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    Process for production of fatty acids
    171.
    发明公开
    Process for production of fatty acids 失效
    生产脂肪酸的方法

    公开(公告)号：EP0249359A3

    公开(公告)日：1988-12-21

    申请号：EP87304671

    申请日：1987-05-27

    Applicant: STAUFFER CHEMICAL COMPANY

    Inventor： Mirviss, Stanley Burton

    IPC: C07C51/295

    CPC classification number: C07C51/295

    Abstract: Process for the production of fatty acids by oxidative dehydrogenation of straight or branch chain primary alcohols of from C-4 to C-30 chain lengths per molecule, or mixtures of branch and straight chains, which are selectively reacted with an anhydrous alkali metal hydroxide. In the reaction, the temperature of reaction is gradually increased to maintain the reaction medium in a liquid non-viscous state. The reaction temperature is, however, maintained at a sufficiently low temperature to minimize by-product formation. The process is conducted at temperatures of from about 175°C to about 400°C for sufficient time to form the sodium salt of the acid which is then converted to the acid utilizing a mineral acid.

    2-(2-substituted benzoyl)-4-(substituted)-1,3-cyclohexanediones, a process for their production and a herbicidal composition containing them
    175.
    发明公开
    2-(2-substituted benzoyl)-4-(substituted)-1,3-cyclohexanediones, a process for their production and a herbicidal composition containing them 失效
    2-（2-取代苯甲酰基）-4-（取代的）-1,3-环己二酸，其生产方法和含有它们的除草剂组合物

    公开(公告)号：EP0264859A3

    公开(公告)日：1988-07-06

    申请号：EP87115188

    申请日：1987-10-16

    Applicant: STAUFFER CHEMICAL COMPANY

    Inventor： Chin, Hsiao-Ling Mao

    IPC: C07C49/813 ,  C07C49/84 ,  C07C79/36 ,  C07C49/792 ,  C07C45/54 ,  C07C147/06 ,  A01N35/06 ,  A01N41/10

    CPC classification number: C07C205/45 ,  A01N35/06 ,  A01N37/42 ,  A01N41/10 ,  C07C45/54 ,  C07C49/813 ,  C07C49/835 ,  C07C49/84 ,  C07C317/00

    Abstract: Compounds of the formula
    wherein
        R is halogen; C₁-C₂ alkyl; C₁-C₂ alkoxy; trifluoromethoxy; di­fluoromethoxy; nitro; cyano; C₁-C₂ haloalkyl; R a SO n - wherein n is 0 or 2 and R a is C₁-C₂ alkyl; trifluoromethyl or difluoromethyl;
        R¹ is hydrogen, C₁-C₄ alkyl, halogen, phenyl or substituted phenyl;
        R² is hydrogen or C₁-C₄ alkyl; or
        R¹ and R² together are C₂-C₅ alkylene;
        R³ is hydrogen, C₁-C₄ alkyl, phenyl or substituted phenyl, with the proviso that R¹ and R³ are not both phenyl or substituted phenyl;
        R⁴ is hydrogen or C₁-C₄ alkyl;
        R⁵ is hydrogen, halogen or C₁-C₄ alkyl;
        R⁶ is halogen, cyano, nitro, trifluoromethyl, -C(O)-OR f wherein R f is C₁-C₄ alkyl, or -C(O)NR₂ b wherein R b is hydrogen or C₁-C₂ alkyl;
        R⁷ and R⁸ independently are (1) hydrogen; (2) halogen; (3) C₁-C₄ alkyl; (4) C₁-C₄ alkoxy; (5) trifluoromethoxy; (6) cyano; (7) nitro; (8) C₁-C₄ haloalkyl; (9) R b SO n - wherein n is the integer 0, 1 or 2; and R b is (a) C₁-C₄ alkyl; (b) C₁-C₄ alkyl substituted with halogen or cyano; (c) phenyl; or (d) benzyl; (10) -NR c R d wherein R c and R d independently are hydrogen or C₁-C₄ alkyl; (11) R e C(O)- wherein R e is C₁-C₄ alkyl or C₁-C₄ alkoxy; or (12) -SO₂NR c R d wherein R c and R d are as defined; and (13) -N(R c )C(O)R d wherein R c and R d are as defined; and their salts.

    Process for production of isothiocyanates
    177.
    发明公开
    Process for production of isothiocyanates 失效
    Verfahren zur Herstellung von Isothiocyanaten。

    公开(公告)号：EP0266552A1

    公开(公告)日：1988-05-11

    申请号：EP87114223.8

    申请日：1987-09-29

    Applicant: STAUFFER CHEMICAL COMPANY

    Inventor： Telschow, Jeffrey Earl ,  Bright, Danielle Angrand

    IPC: C07C331/16

    CPC classification number: C07C331/16

    Abstract: Isothiocyanates are formed by oxidizing, with gaseous oxygen or air, in the presence of a metal oxidation catalyst a dithiocarbamate with appropriate control of the pH of the reaction medium to suppress the formation of by-products. Optionally a quaternary ammonium halide catalyst can be used to increase product yield.

    Abstract translation: 通过在适当控制反应介质的pH以抑制副产物的形成的情况下，在金属氧化催化剂二硫代氨基甲酸盐的存在下，用气态氧气或空气氧化异硫氰酸酯。 任选地，可使用季铵卤化物催化剂来提高产物产率。

    Improved process for conducting lipase enzyme hydrolysis
    178.
    发明公开
    Improved process for conducting lipase enzyme hydrolysis 失效
    Verfahren zurDurchführungvon enzymematischen Hydrolysen mit Lipasen。

    公开(公告)号：EP0257716A2

    公开(公告)日：1988-03-02

    申请号：EP87201590.4

    申请日：1987-08-21

    Applicant: STAUFFER CHEMICAL COMPANY

    Inventor： Dahod, Samun Kalim

    IPC: C12P1/00 ,  C12P7/40 ,  C12P41/00

    CPC classification number: C12P7/40 ,  C12P1/00 ,  C12P41/005

    Abstract: Lipase hydrolysis of an ester group of a substrate can be conducted in the absence of large quantities of water and excess enzyme without extensive inhibition of enzyme activity due to water-soluble product alcohol. A lipase reaction can be efficiently conducted by dispersing a water-­immiscible organic substrate phase in an aqueous phase, washing the reaction continuously while the reaction mixture is maintained in the dispersed state, and continuously removing an amount of aqueous phase substantially equivalent to the washing solution added. The washing solution can be an aqueous neutralizing solution. By this process, water-­soluble product alcohol can be removed from the reaction mixture without removal of substantial quantities of water-­soluble enzyme.

    Abstract translation: 在不存在大量水和过量酶的情况下，可以进行基质酯基的脂肪酶水解，而不会由于水溶性产物醇而对酶活性的广泛抑制。 通过将水不混溶的有机底物相分散在水相中，可以有效地进行脂肪酶反应，在反应混合物保持分散状态的同时连续洗涤反应，连续除去与洗涤液基本相当的水相量 添加。 洗涤溶液可以是水性中和溶液。 通过该方法，可以从反应混合物中除去水溶性产物醇，而不除去大量的水溶性酶。

    Certain 2-benzoyl-1,3,5-cyclohexanetriones
    180.
    发明公开
    Certain 2-benzoyl-1,3,5-cyclohexanetriones 失效
    某些2-苯甲酰基-1,3,5-环己烷三酮

    公开(公告)号：EP0252298A2

    公开(公告)日：1988-01-13

    申请号：EP87108083.4

    申请日：1987-06-04

    Applicant: STAUFFER CHEMICAL COMPANY

    Inventor： Carter, Charles Garvie

    IPC: C07C49/792 ,  C07C49/813 ,  C07C49/84 ,  C07C205/06 ,  C07C69/76 ,  C07C45/54 ,  C07C255/50 ,  C07C309/28 ,  C07C317/14 ,  C07C323/09 ,  A01N35/06

    CPC classification number: C07C205/45 ,  A01N35/06 ,  A01N37/38 ,  A01N41/06 ,  A01N41/10 ,  C07C45/54 ,  C07C49/792 ,  C07C49/813 ,  C07C49/835 ,  C07C49/84 ,  C07C255/00 ,  C07C317/00 ,  C07C323/00

    Abstract: Compounds of the formula
    wherein

    R is hydrogen; halogen; C 1 -C 2 alkyl; C 1 -C 2 alkoxy; nitro; cyano; C 1 -C 2 haloalkyl; or R a SO n -wherein n is 0 or 2 and Ra is C 1 -C 2 alkyl, trifluoromethyl or difluoromethyl; or trifluoromethoxy or difluoromethoxy;
    R 1 is hydrogen or C,-C 4 alkyl;
    R 2 is hydrogen or C 1 -C 4 alkyl; or
    R 1 and R 2 together are C 2 -C 5 alkylene;
    R 2 is C 1 -C 4 alkyl;
    R 4 is C 1 -C 4 alkyl; or
    R 3 and R 4 together are C 2 -C 6 alkylene;
    R 6 and R 6 independently are (1) hydrogen; (2) halogen; (3) C 1 -C 4 alkyl; (4) C 1 -C 4 alkoxy; (5) trifluoromethoxy; (6) cyano; (7) nitro; (8) C 1 -C 4 haloalkyl; (9) R b SO n - wherein n is the integer 0, 1 or 2; and R b is (a) C 1 -C 4 alkyl; (b) C 1 -C 4 alkyl substituted with halogen or cyano; (c) phenyl; or (d) benzyl; (10) -NR c R d wherein R c and R d independently are hydrogen or C 1 -C 4 alkyl; (11) R e C(O)- wherein R e is C 1 -C 4 alkyl or C 1 -C 4 alkoxy; or (12) -SO 2 NR c R d wherein R c and R d are as defined; and (13) -N(R c )C(O)R d wherein R c and R d are as defined and their salts.

    Abstract translation: 下式的化合物其中R是氢; 卤素; C1-C2烷基; C1-C2烷氧基; 硝基; 氰基; C1-C2卤代烷基; 或RaSO n - 其中n是0或2并且R a是C 1 -C 2烷基，三氟甲基或二氟甲基; 或三氟甲氧基或二氟甲氧基; R1是氢或C1-C4烷基; R2是氢或C1-C4烷基; 或R1和R2一起为C2-C5亚烷基; R2是C1-C4烷基; R4是C1-C4烷基; 或R3和R4一起为C2-C6亚烷基; R6和R6独立地是（1）氢; （2）卤素; （3）C 1 -C 4烷基; （4）C 1 -C 4烷氧基; （5）三氟甲氧基; （6）氰基; （7）硝基; （8）C 1 -C 4卤代烷基; （9）RbSOn-其中n是整数0,1或2; 并且R b是（a）C 1 -C 4烷基; （b）被卤素或氰基取代的C1-C4烷基; （c）苯基; 或（d）苄基; （10）-NR c R d，其中R c和R d独立地为氢或C 1 -C 4烷基; （11）ReC（O） - ，其中Re是C1-C4烷基或C1-C4烷氧基; 或（12）-SO2NRcRd，其中Rc和Rd如所定义; 和（13）-N（Rc）C（O）Rd，其中Rc和Rd如上定义。

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