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    OXIDE CATALYSTS AND PROCESS FOR PRODUCING epsilon -CAPROLACTAM BY USING THE SAME
    111.
    发明申请
    OXIDE CATALYSTS AND PROCESS FOR PRODUCING epsilon -CAPROLACTAM BY USING THE SAME 审中-公开
    氧化物催化剂及其制备方法

    公开(公告)号：WO00039084A1

    公开(公告)日：2000-07-06

    申请号：PCT/JP1999/007301

    申请日：1999-12-24

    IPC: B01J21/12 ,  B01J29/06 ,  B01J29/40 ,  C07D201/06 ,  C07D201/04

    CPC classification number: B01J29/04 ,  B01J21/12 ,  B01J29/06 ,  B01J29/40 ,  B01J29/405 ,  C07D201/06 ,  Y02P20/52

    Abstract: A method for producing epsilon -caprolactam by reacting cyclohexanone with a nitrogen source and oxygen wherein epsilon -caprolactam is produced from cyclohexanone in a single stage at a high selectivity by effecting the reaction in the presence of an oxide catalyst containing one or more metals M(s) selected from metals belonging to the groups 3 to 12 in the periodic table.

    Abstract translation: 一种通过使环己酮与氮源和氧气反应生成ε-己内酰胺的方法，其中ε-己内酰胺是通过在含有一种或多种金属M的氧化物催化剂的存在下在高选择性下由环己酮制备的， s）选自属于周期表中第3至12族的金属。

    ラクタム合成方法
    112.
    发明申请
    ラクタム合成方法 审中-公开
    LACTAM合成方法

    公开(公告)号：WO2003091208A1

    公开(公告)日：2003-11-06

    申请号：PCT/JP2002/004425

    申请日：2002-05-07

    Applicant: 独立行政法人産業技術総合研究所 ,  畑田 清隆 ,  佐藤 修 ,  生島 豊 ,  鳥居 一雄

    Inventor： 畑田 清隆 ,  佐藤 修 ,  生島 豊 ,  鳥居 一雄

    IPC: C07D201/06

    CPC classification number: C07D223/10

    Abstract: A method of continuously manufacturing lactam under high temperature and high pressure fluid, characterized by comprising the step of leading ketone and a hydroxylamine compound in a reaction field under high temperature and high pressure conditions of circulating fluid to efficiently synthesize lactam in a short time, whereby lactam can be rapidly synthesized continuously from ketone under the high temperature and high pressure fluid conditions of 175 C or higher in temperature range and 7 MPa or higher in pressure range.

    Abstract translation: 一种在高温高压液体下连续制造内酰胺的方法，其特征在于包括在高温和高压条件下在反应场中引导酮和羟胺化合物在循环流体中在短时间内有效合成内酰胺的步骤，由此 在温度范围为175℃或更高的高温高压流体条件下，丙酮可以从酮连续快速合成，压力范围为7MPa或更高。

    Method for producing laurolactam form cyclododecanone
    117.
    发明专利
    Method for producing laurolactam form cyclododecanone 有权

    公开(公告)号：JP2004099585A

    公开(公告)日：2004-04-02

    申请号：JP2003007027

    申请日：2003-01-15

    Applicant: Ube Ind Ltd ,  宇部興産株式会社

    Inventor： KURODA NOBUYUKI ,  KAWAI JOJI ,  SHIMOMURA HIDEO

    IPC: C07D225/02 ,  C07D201/04 ,  C07D201/06

    CPC classification number: C07D201/06 ,  C07D201/04

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing laurolactam in a high purity from cyclododecanone in a high efficiency.
    SOLUTION: This method for producing laurolactam by performing the reaction of starting cyclododecanone raw material with a mineral salt of hydroxylamine and converting the obtained cyclododecanone oxime by Beckmann rearrangement reaction is provided by controlling by ≤1,000 ppm each of the contents of oxygen atom-containing 12C hydrocarbon compounds, e.g. cyclododecenone or epoxycyclododecane and cycloaliphatic unsaturated 12C hydrocarbons contained in the cyclododecanone raw material as impurities.
    COPYRIGHT: (C)2004,JPO

    PRODUCTION OF EPSILON-CAPROLACTAM
    119.
    发明专利
    PRODUCTION OF EPSILON-CAPROLACTAM 失效

    公开(公告)号：JPH08198845A

    公开(公告)日：1996-08-06

    申请号：JP1252495

    申请日：1995-01-30

    Applicant: MITSUBISHI CHEM CORP

    Inventor： WATANABE KOJI ,  TEZUKA MAKOTO ,  YONEMORI TSUTOMU

    IPC: C07D201/04 ,  C07D201/06

    Abstract: PURPOSE: To obtain the subject high-purity compound without forming a by- product by making an isomerization inhibitor coexist in a catalytic hydration reaction system of cyclohexene, dehydrating a formed substance, then reacting it with hydroxylamine and further subjecting the reaction product to Beckmann rearrangement. CONSTITUTION: An isomerization inhibitor in an amount of preferably 240-390ppm such as a cyclic diene is made to coexist in a catalytic hydration reaction system of cyclohexene produced by partial hydrogenation of benzene to form cyclohexanol. Cyclohexanol is dehydrated into cyclohexanone, which is reacted with hydroxylamine to give cyclohexanone oxime. Cyclohexanone oxime is further subjected to Beckmann rearrangement to give the objective compound.

    PRODUCTION OF EPSILON-CAPROLACTAM
    120.
    发明专利
    PRODUCTION OF EPSILON-CAPROLACTAM 失效

    公开(公告)号：JPH08176102A

    公开(公告)日：1996-07-09

    申请号：JP31857594

    申请日：1994-12-21

    Applicant: MITSUBISHI CHEM CORP

    Inventor： TEZUKA MAKOTO ,  TOWATA MASATO ,  YONEMORI TSUTOMU

    IPC: C07D201/06 ,  C07C35/08

    Abstract: PURPOSE: To provide the method for producing the ε-caprolactam useful on industry, enabling to produce the ε-caprolactam not inferior to the conventional quality at a low cost. CONSTITUTION: The method for producing the ε-caprolactam by hydrating cyclohexene, subjecting the obtained cyclohexanol to a dehydrogenation reaction, reacting the obtained cyclohexanone with hydroxylamine and subsequently subjecting the obtained cyclohexanone oxime to a Beckmann rearrangement, is characterized by reducing indene compounds contained in the cyclohexanol fed to the dehydrogenation reaction to

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