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    세라믹 경량연와의 제조방법
    16.
    发明授权
    세라믹 경량연와의 제조방법 失效
    陶瓷砖的制备方法

    公开(公告)号：KR1019910005025B1

    公开(公告)日：1991-07-22

    申请号：KR1019890006467

    申请日：1989-05-15

    Applicant: 한국화학연구원

    Inventor： 백행남 ,  서태수 ,  곽중협

    IPC: C04B38/10

    Abstract: lightweight ceramic brick having 0.08-1.5 mm micropore, 0.3-0.9 g/cm3 bulk density and 5-30 kg/cm2 compressive strength is produced by foaming a slurry as a ceramic raw material with a foaming agent, mixing the foamed material with a viscosity- controlling agent and strength-promoting agent, and molding, drying and firing the mixt. The slurry has 7-14 of hydrogen- ion concentration coefficient. The ceramic brick is used as a furnace material and low-temp. plant material.

    Abstract translation: 通过使用发泡剂使作为陶瓷原料的浆料发泡，将发泡材料与粘度相混合来制造具有0.08-1.5mm微孔，0.3-0.9g / cm3堆积密度和5-30kg / cm2抗压强度的轻质陶瓷砖 - 控制剂和强力促进剂，以及成型，干燥和焙烧混合物。 该浆料具有7-14的氢离子浓度系数。 陶瓷砖用作炉料和低温。 植物材料。

    음이온 포스핀 금속 착화합물이 층간 결합된 하이드로탈사이트 형태의 새로운 화학물질 및 이의 제조방법
    18.
    发明授权
    음이온 포스핀 금속 착화합물이 층간 결합된 하이드로탈사이트 형태의 새로운 화학물질 및 이의 제조방법 失效
    支链氢化间硝基喹啉金属络合物及其制备方法

    公开(公告)号：KR1019960010080B1

    公开(公告)日：1996-07-25

    申请号：KR1019930006150

    申请日：1993-04-13

    Applicant: 한국화학연구원

    Inventor： 백행남 ,  이정호 ,  심규선 ,  김형록 ,  이기화 ,  한요한

    IPC: B01J21/16

    Abstract: TtLl(SP)m-[M(II)1-xM(III)x(OH)2 X+(Ax/n)= yH2O) is one that anion phosphine metal complex(eqn 1: TtLl(SP)m) is coupled between layers of hydrotalcite compound (eqn 2: [M(II)1-xM(III)x(OH)2 X+(Ax/n)= yH2O), where T is Rh, Co, Ru, Ir, Pt, Ni, Cu, Mn, Fe, Pd, Ag or Au; L is Cl, CO, NO, COD, H, SR, OH, NH3 or alkylamine; SP is anion phosphine ligand, sulfonated or carbonated alkyl or anion allyl phosphine; t is 1-2; l is 0-8; m is 1-8; M(II) is Mg, Ni, Co, Fe, An, Cu or Li; M(III) is Al, Cr or Fe; A is organic or inorganic anion with quantity of electric charge of n; X is 0.2-0.4; n is the quantity of electric charge of A; y is the number of water molecule.

    Abstract translation: Ttll（SP）m- [M（II）1-xM（III）x（OH）2 X +（Ax / n）= yH2O）是阴离子膦金属络合物（等式1：TtL1（SP） 水滑石化合物层（方程2：[M（II）1-xM（III）x（OH）2 X +（Ax / n）= yH 2 O），其中T是Rh，Co，Ru，Ir，Pt，Ni， Cu，Mn，Fe，Pd，Ag或Au; L是Cl，CO，NO，COD，H，SR，OH，NH 3或烷基胺; SP是阴离子膦配体，磺化或碳酸化烷基或阴离子烯丙基膦; t是1-2; l为0-8; m为1-8; M（II）是Mg，Ni，Co，Fe，An，Cu或Li; M（III）为Al，Cr或Fe; A是电荷量为n的有机或无机阴离子; X为0.2-0.4; n是A的电荷量; y是水分子的数量。

    헤테로폴리산계 촉매의 제조방법
    20.
    发明授权
    헤테로폴리산계 촉매의 제조방법 失效
    生产杂多酸催化剂的方法

    公开(公告)号：KR1019960003795B1

    公开(公告)日：1996-03-22

    申请号：KR1019930006148

    申请日：1993-04-13

    Applicant: 한국화학연구원

    Inventor： 백행남 ,  이정호 ,  이기화 ,  신현관

    IPC: B01J27/199

    Abstract: This is new heteropolyacid-based catalyst of formula (I). The manufacturing method comprises :1)dissolving 12-molybdophosphoric acid in water followed by adding phosphoric acid and vanadium pentoxide; 2)refluxing the mixture for 12hrs at an elevated temp. to produce molybdovanadophosphoric acid solution(A); 3)dissolving one kind of Cu, Ce, Ru, Bi, Sb N-heterocyclic compd and above one of oxalic acid or its salts(B); 4)adding solution B to solution A with stirring at 30-80deg.C and maturing the stirred mixture; 5)cooling it to room temp and stirring for 30min, filtering and washing it; 6)drying the cake and molding; and 7)1st firing at 380-450deg.C for 2-10hrs, and 2nd firing at 260-420deg.C for 2-10hrs.

    Abstract translation: 这是式（I）的新型杂多酸催化剂。 制造方法包括：1）将12-钼磷酸溶解在水中，然后加入磷酸和五氧化二钒; 2）在升高的温度下将混合物回流12小时。 生产钼钒磷酸溶液（A）; 3）溶解一种草酸或其盐（B）中的一种Cu，Ce，Ru，Bi，Sb N-杂环化合物; 4）将溶液B在30-80℃搅拌下加入到溶液A中，熟化搅拌的混合物; 5）将其冷却至室温并搅拌30分钟，过滤并洗涤; 6）干燥蛋糕和成型; 7）第一次烧制380-450℃2-10小时，第二次焙烧260-420℃2-10小时。

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