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    MULTICHAIN TYPE AMINE DERIVATIVE AND ITS PRODUCTION
    131.
    发明专利
    MULTICHAIN TYPE AMINE DERIVATIVE AND ITS PRODUCTION 失效

    公开(公告)号：JPH08188560A

    公开(公告)日：1996-07-23

    申请号：JP58895

    申请日：1995-01-06

    Applicant: KAO CORP

    Inventor： MIYAJIMA TETSUYA ,  KITSUKI TOMOHITO ,  KITA KATSUMI

    IPC: A61K8/00 ,  A61K8/40 ,  A61Q5/00 ,  A61Q5/02 ,  A61Q5/12 ,  A61Q19/10 ,  C07C213/02 ,  C07C215/40 ,  C11D1/62 ,  A61K7/075 ,  A61K7/50

    Abstract: PURPOSE: To obtain the subject new compound, having low irritancy to the skin or hair, good in tough thereon, excellent in foaming power and emulsification stability and useful for various detergents, emulsifying agents, conditioning agents, etc. CONSTITUTION: A multichain type amine derivative of formula I [R is a (hydroxyl-substituted)straight-chain or branched chain 1-24C alkyl or alkenyl; R is a (hydroxyl-substituted)straight-chain or branched chain 1-4C alkyl or alkenyl; X is a halogen], e.g. tris(2-hydroxy-4,4-dimethyl-4-azoniadodecyl)amine chloride. The compound of formula I is obtained by reacting an amine derivative of formula II with one or two or more halogenated hydrocarbons having different R groups of the formula R -X. Furthermore, the reaction is preferably carried out by reacting the compound of formula II with the halogenated hydrocarbon in an equiv. amount of 2-10 times based on three amino groups in the compound of formula II in the presence of, e.g. an inert solvent at 20-150 deg.C, preferably 60-120 deg.C.

    PRODUCTION OF GLYCERYL-ETHERIFIED PENTAERYTHRITOL
    132.
    发明专利
    PRODUCTION OF GLYCERYL-ETHERIFIED PENTAERYTHRITOL 失效

    公开(公告)号：JPH08143496A

    公开(公告)日：1996-06-04

    申请号：JP28042394

    申请日：1994-11-15

    Applicant: KAO CORP

    Inventor： HASHIZUME NAOMICHI ,  KAMIYA HIROSHI ,  KITA KATSUMI

    IPC: C07C41/03 ,  C07C43/13

    Abstract: PURPOSE: To obtain a glyceryl-etherified pentaerythritol reduced in color and malodor and useful as a base material, an emulsifier, etc., for cosmetics, etc., in good productivity by reacting pentaerythritol with glycidyl ether in the absence of a solvent in a specific temperature range. CONSTITUTION: (A) Pentaerythritol is reacted with (B) a glycidyl ether of formula I (R is 1-36C alkyl, alkenyl) in the absence of a solvent at 200-400 deg.C, preferably 200-300 deg.C, to obtain a glyceryetherified pentaerythritol of formula: (Y)4 -S (S is the residue obtained by removing all hydroxyl groups from pentaerythritol; Y is a group selected from a group of formula II, a group of formula III and a hydroxyl group, wherein at least one of the Y groups comprises the group of formula II or the group of formula III). R is preferably a 3-36C branched alkyl of formula IV (q, r are integers of 0-33 wherein the sum of q and r is 0-33).

    CARBOXYETHYL ETHER DERIVATIVE AND DETERGENT COMPOSITION CONTAINING THE SAME
    133.
    发明专利
    CARBOXYETHYL ETHER DERIVATIVE AND DETERGENT COMPOSITION CONTAINING THE SAME 失效

    公开(公告)号：JPH0859545A

    公开(公告)日：1996-03-05

    申请号：JP19940294

    申请日：1994-08-24

    Applicant: KAO CORP

    Inventor： YANO SHINJI ,  FUKUDA REIKO ,  KITA KATSUMI

    IPC: C11D1/06 ,  C07C59/125

    Abstract: PURPOSE: To obtain a new carboxyethyl ether derivative useful for detergent composition, etc., excellent in cleansing property and foaming power. CONSTITUTION: A compound of formula I [R is a 1-20C alkyl; R is a 4-12C alkyl; M is H, an alkali metal, ammonium, an alkylamine or an alkanolamine; m is 0-10], e.g. 1,3-di-O-octylglyceryl-2-O-ethylcarboxylate. Furthermore, the compound of formula I is obtained by reacting a compound of formula II with acrylonitrile and hydrolyzing the resultant compound of formula III.

    ORGANO(POLY)SILOXANE MODIFIED WITH POLYVALENT METALLIC SALT OF PHOSPHORIC ESTER, PRODUCTION THEREOF AND GELLING AGENT CONTAINING THE SAME
    135.
    发明专利
    ORGANO(POLY)SILOXANE MODIFIED WITH POLYVALENT METALLIC SALT OF PHOSPHORIC ESTER, PRODUCTION THEREOF AND GELLING AGENT CONTAINING THE SAME 失效

    公开(公告)号：JPH07316169A

    公开(公告)日：1995-12-05

    申请号：JP11294594

    申请日：1994-05-26

    Applicant: KAO CORP

    Inventor： IHARA TAKESHI ,  YANO SHINJI ,  KITA KATSUMI

    IPC: C09K3/00 ,  C07F9/09 ,  C07F19/00 ,  C08G77/38 ,  C08G77/395 ,  C08L83/04 ,  C08L83/08

    Abstract: PURPOSE:To obtain the transparent organo(poly)siloxane, capable of providing thixotropic rheological characteristics to a silicone oil, having high safety and good in feeling of use by modifying Si atom with a specific polyvalent metallic salt group of a phosphoric ester. CONSTITUTION:This organo(poly)siloxane is obtained by modifying Si atom in an organo(poly)siloxane with a polyvalent metallic salt group of a phosphoric ester of formula I [R and R are each a 2-20C straight-chain or branched chain alkylene; R is a 1-20C straight-chain or branched chain alkyl; R is a 1-22C straight-chain or branched chain alkyl; M is an alkaline earth metal or a bi- or a polyvalent transition metal; (p) and (q) are each 0-200; (n) is the valence of M]. This method for producing the organo(poly)siloxane is to preferably react the organo(poly)siloxane of formula II (at least one of X' and (x) X Y' is H and the rest are each an alkyl, phenyl, etc.; Z' is H, an alkyl, etc.; R to R are each an alkyl, an alkoxy, etc.) with a polyvalent metallic salt of a phosphoric acid ester of formula III containing an unsaturated group in a solvent capable of dissolving both the raw materials such as toluene at 20-100 deg.C for 1-10hr.

    POLYSACCHARIDE DERIVATIVE, ITS PRODUCTION AND COSMETIC AND CLEANING AGENT COMPOSITION CONTAINING THE DERIVATIVE
    136.
    发明专利
    POLYSACCHARIDE DERIVATIVE, ITS PRODUCTION AND COSMETIC AND CLEANING AGENT COMPOSITION CONTAINING THE DERIVATIVE 失效

    公开(公告)号：JPH07304801A

    公开(公告)日：1995-11-21

    申请号：JP9734394

    申请日：1994-05-11

    Applicant: KAO CORP

    Inventor： KAMIYA HIROSHI ,  KITA KATSUMI

    IPC: A61K8/72 ,  A61K8/00 ,  A61K8/73 ,  A61Q5/00 ,  A61Q5/02 ,  A61Q19/00 ,  A61Q19/10 ,  C08B15/06 ,  C08B31/00 ,  C08B37/00 ,  C11D3/26 ,  A61K7/00 ,  A61K7/06 ,  A61K7/075 ,  A61K7/48 ,  A61K7/50

    Abstract: PURPOSE:To produce a polysaccharide derivative useful as a cosmetic and a cleaning agent having excellent water-retainability and feeling, keeping the effect over a long period, giving excellent feeling to the skin and resistant to sweat and water by introducing a carboxybetaine group to a polysaccharide. CONSTITUTION:This polysaccharide derivative is expressed by the formula (Z is a polysaccharide residue obtained by removing n-OH groups from a polysaccharide molecule; R and R each is a 1-3C straight or branched chain alkyl which may have hydroxyl group; A is a 1-3C straight or branched chain alkylene; (n) is a number not larger than the total number of hydroxyl groups in the polysaccharide molecule). The polysaccharide is selected from beta-1,4-glucan, alpha-1,4-glucan, alpha-1,6-glucan, pullulan, their hydroxyethyl derivatives, hydroxypropyl derivatives and 2,3-hydroxypropyl derivatives, for example cellulose or starch. The average degree substitution of the carboxybetaine group per one sugar residue in the polysaccharide molecule is 0.1-0.3. The derivative is produced by converting a polysaccharide of formula Z-(OH)n to a deoxyhalogenated polysaccharide, reacting with an amine and reacting the resultant aminopolysaccharide with a monohalogenated carboxylic acid salt.

    AMIDE-POLYCARBOXYLIC ACID OR ITS SALT AND PRODUCTION THEREOF
    137.
    发明专利
    AMIDE-POLYCARBOXYLIC ACID OR ITS SALT AND PRODUCTION THEREOF 失效

    公开(公告)号：JPH0797359A

    公开(公告)日：1995-04-11

    申请号：JP33579193

    申请日：1993-12-28

    Applicant: KAO CORP

    Inventor： KITSUKI TOMOHITO ,  NAKANO AKIKO ,  KITA KATSUMI ,  FUJIKURA YOSHIAKI

    IPC: C07C231/02 ,  C07C231/12 ,  C07C231/14 ,  C07C233/18 ,  C07C233/20 ,  C07C233/36 ,  C07C233/38 ,  C07C235/08 ,  C07C235/10 ,  C07C235/28

    Abstract: PURPOSE:To obtain the subject novel compound which is useful as a base material for cosmetics, detergent or emulsifier, because it has excellent foaming properties with reduced skin irritation to give comfortable feelings to skin and hair. CONSTITUTION:A compound of formula I (R , R are a 1 to 36C alkyl, a 1 to 36C alkenyl; X is a 2 to 4C alkylene or alkenylene which may be substituted with OH or COOH; Y is H, cation) or its salt, for example, 4-8-didecyl-3,9- dioxo-6-hydroxy-4,8-diaza-1,11-undecanedicarboxylic acid. The compound of formula I is obtained by reaction between a compound of formula II and a compound of formula III or by reaction of the compound of formula II with a compound of formula IV (R , R are H, a 1 to 5C alkyl, a 1 to 5C alkenyl) followed by hydrolysis of the product when R and R each is an alkyl or an alkenyl.

    AMINE DERIVATIVE AND ITS PRODUCTION
    138.
    发明专利
    AMINE DERIVATIVE AND ITS PRODUCTION 失效

    公开(公告)号：JPH0725837A

    公开(公告)日：1995-01-27

    申请号：JP17315693

    申请日：1993-07-13

    Applicant: KAO CORP

    Inventor： KAMIYA HIROSHI ,  KITA KATSUMI ,  FUJIKURA YOSHIAKI

    IPC: C07C213/04 ,  C07C217/28

    Abstract: PURPOSE:To obtain a new amine derivative having low melting point and O/W type emulsion forming characteristics and simultaneously, excellent also in storage stability in forming emulsion and extremely useful as a base for cosmetic, toiletry component and a surfactant such as emulsifying agent. CONSTITUTION:A compound of formula I [R is H, CH3, CH2CH2OH, formula II or formula III (R is isostearyl which is isostearyl alcohol residue obtained by reducing isostearic acid obtained as a by-product of dimer acid); R is formula II or formula III; R is CH3CH2OH, C(CH2OH)3, CCH3(CH2OH)2], e.g. 1mol glycidyl isostearyl ether adduct of trimethylolaminomethane. The compound of formula I wherein R is H, formula II or formula III is obtained by reacting amines of formula IV with glycidyl isostearyl ether of formula V.

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