst and 1,3-butadiene, (b) distilling stream 1 in a column to obtain a high-1,3-butadiene stream 2 as the top product and a low-1,3-butadiene stream 3 as the bottom product which comprises 3-pentenenitrile, the at least one catalyst and 2-methyl-3-butenenitrile, (c) distilling stream 3 in a column to obtain a stream 4 as the top product which comprises 1,3-butadiene, a stream 5 which comprises 3-pentenenitrile and 2-methyl-3-butenenitrile at a side draw of the column, and a stream 6 as the bottom product which comprises the at least one catalyst, (d) distilling stream 5 to obtain a stream 7 as the top product which comprises 2-methyl-3-butenenitrile, and a stream 8 as the bottom product which comprises 3-pentenenitrile.
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公开(公告)号:AT453652T
公开(公告)日:2010-01-15
申请号:AT04790949
申请日:2004-10-28
Applicant: BASF SE
Inventor: BARTSCH MICHAEL , BAUMANN ROBERT , HADERLEIN GERD , FLORES MIGUEL ANGEL , JUNGKAMP TIM , LUYKEN HERMANN , SCHEIDEL JENS , SIEGEL WOLFGANG
IPC: C07F9/48 , B01J31/18 , B01J31/24 , C07C253/10 , C07C253/30 , C07C255/07 , C07C255/09 , C07F9/12 , C07F9/50 , C07F9/6574
Abstract: The invention relates to phosphinite phosphites I of formula 1, 2, 3, 4, 5 or 6 and mixtures thereof, wherein R1, R2, R4 independently represent an alkyl or alkylene group with 1 to 8 carbon atoms, provided that at least one of the groups R1, R2, R4 is different from H; R5 to R22 independently represent H, an alkyl or alkylene group with 1 to 8 carbon atoms; R3 is H, methyl or ethyl; X is F, Cl or CF3, if n=1 or 2 and X is H, if n=0.
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