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    Method for producing alcohol
    181.
    发明专利
    Method for producing alcohol 审中-公开
    生产醇的方法

    公开(公告)号：JP2009167129A

    公开(公告)日：2009-07-30

    申请号：JP2008007497

    申请日：2008-01-17

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： IWAHAMA TAKAHIRO ,  ISHII YASUTAKA

    IPC: C07C29/34 ,  C07B61/00 ,  C07C31/12 ,  C07C31/125

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an alcohol, by which the alcohol having an elongated carbon chain can efficiently be produced from a primary alcohol in the presence of a small amount of a catalyst.
    SOLUTION: The method for producing the alcohol is characterized by dimerizing the primary alcohol in the presence of a compound of an element in the groups 8 to 10 in the periodic table, a phosphine-based ligand and a base to obtain the alcohol having the elongated carbon chain. The primary alcohol includes ethanol, 1-propanol, and 1-butanol. The compound of the element in the groups 8 to 10 in the periodic table includes an iridium compound. The compound of the element in the groups 8 to 10 in the periodic table is preferably used in an amount of

    Abstract translation: 待解决的问题：提供一种生产醇的方法，通过该方法可以在少量的催化剂存在下，由伯醇有效地制备具有细长碳链的醇。 解决方案：醇的制备方法的特征在于在元素周期表第8-10族元素的化合物，膦类配体和碱的存在下使伯醇二聚，得到醇 具有细长的碳链。 伯醇包括乙醇，1-丙醇和1-丁醇。 元素周期表第8-10族元素的化合物包括铱化合物。 元素周期表中第8至10族元素的化合物优选以基于伯醇的<0.1mol％的量使用。 版权所有（C）2009，JPO＆INPIT

    Method for producing 1(4h)-naphthalenone derivative
    184.
    发明专利
    Method for producing 1(4h)-naphthalenone derivative 审中-公开
    生产1（4H） - 三苯基膦衍生物的方法

    公开(公告)号：JP2007238493A

    公开(公告)日：2007-09-20

    申请号：JP2006062136

    申请日：2006-03-08

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA ,  IWAHAMA TAKAHIRO

    IPC: C07C45/49 ,  C07B61/00 ,  C07C49/643 ,  C07C49/755

    Abstract: PROBLEM TO BE SOLVED: To provide a method for easily producing a 1(4H)-naphthalenone derivative in a high yield.
    SOLUTION: A styrene derivative is reacted with carbon monoxide in the presence of a palladium compound catalyst and a catalyst comprising a heteropoly acid or an oxoacid containing an element of P or Si and an element selected from V, Mo and W, to obtain the 1(4H)-naphthalenone derivative represented by formula (2) (wherein, R
    1 to R
    5 indicate each hydrogen or a group containing a nonmetal element).
    COPYRIGHT: (C)2007,JPO&INPIT

    Abstract translation: 待解决的问题：提供以高产率容易地制备1（4H） - 萘酮衍生物的方法。 解决方案：苯乙烯衍生物在钯化合物催化剂和包含杂多酸或含有P或Si元素的含氧酸和选自V，Mo和W的元素的催化剂存在下与一氧化碳反应， 得到由式（2）表示的1（4H） - 萘酮衍生物（其中，R 1 至R 5 表示每个氢或含有非金属元素的基团）。 版权所有（C）2007，JPO＆INPIT

    Method for producing alcohol
    185.
    发明专利
    Method for producing alcohol 有权
    生产醇的方法

    公开(公告)号：JP2007223947A

    公开(公告)日：2007-09-06

    申请号：JP2006046312

    申请日：2006-02-23

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  IWAHAMA TAKAHIRO

    IPC: C07C29/34 ,  C07B61/00 ,  C07C31/12 ,  C07C31/125

    Abstract: PROBLEM TO BE SOLVED: To provide a method for provide an alcohol, with which an alcohol with an extended carbon chain is obtained from an alcohol in a high yield.
    SOLUTION: The method for producing an alcohol comprises dimerizing a primary alcohol in the presence of a compound of an element of the group 8 to 10 of the periodic table and a base to give an alcohol with an extended carbon chain. The reaction is preferably carried out in the presence of a hydrogen receptor. An iridium compound is preferably used as the compound of an element of the group 8 to 10 of the periodic table. The base is preferably a strong base, for example, an alkali metal hydroxide such as sodium hydroxide, potassium hydroxide, etc., or an alkali metal alkoxide such as potassium t-butoxide, etc.
    COPYRIGHT: (C)2007,JPO&INPIT

    Abstract translation: 要解决的问题：提供一种提供醇的方法，以高产率从醇中获得具有延伸碳链的醇。 解决方案：醇的制备方法包括在元素周期表第8至10族元素的化合物和碱的存在下使伯醇二聚，得到具有延伸碳链的醇。 该反应优选在氢受体存在下进行。 优选使用铱化合物作为元素周期表第8〜10族元素的化合物。 碱优选为强碱，例如碱金属氢氧化物如氢氧化钠，氢氧化钾等，或碱金属醇盐如叔丁醇钾等。版权所有（C）2007， JPO＆INPIT

    Method for producing ketone
    186.
    发明专利
    Method for producing ketone 审中-公开
    生产酮的方法

    公开(公告)号：JP2006248952A

    公开(公告)日：2006-09-21

    申请号：JP2005066404

    申请日：2005-03-09

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  IWAHAMA TAKAHIRO ,  NAKANO TATSUYA

    IPC: C07C221/00 ,  C07B61/00 ,  C07C225/06 ,  C07C225/22 ,  C07D207/27 ,  C07D209/08 ,  C07D211/44 ,  C07D215/06 ,  C07D217/06 ,  C07D223/04 ,  C07D295/08 ,  C07D295/10

    Abstract: PROBLEM TO BE SOLVED: To provide a method for simply producing a ketone containing a nitrogen atom at the α-position such as an α-aminoketone in a high yield.
    SOLUTION: The production method comprises reacting an alcohol represented by formula (1) (R
    1 is a hydrogen atom or an organic group) with a nitrogen atom-containing compound represented by formula (2) (R
    2 and R
    3 are the same or different and are each a hydrogen atom or an organic group and R
    2 and R
    3 may be mutually bonded with an adjacent nitrogen atom to form a ring) in the presence of a compound of an element of the group VIII of the periodic table to give a ketone represented by formula (3).
    COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 待解决的问题：提供一种在α-位上简单地生产含α-氮杂原子的酮的方法，例如α-氨基酮以高产率。 解决方案：制备方法包括使由式（1）表示的醇与式（2）表示的含氮原子化合物反应，其中R 1为氢原子或有机基团， （R SP＆gt; 2＆lt; SP＆gt;和＆lt; SP＆gt; 3＆lt; SP＆gt; 3相同或不同，并且各自为氢原子或有机基团，且R 2 和R 3周期表第VIII族元素的化合物存在下，可以与相邻的氮原子相互键合形成环），得到由式（3）表示的酮。 版权所有（C）2006，JPO＆NCIPI

    Method for producing nitrile compound
    187.
    发明专利
    Method for producing nitrile compound 审中-公开
    生产氮化合物的方法

    公开(公告)号：JP2006248927A

    公开(公告)日：2006-09-21

    申请号：JP2005064657

    申请日：2005-03-08

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  IWAHAMA TAKAHIRO ,  NAKANO TATSUYA

    IPC: C07C253/30 ,  C07B61/00 ,  C07C255/32 ,  C07C255/33 ,  C07C255/37

    Abstract: PROBLEM TO BE SOLVED: To provide a method for efficiently producing a nitrile compound having a carbon chain extended by α-alkylation of a nitrile compound in the presence of a catalyst under a mild condition. SOLUTION: The production method comprises reacting a nitrile compound represented by formula (1) (R 1 and R 2 are the same or different and are each a hydrogen atom or an organic group and R 1 and R 2 may be mutually bonded with an adjacent carbon atom to form a ring) with an alcohol represented by formula (2) (R 3 and R 4 are the same or different and are each a hydrogen atom or an organic group and R 3 and R 4 may be mutually bonded with an adjacent carbon atom to form a ring) to give a nitrile compound having an extended carbon chain represented by formula (3) in the presence of a compound of an element of the group 9 of the periodic table and a base. COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 待解决的问题：提供一种在温和条件下，在催化剂存在下，有效地制备具有通过腈化合物的α-烷基化延伸的碳链的腈化合物的方法。 解决方案：制备方法包括使由式（1）表示的腈化合物（R 1 SP＆lt; SP＆gt;和R 2 SP 2）相同或不同，并且各自为氢原子 或有机基团，并且R 1和R 2彼此可以与相邻的碳原子相互键合形成环）与式（2）表示的醇（R' SP> 3 和R 4 相同或不同，并且各自为氢原子或有机基团，并且R“SP”3 和R SP'可以与相邻的碳原子相互键合以形成环）以在周期表第9族元素的化合物存在下得到具有由式（3）表示的延伸碳链的腈化合物和 一个基地 版权所有（C）2006，JPO＆NCIPI

    METHOD FOR PRODUCING AROMATIC CARBOXYLIC ACID
    188.
    发明专利
    METHOD FOR PRODUCING AROMATIC CARBOXYLIC ACID 审中-公开

    公开(公告)号：JP2004256482A

    公开(公告)日：2004-09-16

    申请号：JP2003051362

    申请日：2003-02-27

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07C51/255 ,  B01J23/44 ,  B01J27/199 ,  C07B61/00 ,  C07C51/145 ,  C07C63/04 ,  C07C65/21 ,  C07C67/29 ,  C07C69/14

    Abstract: PROBLEM TO BE SOLVED: To produce an aromatic carboxylic acid corresponding to an aromatic compound from the aromatic compound by using an inexpensive oxidizing agent excellent in handleability and having little load on environment. SOLUTION: The method for producing the aromatic carboxylic acid comprises producing the corresponding aromatic carboxylic acid in which the carboxy group of the carboxylic acid is bonded to an aromatic ring of (C) an aromatic compound by reacting the aromatic compound (C) with (D) carbon monoxide and (E) molecular oxygen in the presence of (A) a palladium compound catalyst and (B) a catalyst composed of (B1) a heteropoly acid or its salt or (B2) a mixture of oxo acids or their salts containing an element of P or Si with at least one element selected from V, Mo and W. COPYRIGHT: (C)2004,JPO&NCIPI

    Method for producing carboxylic acid using manganese catalyst or the like
    190.
    发明专利
    Method for producing carboxylic acid using manganese catalyst or the like 有权
    使用锰锰催化剂生产羧酸的方法或类似方法

    公开(公告)号：JP2003327557A

    公开(公告)日：2003-11-19

    申请号：JP2002282040

    申请日：2002-09-26

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07C51/353 ,  C07B61/00 ,  C07C53/126 ,  C07C53/128 ,  C07C53/134 ,  C07C53/136 ,  C07C55/02

    Abstract: PROBLEM TO BE SOLVED: To provide a method for efficiently producing a carboxylic acid corresponding to a compound in which an alkyl group or an alkenyl group is bound to the α-position with respect to an acyloxycarbonyl group by a catalytic radical addition reaction.
    SOLUTION: The method for producing the carboxylic acid represented by formula (3a) or (3b) (wherein, R
    b and R
    c denote each a hydrogen atom, an organic group or the like; and R
    d , R
    e , R
    f , R
    g , R
    h and R
    i denote each a hydrogen atom, an organic group or the like) is carried out as follows. An acyloxycarbonyl group-containing compound represented by general formula (1) [wherein, R
    a denotes a hydrogen atom, an organic group or the like; and R
    b and R
    c are each the same as in formula (3a) or (3b)] is reacted with a compound represented by formula (2a) or (2b) [wherein, R
    d , R
    e , R
    f , R
    g , R
    h and R
    i are each the same as in formula (3a) or (3b)] and having a carbon - carbon unsaturated bond in the presence of a catalyst of a compound of groups 5-9 elements of the periodic table and oxygen to produce the carboxylic acid represented by formula (3a) or (3b) or its cyclization product.
    COPYRIGHT: (C)2004,JPO

    Abstract translation: 待解决的问题：提供一种方法，用于通过催化自由基加成反应有效地制备相对于酰氧基羰基将烷基或烯基与α-位相结合的化合物相应的羧酸 。 解决方案：由式（3a）或（3b）表示的羧酸的制备方法（其中，R SP和R SP均表示氢原子， 有机基团等; R 1，R 2，R 3，R 6， SP> h 和R i 表示氢原子，有机基团等）如下进行。 由通式（1）表示的含酰氧基羰基的化合物[其中，R“表示氢原子，有机基团等; 和式（2a）或（2b）表示的化合物与式（3a）或（3b）中的每一个相同）与R（SP）b和/ [其中，R d ，R f ，R SP＆gt;和R＆lt; SP＆gt; i＆lt; / SP＆gt;各自与式（3a）或（3b）中相同]，并且在5-9元素的化合物的催化剂存在下具有碳 - 碳不饱和键 的周期表和氧气以产生由式（3a）或（3b）表示的羧酸或其环化产物。 版权所有（C）2004，JPO

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