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    PRODUCTION OF POLYURETHANE FOAM
    11.
    发明专利
    PRODUCTION OF POLYURETHANE FOAM 失效

    公开(公告)号：JPH08269157A

    公开(公告)日：1996-10-15

    申请号：JP10306195

    申请日：1995-04-03

    Applicant: KAO CORP

    Inventor： ISAYAMA YASUTOSHI ,  MORII MASAYOSHI ,  HIRAISHI TOKUJI ,  NOMURA TAKAYUKI

    IPC: C08J9/02 ,  C08G18/40 ,  C08G18/54 ,  C08G101/00 ,  C08J9/14

    Abstract: PURPOSE: To obtain a polyurethane foam by carrying out a urethanization reaction in the presence of a formaldehyde addition condensation product (salt) of an aromatic compound, having dimensional stability under various conditions despite of conventional molding density, useful as a heat insulating material, etc. CONSTITUTION: In obtaining this polyurethane foam from a polyol and a polyisocyanate in the presence of a blowing agent, a catalyst and other auxiliaries, a urethanization reaction is carried out in the presence of a formaldehyde addition condensation product (salt) of an aromatic compound and/or its salt. A formaldehyde addition condensation product of one or more compounds selected from the group consisting of a melaminesulfonic acid, a phenolsulfonic acid and a naphthalenesulfonic acid is used as the condensate and the number- average molecular weight of the condensate is preferably 2,000-50,000 and, for example, 1-5 pts.wt. of the condensate is used based on 100 pts.wt. of the polyol.

    CATALYST FOR PRODUCING POLYURETHANE AND PRODUCTION OF POLYURETHANE USING THE SAME
    12.
    发明专利
    CATALYST FOR PRODUCING POLYURETHANE AND PRODUCTION OF POLYURETHANE USING THE SAME 失效

    公开(公告)号：JPH0790040A

    公开(公告)日：1995-04-04

    申请号：JP26182393

    申请日：1993-09-24

    Applicant: KAO CORP

    Inventor： MORII MASAO ,  FUKUSHIMA TETSURO ,  ISAYAMA YASUTOSHI ,  HARADA SHOICHIRO

    IPC: C08G18/18

    Abstract: PURPOSE:To obtain the subject low smellable catalyst having a good catalytic activity, and useful as a catalyst for producing polyurethane molded products. CONSTITUTION:This catalyst is represented by the formula (n) is 8-12, preferably 9). The catalyst is obtained preferably e.g. by subjecting 8-diaminooctane, etc., to a reductive methylation reaction, etc. The catalyst is preferably used, when a polyol is reacted with a polyisocyanate compound such as 2,4-tolylene diisocyanate. For example, N,N,N',N'-tetramethylnonanediamine is preferably used as the catalyst.

    CATALYST COMPOSITION FOR PRODUCTION OF POLYURETHANE FOAM AND PRODUCTION OF POLYURETHANE FOAM BY USING THE SAME
    14.
    发明专利
    CATALYST COMPOSITION FOR PRODUCTION OF POLYURETHANE FOAM AND PRODUCTION OF POLYURETHANE FOAM BY USING THE SAME 失效

    公开(公告)号：JPH05209034A

    公开(公告)日：1993-08-20

    申请号：JP1116592

    申请日：1992-01-24

    Applicant: KAO CORP

    Inventor： HARADA SHOICHIRO ,  MORII MASAYOSHI ,  ISAYAMA YASUTOSHI

    IPC: C08G18/20 ,  C08G18/18 ,  C08G18/30 ,  C08G18/32 ,  C08G18/48 ,  C08G101/00

    Abstract: PURPOSE:To obtain the subject composition which can give a polyurethane foam with good thermal conductivity, friability and mold filling property by incorporating three tert. amine compounds each containing a specified ring structure. CONSTITUTION:The objective composition is obtained by mixing three tert. amine compounds each containing a ring structure in the molecule and represented by formula I (wherein R1 and R2 are each 1-3C alkyl or dimethylaminoalkyl or hydroxyalkyl with 1-3C alkyl), formula II (wherein R3 and R4 are each 1-3C alkyl or cyclohexyl) and formula III (wherein R5 is H or 1-C alkyl; R is 1-4C alkyl or hydroxyalkyl). The mixing ratio is such that 5-20wt.% compound of formula I, 5-20wt.% compound of formula II and 60-90wt.% compound of formula III are mixed with each other. Only when a catalyst containing all of these three compounds is used, a urethane foam with good thermal conductivity, friability and mold filling property can be produced.

    CATALYST FOR POLYURETHANE PRODUCTION
    16.
    发明专利
    CATALYST FOR POLYURETHANE PRODUCTION 失效

    公开(公告)号：JPH03190915A

    公开(公告)日：1991-08-20

    申请号：JP33242389

    申请日：1989-12-20

    Applicant: KAO CORP

    Inventor： MORII MASAYOSHI ,  HARADA SHOICHIRO ,  ISAYAMA YASUTOSHI

    IPC: C08G18/20 ,  C08G18/18

    Abstract: PURPOSE:To obtain the subject new non-shift type catalyst consisting of a specific compound having strong catalyst activity and reduced in amount used without shifting to a surface of resin or vaporization after the reaction. CONSTITUTION:The aimed catalyst consisting of a compound expressed by the formula (R is H or methyl; n is 0-3). The aimed catalyst is obtained by adding ethylene oxide or propylene oxide to N-methyl-4-hydroxy-piperidine using potassium hydroxide as a catalyst.

    CATALYST COMPOSITION FOR POLYMERIZING POLYURETHANE
    17.
    发明专利
    CATALYST COMPOSITION FOR POLYMERIZING POLYURETHANE 失效

    公开(公告)号：JPH01319521A

    公开(公告)日：1989-12-25

    申请号：JP15171388

    申请日：1988-06-20

    Applicant: KAO CORP

    Inventor： ISAYAMA YASUTOSHI

    IPC: C08G18/16 ,  C08G18/18

    Abstract: PURPOSE:To obtain the subject composition, useful for producing polyurethane, such as rigid foam, of electric refrigerators, etc., and capable of improving resin fluidity, etc., and curing in a short time by compounding an organic carboxylate of a tertiary amine with a specific amount of a quaternary ammonium salt compound. CONSTITUTION:The objective composition obtained by mixing (A) a tertiary amine (e.g., N-methylmorpholine) with, as necessary, a polar organic solvent, stirring the resultant mixture while cooling a container, adding and mixing an organic carboxylic acid (preferably formic, acetic acid, etc.) in an amount of 0.1-1.0 equiv. based on 1 equiv. N of the tertiary amine in divided several portions, cooling the resultant mixture and compounding (B) 5-50wt.% quaternary ammonium salt compound (obtained by reacting an acid in the presence of a tertiary amine and then reacting an alkylene oxide in an amount of >=1mol based on 1mol tertiary amine) so as to provide 100wt.% total amount of both components (A) and (B).

    Method for producing polyurethane foam
    18.
    发明专利
    Method for producing polyurethane foam 有权
    生产聚氨酯泡沫的方法

    公开(公告)号：JP2005171047A

    公开(公告)日：2005-06-30

    申请号：JP2003411593

    申请日：2003-12-10

    Applicant: Kao Corp ,  花王株式会社

    Inventor： ISHIKAWA ATSUSHI ,  ISAYAMA YASUTOSHI

    IPC: C08G18/20 ,  C08G101/00

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing polyurethane foam in which the amount of VOC (volatile organic compounds) generated from polyurethane foam on the basis of an amine-based catalyst is reduced even in a high-temperature state and fogging hardly occurs and which has excellent heat resistance, excellent hardness properties and small residual compressive strain.
    SOLUTION: The method for producing a polyurethane foam comprises reacting a polyol component with an isocyanate component in the presence of a catalyst containing a compound represented by formula (I): (CH
    3 )
    2 N(CH
    2 )
    p OH (1) (p is an integer of 4-9) and a compound represented by formula (II) (R
    1 is a 2 or 3C straight-chain or branched-chain aminoalkyl group or hydroxyalkyl group; R
    2 is a hydrogen atom or a 1-4C straight-chain or branched-chain alkyl group) and a blowing agent. The polyurethane foam is obtained by the production method.
    COPYRIGHT: (C)2005,JPO&NCIPI

    Abstract translation: 要解决的问题：提供一种聚氨酯泡沫的制造方法，其中，即使在高温状态下，基于胺系催化剂的聚氨酯泡沫产生的VOC（挥发性有机化合物）的量也降低， 几乎不发生起雾，具有优异的耐热性，优异的硬度特性和较小的残余压缩应变。 解决方案：聚氨酯泡沫的制造方法包括在含有式（I）表示的化合物的催化剂存在下使多元醇组分与异氰酸酯组分反应：（CH 3 SB 3）SB （2）表示的化合物（Ⅱ）表示的化合物（式中，R 1，R 2，R 3，R 5， R 1 是2或3C直链或支链氨基烷基或羟烷基; R 2 SP 2是氢原子或1-4C直链或支链 链烷基）和发泡剂。 通过制造方法得到聚氨酯泡沫。 版权所有（C）2005，JPO＆NCIPI

    CATALYST COMPOSITION FOR PRODUCING POLYURETHANE
    19.
    发明专利
    CATALYST COMPOSITION FOR PRODUCING POLYURETHANE 失效

    公开(公告)号：JPH06179735A

    公开(公告)日：1994-06-28

    申请号：JP35449192

    申请日：1992-12-15

    Applicant: KAO CORP

    Inventor： HARADA SHOICHIRO ,  MORII MASAYOSHI ,  ISAYAMA YASUTOSHI

    IPC: C08G18/20 ,  C08G18/18 ,  C08G18/32 ,  C08G101/00

    Abstract: PURPOSE:To obtain a polyurethane excellent in thermal conductivity, friability and filling properties by reacting an organic polyisocyanate with a polyol in the presence of a specific catalyst composition and a foaming agent. CONSTITUTION:The catalyst composition is composed of 50-70wt.% 1- methylimdazole and/or 1-isobutyl-2-methylimidazole, 20-30wt.% N,N,N- trimethylaminoethylpiperazine, 5-15wt.% bis (dimethylaminoethyl) ether and 5-10wt.% formic acid. Furthermore, the objective polyurethane is obtained by reacting an organic polyisocyanate (preferably crude diphenylmethane diisocyanate, crude tolylene diisocyanate, etc.) with a polyol (preferably polyester polyols, a glycol, glycerol, etc.) in the presence of this catalyst composition and a foaming agent. Water used as the foaming agent is added in an amount of preferably 3-6 pts.wt. based on 100 pts.wt. polyol.

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