公开(公告)号：KR1020100074754A

公开(公告)日：2010-07-02

申请号：KR1020080133267

申请日：2008-12-24

Applicant: 전북대학교산학협력단

Inventor： 손인진 ,  고인용 ,  이동목 ,  윤진국 ,  박나라

IPC: C04B35/58 ,  C04B35/565 ,  H01L21/24

CPC classification number: C04B35/58085 ,  C04B35/565 ,  C04B35/584 ,  C04B35/62615 ,  C04B2235/5454 ,  C04B2235/604 ,  C04B2235/6581 ,  C04B2235/666

Abstract: PURPOSE: A producing method of a metal silicide-silicon carbide-silicon nitride composite material is provided to produce the composite material within two minutes by a single process of indirect heating using an induced current. CONSTITUTION: A producing method of a metal silicide-silicon carbide-silicon nitride composite material comprises the following steps: nano-confricating a mixture of metal carbide, metal-nitride, and silicon powder; synthesizing the metal silicide-silicon carbide-silicon nitride composite material by adding the heat generated from an induced current and a pressure to the mixture; removing the pressure and the induced current from the synthesized metal silicide-silicon carbide-silicon nitride composite material; and cooling the metal silicide-silicon carbide-silicon nitride composite material.

Abstract translation: 目的：提供金属硅化物 - 碳化硅 - 氮化硅复合材料的制造方法，通过使用感应电流的单次间接加热工艺在两分钟内生产复合材料。 构成：金属硅化物 - 碳化硅 - 氮化硅复合材料的制造方法包括以下步骤：将金属碳化物，金属氮化物和硅粉末的混合物纳米化; 通过将从感应电流和压力产生的热量加入到混合物中来合成金属硅化物 - 碳化硅 - 氮化硅复合材料; 从合成的金属硅化物 - 碳化硅 - 氮化硅复合材料中去除压力和感应电流; 并冷却金属硅化物 - 碳化硅 - 氮化硅复合材料。

公开(公告)号：KR1020100024213A

公开(公告)日：2010-03-05

申请号：KR1020080082968

申请日：2008-08-25

Applicant: 전북대학교산학협력단

Inventor： 손인진 ,  우기도 ,  김병량 ,  문민석 ,  박정환

IPC: B82B3/00 ,  B82B1/00 ,  B82Y40/00

CPC classification number: C01B32/90 ,  B82Y30/00 ,  B82Y40/00 ,  C01P2004/64

Abstract: PURPOSE: A manufacturing method of a nano structure metal carbide and the and nano structure metal carbide manufactured from thereof are provided to perform a pressing molding and a sintering operation at high temperature in several minutes by heating nano powder with a heat generated from an inducing current or an impulse current. CONSTITUTION: A manufacturing method of a nano structure metal carbide comprises the following steps: nano pulverizing the metal carbide powder to make a nano particle size by ball milling; pressing molding and sintering the powder from the nano pulverizing step while heating the powder with a heat generated from an electric current; and cooling the pressing molded and sintered nano structure at room temperature when the contraction length does not change by blocking the electric current. The metal carbide powder is selected from the group consisting of titanium carbide, tungsten carbide, silicon carbide, tantalium carbide, vanadium carbide, and niobium carbide.

Abstract translation: 目的：提供纳米结构金属碳化物的制造方法和由其制造的纳米结构金属碳化物，以在几分钟内通过用感应电流产生的热量加热纳米粉末进行压制成型和烧结操作 或脉冲电流。 构成：纳米结构金属碳化物的制造方法包括以下步骤：通过球磨将纳米粉碎金属碳化物粉末制成纳米粒度; 在从电流产生的热量加热粉末的同时，从纳米粉碎步骤中压制和烧结粉末; 并且当收缩长度不通过阻断电流而改变时，在室温下冷却压制和烧结的纳米结构。 金属碳化物粉末选自碳化钛，碳化钨，碳化硅，碳化钽，碳化钒和碳化铌。

公开(公告)号：KR100810048B1

公开(公告)日：2008-03-05

申请号：KR1020060090703

申请日：2006-09-19

Applicant: 전북대학교산학협력단

Inventor： 손인진 ,  윤진국 ,  홍경태 ,  박현국 ,  김동기

IPC: C04B35/569 ,  C04B35/14 ,  B82Y40/00 ,  B82Y30/00

CPC classification number: C04B35/58085 ,  C04B35/565 ,  C04B35/62615 ,  C04B2235/3843 ,  C04B2235/428 ,  C04B2235/5454 ,  C04B2235/666 ,  C04B2235/781

Abstract: A method for preparing metal silicide-SiC composites is provided to produce nano-size metal silicide-SiC composites having excellent oxidation resistance and mechanical properties within a short time. A method for preparing metal silicide-SiC composites includes the steps of: pulverizing a mixture of a metal carbide and a silicon powder into nanopowder by a planetary ball milling method; applying pressure and heat to the nano-powdered mixture to synthesize a metal silicide-SiC composite, wherein the heat is generated by an induced current; removing the pressure and induced current from the synthesized metal silicide-SiC composite; and cooling the metal silicide-SiC composite. Further, the metal carbide is at least one selected from a group consisting of TiC, MO2C, VC, TaC, NbC, WC, or ZrC.

Abstract translation: 提供了一种制备金属硅化物-SiC复合材料的方法，以在短时间内制备具有优异抗氧化性和机械性能的纳米尺寸金属硅化物 - SiC复合材料。 制备金属硅化物-SiC复合材料的方法包括以下步骤：通过行星球磨法将金属碳化物和硅粉末的混合物粉碎成纳米粉末; 向纳米粉末混合物施加压力和热量以合成金属硅化物-SiC复合材料，其中热量由感应电流产生; 从合成的金属硅化物 - SiC复合材料中去除压力和感应电流; 并冷却金属硅化物 - SiC复合材料。 此外，金属碳化物为选自TiC，MO2C，VC，TaC，NbC，WC或ZrC中的至少一种。