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公开(公告)号：US3607692A
公开(公告)日：1971-09-21
申请号：US3607692D
申请日：1969-09-17
Applicant: BASF AG
Inventor： SANNER AXE , KRAUCH CARL HEINRICH
IPC: D06N3/04 , C08F2/36 , C08F2/46 , C08F291/18 , C08J9/28 , D06M14/18 , B01J1/10 , B01J1/12 , C08C17/08
CPC classification number: C08J9/28 , C08F291/18 , C08J2201/0547 , D06M14/18 , Y10S428/904 , Y10S521/915
Abstract: Production of poromeric materials by impregnating flat fibrous structures with liquids containing monoolefinically unsaturated monomers and high polymeric plastics in dissolved, emulsified or dispersed form, but no polyolefinically unsaturated monomers, freezing the impregnated fibrous structures, irradiating the frozen structures to effect polymerization of the monomers, and freeing the poromeric materials from the remaining liquid. The poromeric materials may be used as floor coverings, insulating materials, leather substitutes and coating materials.
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公开(公告)号：WO1997042259A1
公开(公告)日：1997-11-13
申请号：PCT/FR1997000796
申请日：1997-05-06
Applicant: FINANCIERE ELYSEES BALZAC , CHEVALIER, Christophe , CHANZY, Henri , WERTZ, Jean-Luc
Inventor： FINANCIERE ELYSEES BALZAC
IPC: C08J09/26
CPC classification number: C08J9/26 , A47L13/16 , C08J9/0085 , C08J9/28 , C08J2201/0444 , C08J2201/0547 , C08J2301/02
Abstract: The invention discloses a method for manufacturing alveolate cellulose products (sponges, sponge-cloths...), from a cellulose raw material, which comprises: dissolving at least partially the said cellulose raw material in an intrinsic solvent; incorporating, under agitation, into the resulting mixture an effective amount of at least one pore forming agent; the said pore forming agent(s), compatible with the cellulose mixture, being suitable for generating, when their action develops, a macro- and a microporosity; gelling the consistent homogeneous mass thus obtained; treating the said gelled mass under conditions where the dissolved cellulose precipitates and the action of the pore forming agent(s) present develops. The said method is an advantageous alternative to the polluting viscose method. The products obtained have properties quite similar to those of the products obtained by the said viscose method. The said new products are part of the invention.
Abstract translation: 本发明公开了一种从纤维素原料制造蜂窝状纤维素产品（海绵，海绵布...）的方法，该方法包括：至少部分地将所述纤维素原料溶解在固有溶剂中; 在搅拌下将有效量的至少一种成孔剂并入所得混合物中; 与纤维素混合物相容的所述成孔剂适于在其作用发生时产生大孔和微孔; 凝胶化由此获得的一致均匀质量; 在溶解的纤维素沉淀条件和成孔剂的作用存在的条件下处理所述胶凝物质。 所述方法是污染粘胶法的有利替代方案。 获得的产品具有与通过所述粘胶法获得的产品非常相似的性质。 所述新产品是本发明的一部分。
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13.发明公开PRODUCTION METHOD FOR POROUS CELLULOSE BEADS AND ABSORBENT EMPLOYING SAME 有权HERSTELLUNGSVERFAHRENFÜRPORÖSECELLULOSEPERLEN UND ABSORPTIONSMITTEL DAMIT
公开(公告)号：EP3059252A4
公开(公告)日：2017-08-09
申请号：EP14853802
申请日：2014-10-14
Applicant: KANEKA CORP
Inventor： HAYASHI ASUKA , KAWAI YOSHIKAZU , MORIO KEN-ICHIRO
CPC classification number: B01J20/24 , B01J20/285 , B01J20/286 , B01J20/305 , B01J20/3085 , B01J20/3212 , B01J20/3217 , B01J20/3274 , B01J20/3293 , C07K1/145 , C07K1/22 , C07K17/12 , C08B15/10 , C08J9/16 , C08J9/28 , C08J2201/026 , C08J2201/0547 , C08J2301/00
Abstract: The objective of the present invention is to provide a method for easily and efficiently producing cellulose beads which have pore shape suitable for an adsorbent and of which adsorption performance is excellent without using highly toxic and highly corrosive auxiliary raw material and without industrially disadvantageous cumbersome step. The method for producing porous cellulose beads according to the present invention is characterized in comprising (a) the step of preparing a fine cellulose dispersion by mixing a low temperature alkaline aqueous solution and cellulose, (b) the step of preparing a mixed liquid by adding a crosslinking agent to the fine cellulose dispersion, (c) the step of preparing an emulsion by dispersing the mixed liquid in a dispersion medium, (d) the step of contacting the emulsion with a coagulating solvent.
Abstract translation: 本发明的目的在于提供一种不使用高毒性且高腐蚀性的辅助原料，且不存在工业上不利的繁琐工序，且容易且高效地制造具有适合于吸附剂的孔形状且吸附性能优异的纤维素珠粒的方法。 本发明的多孔性纤维素珠的制造方法的特征在于，包括：（a）将低温碱性水溶液与纤维素混合而制备微细纤维素分散液的工序;（b）通过添加混合液 （c）通过将该混合液分散在分散介质中来制备乳液的步骤，（d）使该乳液与凝结溶剂接触的步骤。
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公开(公告)号：EP0897411B1
公开(公告)日：2003-10-01
申请号：EP97923135.4
申请日：1997-05-06
Applicant: FINANCIERE ELYSEES BALZAC
Inventor： CHEVALIER, Christophe , CHANZY, Henri , WERTZ, Jean-Luc
CPC classification number: C08J9/26 , A47L13/16 , C08J9/0085 , C08J9/28 , C08J2201/0444 , C08J2201/0547 , C08J2301/02
Abstract: The invention discloses a method for manufacturing alveolate cellulose products (sponges, sponge-cloths...), from a cellulose raw material, which comprises: dissolving at least partially the said cellulose raw material in an intrinsic solvent; incorporating, under agitation, into the resulting mixture an effective amount of at least one pore forming agent; the said pore forming agent(s), compatible with the cellulose mixture, being suitable for generating, when their action develops, a macro- and a microporosity; gelling the consistent homogeneous mass thus obtained; treating the said gelled mass under conditions where the dissolved cellulose precipitates and the action of the pore forming agent(s) present develops. The said method is an advantageous alternative to the polluting viscose method. The products obtained have properties quite similar to those of the products obtained by the said viscose method. The said new products are part of the invention.
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公开(公告)号：JPWO2015056681A1
公开(公告)日：2017-03-09
申请号：JP2015542620
申请日：2014-10-14
Applicant: 株式会社カネカ
CPC classification number: B01J20/24 , B01J20/285 , B01J20/286 , B01J20/305 , B01J20/3085 , B01J20/3212 , B01J20/3217 , B01J20/3274 , B01J20/3293 , C07K1/145 , C07K1/22 , C07K17/12 , C08B15/10 , C08J9/16 , C08J9/28 , C08J2201/026 , C08J2201/0547 , C08J2301/00
Abstract: 本発明は、毒性・腐食性の高い副原料を使わず、工業的に不利である煩雑な工程を経ることなく簡便に、吸着体に好適な細孔形状を有する吸着性の優れたセルロースビーズを製造する方法を提供する。本発明に係る多孔質セルロースビーズの製造方法は、a)低温のアルカリ水溶液とセルロースとを混合してセルロース微分散液を作製する工程、b)前記セルロース微分散液に架橋剤を加え混合液を作製する工程、c)前記混合液を分散媒に分散させてエマルションを作製する工程、d)前記エマルションを凝固溶媒に接触させる工程を含むことを特徴とする。
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Patent Agency Ranking
公开(公告)号：WO2015142159A1
公开(公告)日：2015-09-24
申请号：PCT/MY2015/000016
申请日：2015-03-13
Applicant: UNIVERSITI KEBANGSAAN MALAYSIA
Inventor： Sarani Binti Zakaria , Chia Chin Hua , Hatika Kaco
CPC classification number: C08J9/28 , C08B16/00 , C08H8/00 , C08J5/18 , C08J9/0052 , C08J9/0071 , C08J2201/0504 , C08J2201/0547 , C08J2205/022 , C08J2301/02
Abstract: The present invention aims to provide a method for preparing a bio-based material which includes the steps of extracting celluloses from lignocellulosic biomass and regenerating a cellulose film. After that, preparing a metal-graphene oxide nano-composite and subsequently mixing the metal-graphene oxide nano-composite into the cellulose film solution to form an interaction mixture. Subsequently, the interaction mixture is coagulated in a non-solvent coagulant, and a highly porous structure of a cellulose membrane is regenerated. Particularly, the regenerated cellulose membrane has anti-bacterial properties and is tested against Gram-positive and Gram-negative bacteria.
Abstract translation: 本发明旨在提供一种制备生物基材料的方法，其包括从木质纤维素生物质中提取纤维素并再生纤维素膜的步骤。 之后，制备金属 - 石墨烯氧化物纳米复合材料，随后将金属 - 石墨烯氧化物纳米复合材料混合到纤维素膜溶液中以形成相互作用混合物。 随后，相互作用混合物在非溶剂凝结剂中凝结，再生纤维素膜的高度多孔结构。 特别地，再生纤维素膜具有抗细菌性质，并针对革兰氏阳性菌和革兰氏阴性菌进行测试。
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公开(公告)号：WO2015056681A1
公开(公告)日：2015-04-23
申请号：PCT/JP2014/077362
申请日：2014-10-14
Applicant: 株式会社カネカ
CPC classification number: B01J20/24 , B01J20/285 , B01J20/286 , B01J20/305 , B01J20/3085 , B01J20/3212 , B01J20/3217 , B01J20/3274 , B01J20/3293 , C07K1/145 , C07K1/22 , C07K17/12 , C08B15/10 , C08J9/16 , C08J9/28 , C08J2201/026 , C08J2201/0547 , C08J2301/00
Abstract: 本発明は、毒性・腐食性の高い副原料を使わず、工業的に不利である煩雑な工程を経ることなく簡便に、吸着体に好適な細孔形状を有する吸着性の優れたセルロースビーズを製造する方法を提供する。本発明に係る多孔質セルロースビーズの製造方法は、ａ）低温のアルカリ水溶液とセルロースとを混合してセルロース微分散液を作製する工程、ｂ）前記セルロース微分散液に架橋剤を加え混合液を作製する工程、ｃ）前記混合液を分散媒に分散させてエマルションを作製する工程、ｄ）前記エマルションを凝固溶媒に接触させる工程を含むことを特徴とする。
Abstract translation: 本发明提供了一种具有特殊吸附性的纤维素珠粒的制备方法，其具有适用于吸收剂的多孔形态，在不使用剧毒或腐蚀性辅助材料的情况下进行，并且不需要工业上不利的复杂工艺。 该多孔纤维素珠粒的制造方法的特征在于，包括a）将低温碱性水溶液和纤维素混合的步骤，以及制备纤维素微分散体的步骤，b）将交联剂添加到纤维素微分散体 制备混合溶液，c）将混合溶液分散在分散介质中并制备乳液的步骤，和d）使乳液与凝固介质接触的步骤。
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18.发明公开
公开(公告)号：EP3059252A1
公开(公告)日：2016-08-24
申请号：EP14853802.8
申请日：2014-10-14
Applicant: Kaneka Corporation
Inventor： HAYASHI, Asuka , KAWAI, Yoshikazu , MORIO, Ken-ichiro
CPC classification number: B01J20/24 , B01J20/285 , B01J20/286 , B01J20/305 , B01J20/3085 , B01J20/3212 , B01J20/3217 , B01J20/3274 , B01J20/3293 , C07K1/145 , C07K1/22 , C07K17/12 , C08B15/10 , C08J9/16 , C08J9/28 , C08J2201/026 , C08J2201/0547 , C08J2301/00
Abstract: The objective of the present invention is to provide a method for easily and efficiently producing cellulose beads which have pore shape suitable for an adsorbent and of which adsorption performance is excellent without using highly toxic and highly corrosive auxiliary raw material and without industrially disadvantageous cumbersome step. The method for producing porous cellulose beads according to the present invention is characterized in comprising (a) the step of preparing a fine cellulose dispersion by mixing a low temperature alkaline aqueous solution and cellulose, (b) the step of preparing a mixed liquid by adding a crosslinking agent to the fine cellulose dispersion, (c) the step of preparing an emulsion by dispersing the mixed liquid in a dispersion medium, (d) the step of contacting the emulsion with a coagulating solvent.
Abstract translation: 本发明的目的在于提供一种不使用高毒性且高腐蚀性的辅助原料，且不存在工业上不利的繁琐工序，且容易且高效地制造具有适合于吸附剂的孔形状且吸附性能优异的纤维素珠粒的方法。 本发明的多孔性纤维素珠的制造方法的特征在于，包括：（a）将低温碱性水溶液与纤维素混合而制备微细纤维素分散液的工序;（b）通过添加混合液 （c）通过将该混合液分散在分散介质中来制备乳液的步骤，（d）使该乳液与凝结溶剂接触的步骤。
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公开(公告)号：EP0897411A1
公开(公告)日：1999-02-24
申请号：EP97923135.0
申请日：1997-05-06
Applicant: FINANCIERE ELYSEES BALZAC
Inventor： CHEVALIER, Christophe , CHANZY, Henri , WERTZ, Jean-Luc
CPC classification number: C08J9/26 , A47L13/16 , C08J9/0085 , C08J9/28 , C08J2201/0444 , C08J2201/0547 , C08J2301/02
Abstract: The invention discloses a method for manufacturing alveolate cellulose products (sponges, sponge-cloths...), from a cellulose raw material, which comprises: dissolving at least partially the said cellulose raw material in an intrinsic solvent; incorporating, under agitation, into the resulting mixture an effective amount of at least one pore forming agent; the said pore forming agent(s), compatible with the cellulose mixture, being suitable for generating, when their action develops, a macro- and a microporosity; gelling the consistent homogeneous mass thus obtained; treating the said gelled mass under conditions where the dissolved cellulose precipitates and the action of the pore forming agent(s) present develops. The said method is an advantageous alternative to the polluting viscose method. The products obtained have properties quite similar to those of the products obtained by the said viscose method. The said new products are part of the invention.
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公开(公告)号：EP0303259A3
公开(公告)日：1990-08-01
申请号：EP88113022.3
申请日：1988-08-10
Applicant: Asahi Kasei Kogyo Kabushiki Kaisha
Inventor： Shirokaze, Junichi
CPC classification number: C08J3/14 , C08J9/28 , C08J2201/0482 , C08J2201/0484 , C08J2201/0547 , C08J2301/02
Abstract: A multi-cellular cellulose particle having a multiplicity of cells spaced from one another by cell membranes is described, which cells have a maximum inscribed sphere diameter of larger than 2 µm. The cells have a continuous hole structure in which cells the cells communicate with one another through openings in the membranes separating two adjacent cells. The multi-cellular cellulose particle is prepared by forming drops of a solution of cellulose or a cellulose derivative, cooling the drops at a temperature lower than the solidification temperature of the solution to freeze the drops, and removing the solvent by extraction or nullifying the dissolving power of the solvent.
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