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    171.
    发明专利
    未知

    公开(公告)号：ID24575A

    公开(公告)日：2000-07-27

    申请号：ID20000977

    申请日：1998-11-24

    Applicant: BASF AG

    Inventor： ERBES JORG ,  LUDWIG ALFONS ,  PIPPER GUNTER

    IPC: C08J3/12 ,  B01D11/02 ,  B29B9/16 ,  C08G69/00 ,  C08G69/04 ,  C08G69/16 ,  C08G69/46

    Abstract: A process for continuous extraction of polyamide particles using a recirculating extractant in a vertical extraction column that is divided into two zones comprises treating the polyamide with an aqueous extractant comprising from 40 to 95% by weight of epsi-caprolactam in a first zone at from 100 to 140° C., and then effecting an aftertreatment with water in a second zone. The caprolactam can then be extracted in a conventional manner. The process provides for economical production of polyamide having a low dimer content.

    172.
    发明专利
    未知

    公开(公告)号：DE59605251D1

    公开(公告)日：2000-06-21

    申请号：DE59605251

    申请日：1996-02-03

    Applicant: BASF AG

    Inventor： WARZELHAN VOLKER ,  PIPPER GUNTER ,  SEELIGER URSULA ,  BAUER PETER ,  PAGGA UDO ,  YAMAMOTO MOTONORI

    IPC: C08J5/00 ,  A61L15/26 ,  A61L15/62 ,  C08G63/183 ,  C08G63/20 ,  C08G63/60 ,  C08G63/668 ,  C08G63/672 ,  C08G63/688 ,  C08G63/91 ,  C08J9/00 ,  C08J9/04 ,  C08L67/00 ,  C08L101/16 ,  C09J167/00 ,  D21H19/28

    Abstract: PCT No. PCT/EP96/00457 Sec. 371 Date Aug. 14, 1997 Sec. 102(e) Date Aug. 14, 1997 PCT Filed Mar. 5, 1996 PCT Pub. No. WO96/25446 PCT Pub. Date Aug. 22, 1996Biodegradable polyesters having a molecular weight (Mn) of from 5000 to 50,000 g/mol (measured by gel permeation chromatography), a viscosity number of from 30 to 350 g/ml (measured in 50:50 by weight of o-dichlorobenzene/phenol at a concentration of 0.5% by weight of polyester at 25 DEG C.), and a melting point of from 50 to 170 DEG C., and having both hydroxyl and carboxyl end groups, the molar ratio of carboxyl end groups to hydroxyl end groups being greater than one, which is obtained by reacting a mixture consisting essentially of a1) a mixture consisting essentially of from 45 to 80 mol % of adipic acid or ester-forming derivatives thereof, or mixtures thereof, from 20 to 55 mol % of terephthalic acid or ester-forming derivatives thereof, or mixtures thereof, and from 0 to 5 mol % of a sulfonate compound, where the sum of the individual mole percentages is 100 mol %, and a2) a dihydroxy compound selected from the group consisting of C2-C6-alkanediols and C5-C10-cycloalkanediols, in the presence of from 0.01 to 5 mol %, per mol of component a1), of a compound D having at least three groups capable of ester formation, the molar ratio of a1) to a2) being from 0.4:1 to 1.5:1, polymers and biodegradable thermoplastic molding compositions, processes for their preparation and their use for producing biodegradable moldings, adhesives, foams and blends with starch obtained from the polymers or molding compositions.

    BIODEGRADABLE POLYESTERS
    175.
    发明专利
    BIODEGRADABLE POLYESTERS 未知

    公开(公告)号：PL332303A1

    公开(公告)日：1999-08-30

    申请号：PL33230397

    申请日：1997-09-19

    Applicant: BASF AG

    Inventor： KOWITZ CHRISTOPH ,  BAUER PETER ,  BEIMBORN DIETER BERNHARD ,  BRUCHMANN BERND ,  FALLER UWE ,  LAUN MARTIN ,  PAGGA UDO ,  PIPPER GUNTER ,  WARZELHAN VOLKER

    IPC: C08J5/00 ,  C08G18/42 ,  C08G18/76 ,  C08G18/79 ,  C08G63/20 ,  C09D5/00 ,  C09D167/00 ,  C09D175/04 ,  D01F6/84 ,  D01F6/92 ,  C08G63/78

    Abstract: PCT No. PCT/EP97/04908 Sec. 371 Date Mar. 17, 1999 Sec. 102(e) Date Mar. 17, 1999 PCT Filed Sep. 19, 1997 PCT Pub. No. WO98/12242 PCT Pub. Date Mar. 20, 1998Biodegradable polyesters based on A) 95-99.99 mol % of at least one polyester A containing as monomeric building blocks of an acid component comprising a11) 20-95 mol % of at least one aliphatic or cycloaliphatic dicarboxylic acid or its ester-forming derivative and a12) 5-80 mol % of at least one aromatic dicarboxylic acid or its ester-forming derivative and at least one dihydroxy compound or at least one amino alcohol or their mixtures, and B) 0.01-5 mol % of a mixture comprising mono-, bi-, tri-, tetra- and higher-nuclear isocyanurates or corresponding compounds containing two, three or four functional groups capable of reacting with the end groups of polyester A, or mixtures of the isocyanurates and the corresponding compounds, as well as molding compositions comprising said polyesters, their manufacture and their use in the manufacture of moldings, filsm, fibers and coatings.

    180.
    发明专利
    未知

    公开(公告)号：DE59502072D1

    公开(公告)日：1998-06-10

    申请号：DE59502072

    申请日：1995-02-03

    Applicant: BASF AG

    Inventor： FISCH HERBERT DR ,  PIPPER GUNTER ,  MUEHLBACH KLAUS DR ,  GOERRISSEN HEINER DR

    IPC: C08G69/26 ,  C08J5/18 ,  C08L77/00 ,  C08L77/06

    Abstract: Partly aromatic, partly crystalline, thermoplastic polyamide moulding material (I) contain (A) 40-100 wt.% of a copolyamide contg. (a1) 30-44 mole% terephthalic acid units, (2a) 6-20 mole% isophthalic acid units, (a3) 43-49.5 mole% hexamethylenediamine units and (a4) 0.5-7 mole% of units derived from 6-30C cyclic aliphatic diamines, (B) 0-50 wt.% fibrous or particulate filler, (c) 0-30 wt.% rubber-elastic polymer and (D) 0-30 wt.% normal additives and processing aids. Also claimed are moulded prods. obtd. from (I). Copolyamide (A) comprises 32-40 mole% (a1), 10-18 mole% (a2); 46-48.5 mole% (a3) and 1.5-4 mole% (a4). Pref., (A) has a triamine content of less than 0.5 wt.% and a degree of crystallinity of more than 30%. Pref. diamine (a4) is bis-(4-aminocyclohexyl)-methane (BACM) or bis-(4-amino-4-methylcyclohexyl)-methane.

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