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    아연을 함유하는 이미다졸륨계 이온성 액체를 사용하여 탄화수소 유분으로부터 질소 화합물을 제거하는 방법
    11.
    发明公开
    아연을 함유하는 이미다졸륨계 이온성 액체를 사용하여 탄화수소 유분으로부터 질소 화합물을 제거하는 방법 有权
    使用含锌的咪唑啉类离子液体从碳氢化合物中除去含氮化合物的方法

    公开(公告)号：KR1020100083474A

    公开(公告)日：2010-07-22

    申请号：KR1020090002867

    申请日：2009-01-14

    Applicant: 경희대학교 산학협력단

    Inventor： 김훈식 ,  허은수 ,  정스런 ,  정민석 ,  강호정

    IPC: C10G21/06 ,  C10G53/06

    CPC classification number: C10G21/06 ,  C10G21/20 ,  C10G2300/202

    Abstract: PURPOSE: A method for eliminating a nitrogen compound is provided to efficiently and economically remove an aromatic nitrogen compound using a simple extraction process using imidazole-based ionic liquid containing zinc. CONSTITUTION: A method for eliminating a nitrogen compound from hydrocarbons uses imidazole-based ionic liquid containing zinc which is generated by mixing ZnX_2 with imidazolium alkyl sulfate which is marked as a chemical formula 1. In the chemical formula 1, X is Cl, Br, or I and R1 and R2 are hydrogen or an alkyl group with C1-C10. The nitrogen compound is an aromatic nitrogen compound. A method for eliminating the nitrogen compound from hydrocarbons comprises a step of extracting the nitrogen compound from the hydrocarbons into the ionic liquid by contacting the imidazole-based ionic liquid containing zinc with the hydrocarbons and a step of separating the ionic liquid from the hydrocarbons.

    Abstract translation: 目的：提供一种消除氮化合物的方法，通过使用含有锌的咪唑类离子液体，使用简单的萃取方法有效且经济地除去芳族氮化合物。 构成：从烃中除去氮化合物的方法使用含锌的咪唑类离子液体，其是通过将ZnX_2与咪唑烷基硫酸盐混合而生成的，其标记为化学式1.在化学式1中，X为Cl，Br， 或I且R 1和R 2为氢或具有C 1 -C 10的烷基。 氮化合物是芳族氮化合物。 从烃中除去氮化合物的方法包括通过使含有锌的咪唑类离子液体与烃接触并从离子液体中分离出离子液体的步骤，从烃中将氮化合物提取到离子液体中。

    알킬렌 카보네이트의 제조방법 및 그를 위한 촉매
    13.
    发明授权
    알킬렌 카보네이트의 제조방법 및 그를 위한 촉매 有权
    制备碳酸亚烷基酯的方法和催化剂

    公开(公告)号：KR101232125B1

    公开(公告)日：2013-02-12

    申请号：KR1020100058567

    申请日：2010-06-21

    Applicant: 경희대학교 산학협력단

    Inventor： 김훈식 ,  정민석 ,  누엔딘콴 ,  심유나

    IPC: C07D317/34 ,  B01J31/12 ,  C07D233/96

    Abstract: 본 발명은 알킬렌 옥사이드와 이산화탄소로부터 알킬렌 카보네이트를 제조하는 방법 및 그를 위한 1,3-디알킬이미다졸륨 디할로디알킬포스페이토아연 촉매에 관한 것이다. 본 발명의 제조방법에 따르면, 알킬렌 카보네이트를 온화한 조건에서 짧은 시간에 고수율 및 고순도로 제조할 수 있으며, 본 발명에 따른 1,3-디알킬이미다졸륨 디할로디알킬포스페이토아연 촉매는 가격이 저렴할 뿐만 아니라 열 안정성이 뛰어나 분해되지 않기 때문에 할라이드 부산물을 생성하지 않는다.

    알킬렌 카보네이트의 제조방법 및 그를 위한 촉매
    14.
    发明公开
    알킬렌 카보네이트의 제조방법 및 그를 위한 촉매 有权
    制备亚烷基碳酸酯的方法和催化剂

    公开(公告)号：KR1020110138591A

    公开(公告)日：2011-12-28

    申请号：KR1020100058567

    申请日：2010-06-21

    Applicant: 경희대학교 산학협력단

    Inventor： 김훈식 ,  정민석 ,  누엔딘콴 ,  심유나

    IPC: C07D317/34 ,  B01J31/12 ,  C07D233/96

    Abstract: PURPOSE: A method for preparing alkylene carbonate from alkylene oxide and carbon dioxide is provided to quickly obtain alkylene carbonate of high yield and high purity. CONSTITUTION: A method for preparing alkylene carboante of chemical formula 3 comprises a step of reacting alkylene oxide of chemical formula 2 with carbon dioxide under the presence of 1,3-dialkylimidazolium dihalodialkylphosphato zinc catalyst of chemical formula 1. The reaction is performed at 80-140°C and 10-100 atm. The 1,3-dialkylimidazolium dihalodialkylphosphato zinc is prepared by reacting 1,3-dialkylimidazolium dialkylphosphate of chemical formula 4 with zinc halide of chemical formula 5(ZnX)2.

    Abstract translation: 目的：提供从环氧烷和二氧化碳制备碳酸亚烷酯的方法，以快速获得高产率和高纯度的碳酸亚烃酯。 构成：制备化学式3的亚烷基芳烃的方法包括在化学式1的1,3-二烷基咪唑二卤代二烷基磷酸锌催化剂存在下使化学式2的烯化氧与二氧化碳反应的步骤。反应在80- 140°C和10-100 atm。 通过使化学式4的1,3-二烷基咪唑二烷基磷酸酯与化学式5（ZnX）2的卤化锌反应制备二烷基咪唑鎓二卤代二烷基膦酸锌。

    지방족 디우레아의 제조방법
    15.
    发明公开
    지방족 디우레아의 제조방법 有权
    制备二氧化钛的方法

    公开(公告)号：KR1020110088749A

    公开(公告)日：2011-08-04

    申请号：KR1020100008396

    申请日：2010-01-29

    Applicant: 경희대학교 산학협력단

    Inventor： 김훈식 ,  정민석 ,  누엔딘콴 ,  심유나

    IPC: C07C273/18 ,  C07C275/04

    Abstract: PURPOSE: A method for manufacturing aliphatic diurea is provided to prepare diurea with high yield and high selectivity in a mild condition using water as a reaction solvent and catalyst and to simplify a refining process of products. CONSTITUTION: A method for manufacturing aliphatic diurea comprises a step of reacting C2-8 aliphatic diamine with urea to prepare aliphatic diurea using water as a reaction solvent and a catalyst. The C2-8 aliphatic diamine is 1,2-ethanediamine, 1,3-propanediamine, 1,4-butanediamine, 1,6-hexanediamine, 1,8-octane diamine, 1,2-cyclohexane diamine, 1,3-cyclohexanediamine, 1,4-cyclohexanediamine, 1,3-cyclohexane bismethylamine or 1,4-cyclohexane bismethylamine.

    Abstract translation: 目的：提供一种脂肪族二脲的制造方法，以水作为反应溶剂和催化剂，在温和条件下以高产率和高选择性制备二脲并简化产物的精制过程。 构成：制造脂肪族二脲的方法包括使C 2-8脂族二胺与尿素反应以使用水作为反应溶剂和催化剂制备脂族二脲的步骤。 C2-8脂族二胺是1,2-乙二胺，1,3-丙二胺，1,4-丁二胺，1,6-己二胺，1,8-辛二胺，1,2-环己烷二胺，1,3-环己二胺 1,4-环己烷二胺，1,3-环己烷二甲胺或1,4-环己烷二甲胺。

    이미다졸륨 할로겐화합물을 이용한알킬렌트리티오카보네이트의 제조방법
    18.
    发明公开
    이미다졸륨 할로겐화합물을 이용한알킬렌트리티오카보네이트의 제조방법 有权
    通过使用咪唑烷衍生物制备亚苄基二硫代碳酸酯的方法

    公开(公告)号：KR1020080104690A

    公开(公告)日：2008-12-03

    申请号：KR1020070051817

    申请日：2007-05-29

    Applicant: 경희대학교 산학협력단

    Inventor： 김훈식 ,  이제승 ,  정민석 ,  배현우

    IPC: C07D339/04

    Abstract: A method for preparing an alkylene trithiocarbonate is provided to reduce the generation of polymer by-product and to allow the reaction to be carried out under mild condition with a high selectivity. A method for preparing an alkylene trithiocarbonate represented by the formula 2 comprises the step of reacting an alkylene carbonate represented by the formula 1 and carbon disulfide (CS2) in the presence of an imidazolium halogen compound catalyst, wherein R1 and R2 are independently H, a C1-C4 alkyl group or a phenyl group. The amount of the imidazolium halogen compound catalyst is 0.005-0.1 mol to 1 mol of the alkylene carbonate.

    Abstract translation: 提供了一种制备亚硫代碳酸酯的方法，以减少聚合物副产物的产生，并允许反应在温和条件下以高选择性进行。 制备由式2表示的亚硫代三硫代碳酸酯的方法包括在咪唑鎓卤素化合物催化剂存在下使式1表示的碳酸亚烷基酯与二硫化碳（CS2）反应的步骤，其中R 1和R 2独立地为H， C1-C4烷基或苯基。 咪唑鎓卤化合物催化剂的量相对于1mol碳酸亚烷基酯为0.005-0.1mol。

    함불소알콕시실란 유도체의 제조방법
    19.
    发明授权
    함불소알콕시실란 유도체의 제조방법 有权
    氟化烷基硅烷衍生物的制备方法

    公开(公告)号：KR100778032B1

    公开(公告)日：2007-11-28

    申请号：KR1020060048195

    申请日：2006-05-29

    Applicant: 경희대학교 산학협력단

    Inventor： 김훈식 ,  정민석 ,  이보라 ,  이제승 ,  박상준

    IPC: C07F7/18

    CPC classification number: C07F7/1844 ,  C07F7/12

    Abstract: A method for efficiently preparing a fluorinated alkoxysilane derivative is provided to increase the yield of a reaction of a chlorosilane compound and a fluorinated alcohol using a tertiary amine compound as a media with little formation of side products and recover the products very simply. A method for preparing a fluorinated alkoxysilane derivative represented by the formula(1) comprises a step of reacting a fluorinated alcohol of RfOH with a chlorosilane compound of R1R2R3Si-Cl in the presence of a tertiary amine compound represented by the formula(4b) or (4c) at a temperature of -20 to 50 deg.C, wherein each R1, R2, R3 and R4 is C1-6 hydrocarbonyl or phenyl, Rf is C1-6 fluorinated hydrocarbonyl having 1-8 fluorine atom(s). The reaction is performed under a non-solvent or a non-polar solvent condition.

    Abstract translation: 提供一种有效制备氟化烷氧基硅烷衍生物的方法，以提供氯代硅烷化合物和氟化醇的反应产率，使用叔胺化合物作为介质，几乎不形成副产物并非常简单地回收产物。 制备由式（1）表示的氟化烷氧基硅烷衍生物的方法包括：在由式（4b）表示的叔胺化合物或式（4b）表示的叔胺化合物或（4b）所示的叔胺化合物存在下，使RfOH的氟化醇与R1R2R3Si-Cl的氯硅烷化合物反应的步骤， 4c），其中每个R 1，R 2，R 3和R 4是C 1-6烃基或苯基，R f是具有1-8个氟原子的C 1-6氟化烃基。 反应在非溶剂或非极性溶剂条件下进行。

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