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    METHOD OF OBTAINING DISSYMMETRICALLY SUBSTITUTED TRIAZINES
    21.
    发明专利
    METHOD OF OBTAINING DISSYMMETRICALLY SUBSTITUTED TRIAZINES 未知

    公开(公告)号：PL178167B1

    公开(公告)日：2000-03-31

    申请号：PL31403594

    申请日：1994-10-10

    Applicant: BASF AG

    Inventor： SCHAEFER BERND ,  MAYER HORST

    IPC: C07D251/46 ,  B01J27/122 ,  B01J27/138 ,  B01J31/04 ,  B01J31/22 ,  C07D251/16

    Abstract: PCT No. PCT/EP94/03331 Sec. 371 Date Mar. 29, 1996 Sec. 102(e) Date Mar. 29, 1996 PCT Filed Oct. 10, 1994 PCT Pub. No. WO95/11237 PCT Pub. Date Apr. 27, 1995A process for preparing asymmetrically substituted triazines of the formula I I where R1 is hydrogen, methyl or ethyl, R2 and R3 independently of one another are an unsubstituted or substituted hydrocarbon radical, by reaction of a cyanoguanidine of the formula II II with a carboxylic acid derivative in the presence of an alcohol of the formula III R2-OHIII,which comprises reacting a carboxylic acid ester of the formula IV R3-COOR4IV,where R3 has the abovementioned meaning and R4 is an unsubstituted or substituted hydrocarbon radical, in the presence of a base or of a carboxamide selected from the group consisting of N,N-dialkylformamide, N,N-dialkylacetamide and N-methylpyrrolidone and in the presence of a salt or of a salt-like compound of the elements magnesium, calcium, aluminum, zinc, copper, iron, cobalt, nickel or chromium, is described.

    Herbicidal mixtures having a synergistic effect
    22.
    发明专利
    Herbicidal mixtures having a synergistic effect 未知

    公开(公告)号：AU710367B2

    公开(公告)日：1999-09-16

    申请号：AU7128196

    申请日：1996-09-12

    Applicant: BASF AG

    Inventor： LANDES MAX ,  SIEVERNICH BERND ,  KIBLER ELMAR ,  NUYKEN WESSEL ,  WALTER HELMUT ,  WESTPHALEN KARL-OTTO ,  MAYER HORST ,  HADEN EGON ,  MULDER CHRISTIAAN ,  SCHONHAMMER ALFONS ,  HAMPRECHT GERHARD

    IPC: A01N47/36

    Abstract: Herbicidal mixt. comprises: (a) at least one fluoro-substd. sulphonyl urea derivs. of formula (I) or their salts; and (b) at least one herbicide in a synergistic amt. selected from e.g. buthidazole or cyprazole; allidochlor (CDDA), benzoylprop-ethyl, bromobutide, chlorthiamid, dimepiperate, dimethenamid, diphenamid, etobenzanid (benzchlomet), flampropmethyl, fosamin, isoxaben, monalide, naptalame, pronamid (propyzamid) or propanil; bilanafos (bialophos), buminafos, glufosinate ammonium, glyphospate or sulfosate; amitrole, anilofos or mefenacet; 2,4-D, 2,4-DB, clomeprop, dichlorprop, dichlorprop-P, dichlorprop-P (2,4-DP-P), fenoprop (2,4,5-TP, fluoroxypyr, MCPA, MCPB, mecoprop, mecoprop-P, napropamide, napropanilide or triclopyr, or salts of these. Z = N or CH; R1 = 1-6C alkyl opt. substd. by 1-5 OMe, OEt, SO2Me; CN; Cl; F; SMe; or S(O)Me; halo; ER6; COOR8; NO2; S(O)oR9, SO2NR10R11,; or CONR10R11; E = O; S or NR7; R2 = H; 1-4C alkyl or 1-4C alkoxy opt. substd. by halo; 2-4C alkenyl; 2-4C alkynyl; halo; SO2Me; SO2Et; NO2; CN; or 1-4C alkylthio; R3 = F, CF3; CF2Cl; CF2H; OCF3; OCF2Cl; Cl (when R1 - CO2Me and R2 = F); Me (when R1 = CH2CF3 or CF2CF3); or OCF2H or OCF2Br (when R4 =- OCF3 or OCF2Cl); R4 = OMe; OEt; Me or Et opt. substd. by halo; SMe; SEt; NHMe; NHEt; N(1-2C alkyl)2; or halo; R5 = H, OMe; OEt; or 1-4C alkyl; R6 = 1-4C alkyl, 2-4C alkenyl, 2-4C alkynyl or 3-6C cycloalkyl opt. substd by 1-5 halo (except allyl, OCH2F, OCF2Cl or 2-Cl-Et) when E = O or S; or SO2Me, SO2Et, SO2CF3, SO2-allyl or SO2-propargyl when E = O or NR7; R7 = H; Me; or Et; R8 = 1-6C alkyl opt. mono-, di- or trisubstd. by halo, 1-4C alkoxy, 1-4C alkylthio, 1-4C haloalkoxy, 1-4C alkoxy-1-2C alkoxy, 3-7C cycloalkyl and/or Ph; 5-7C cycloalkyl opt. mono-, di- or trisubstd. by 1-4C alkyl; 3-6C alkenyl; or 3-6C alkynyl; R10 = H; OMe; OEt; or 1-6C alkyl; and R11 = 1-4C alkyl opt. substd by 1-4 halo or 1-4C alkoxy; or 3-6C cycloalkyl; or R10+R11 = 4-6C alkylene with 1 CH2 opt. replaced by O or 1-4C alkylimino; n = 0-3; and o = 1-2.

    23.
    发明专利
    未知

    公开(公告)号：BR9610586A

    公开(公告)日：1999-07-06

    申请号：BR9610586

    申请日：1996-09-12

    Applicant: BASF AG

    Inventor： LANDES MAX ,  SIEVERNICH BERND ,  KIBLER ELMAR ,  NUYKEN WESSEL ,  WALTER HELMUT ,  WESTPHALEN KARL OTTO ,  MAYER HORST ,  HADEN EGON ,  MULDER CHRISTIAAN ,  SCHOENHAMMER ALFONS ,  HAMPRECHT GERHARD

    IPC: A01N47/36

    Abstract: Herbicidal mixt. comprises: (a) at least one fluoro-substd. sulphonyl urea derivs. of formula (I) or their salts; and (b) at least one herbicide in a synergistic amt. selected from e.g. buthidazole or cyprazole; allidochlor (CDDA), benzoylprop-ethyl, bromobutide, chlorthiamid, dimepiperate, dimethenamid, diphenamid, etobenzanid (benzchlomet), flampropmethyl, fosamin, isoxaben, monalide, naptalame, pronamid (propyzamid) or propanil; bilanafos (bialophos), buminafos, glufosinate ammonium, glyphospate or sulfosate; amitrole, anilofos or mefenacet; 2,4-D, 2,4-DB, clomeprop, dichlorprop, dichlorprop-P, dichlorprop-P (2,4-DP-P), fenoprop (2,4,5-TP, fluoroxypyr, MCPA, MCPB, mecoprop, mecoprop-P, napropamide, napropanilide or triclopyr, or salts of these. Z = N or CH; R1 = 1-6C alkyl opt. substd. by 1-5 OMe, OEt, SO2Me; CN; Cl; F; SMe; or S(O)Me; halo; ER6; COOR8; NO2; S(O)oR9, SO2NR10R11,; or CONR10R11; E = O; S or NR7; R2 = H; 1-4C alkyl or 1-4C alkoxy opt. substd. by halo; 2-4C alkenyl; 2-4C alkynyl; halo; SO2Me; SO2Et; NO2; CN; or 1-4C alkylthio; R3 = F, CF3; CF2Cl; CF2H; OCF3; OCF2Cl; Cl (when R1 - CO2Me and R2 = F); Me (when R1 = CH2CF3 or CF2CF3); or OCF2H or OCF2Br (when R4 =- OCF3 or OCF2Cl); R4 = OMe; OEt; Me or Et opt. substd. by halo; SMe; SEt; NHMe; NHEt; N(1-2C alkyl)2; or halo; R5 = H, OMe; OEt; or 1-4C alkyl; R6 = 1-4C alkyl, 2-4C alkenyl, 2-4C alkynyl or 3-6C cycloalkyl opt. substd by 1-5 halo (except allyl, OCH2F, OCF2Cl or 2-Cl-Et) when E = O or S; or SO2Me, SO2Et, SO2CF3, SO2-allyl or SO2-propargyl when E = O or NR7; R7 = H; Me; or Et; R8 = 1-6C alkyl opt. mono-, di- or trisubstd. by halo, 1-4C alkoxy, 1-4C alkylthio, 1-4C haloalkoxy, 1-4C alkoxy-1-2C alkoxy, 3-7C cycloalkyl and/or Ph; 5-7C cycloalkyl opt. mono-, di- or trisubstd. by 1-4C alkyl; 3-6C alkenyl; or 3-6C alkynyl; R10 = H; OMe; OEt; or 1-6C alkyl; and R11 = 1-4C alkyl opt. substd by 1-4 halo or 1-4C alkoxy; or 3-6C cycloalkyl; or R10+R11 = 4-6C alkylene with 1 CH2 opt. replaced by O or 1-4C alkylimino; n = 0-3; and o = 1-2.

    HERBICIDE MIXTURE WITH SYNERGIC EFFECT
    27.
    发明专利
    HERBICIDE MIXTURE WITH SYNERGIC EFFECT 未知

    公开(公告)号：BG102340A

    公开(公告)日：1998-08-31

    申请号：BG10234098

    申请日：1998-03-20

    Applicant: BASF AG

    Inventor： LANDES MAX ,  SIEVERNICH BERND ,  KIBLER ELMAR ,  NUYKEN WESSEL ,  WALTER HELMUT ,  WESIPHALEN KARL-OTTO ,  MAYER HORST ,  HADEN EGON ,  MULDER CHRISTIAAN ,  SCHOENHAMMER ALFONS ,  HAMPRECHT GERHARD

    IPC: A01N47/36

    Abstract: The invention relates to herbicide mixture containing atleast one derivative of sulphonurea having the formulawhere R1 is C1-C5 alkyl, methoxy, ethoxy, SO2CH3, cyano, chloro,fluoro, SCH3, S(0)CH3, halogen, ER6 group where E means 0, S orNR7, COOR8, NO2, S(0)oR9, SO2NR1OR11, CONR1OR11; R2 is hydrogen,C1-C4 alkyl, C2-C4 alkeynyl, halogen, C1-C4 alkoxy, C1-C4halogenalkoxy, C1-C4 halogenalkyl, C1-C2 alkylsulphonyl group,nitro, cyano or C1-C4 alkylthio; R3 means R, CF3, CF2Cl, CF2H,OCF3, OCF2Cl, or provided that R1 is CO2CH3 and simultaneously R2is fluoro, Cl, or provided that R1 is CH2CF3 or CF2CF3, it meansmethyl, or when R4 is OCF3 or OCF2Cl it means OCF2H or OCF2Br; R4is C1-C2 alkoxy, C1-C2 alkyl, C1-C2 alkylthio, C1-C2 alkylamino,Di-C1-C2 alkylamino, halogen, C1-C2 halogenalkyl, C1-C2halogenalkoxy; R5 is hydrogen, C1-C2 alkoxy, C1-C4 alkyl, R6 isC1-C4 alkyl, C2-C4 alkenyl, C2-C4 alkynyl or C3-C6 cycloalkylwhich can have 1 to 5 halogen atoms with the exception of alyl,difluoromethoxy, chlorodifluoromethoxy and 2-chloroethoxy,provided that E means 0 or S, and when E is 0 or NR7, R6 alsomeans methylsulphonyl, ethylsulphonyl, trifluoromethylsulphonyl,alylsulphonyl, propargylsulphonyl or dimethyl sulphamoyl; R7 ishydrogen, methyl or ethyl; R8 is C1-C6 alkyl group which can haveup to three of the following residues: halogen, C1-C4 alkoxy,C1-C4 alkylthio, C1-C4 halogenalkoxy, C1-C4 alkoxy-C1-C2-alkoxy,C3-C7 cycloalkyl and/or phenyl, C5-C7 cycloalkyl group which hasup to three C1-C4 alkyl grlups, C3-C6 alkenyl or C3-C6 alkynyl; R9is C1-C6 alkyl group substituted with halogen, C1-C4 alkoxy, C-C4alkylthio, C1-C4 halogenalkoxy, C1-C4-alkoxy-C1-C2-alkoxy, C3-C7cycloalkyl and/or phenyl, C5-C7 cycloalkyl group with one to threeC1-C4 alkyl groups, C2-C6 alkenyl group or C3-C6 alkynyl group;R10 is hydrogen, C1-C2 alkoxygroup, C1-C6 alkyl group or togetherwith R11 it means C4-C6 alkylene chain where one methylene groupcan be substituted with oxygen atom or with C1-C4 alkylaminogroup, R11 is C1-C4 alkyl group with one to four halogen or C1-C4alkyoxyresidues, C3-C6 cycloalkyl, n is from 0 to 3, 0 is 1-2, Zis N, CH. The invention also relates to salts of the compound.13 claims

    29.
    发明专利
    未知

    公开(公告)号：NO981240D0

    公开(公告)日：1998-03-19

    申请号：NO981240

    申请日：1998-03-19

    Applicant: BASF AG

    Inventor： LANDES MAX ,  SIEVERNICH BERND ,  KIBLER ELMAR ,  NUYKEN WESSEL ,  WALTER HELMUT ,  WESTPHALEN KARL-OTTO ,  MAYER HORST ,  HADEN EGON ,  MULDER CHRISTIAAN ,  SCHOENHAMMER ALFONS ,  HAMPRECHT GERHARD

    IPC: A01N47/36

    Abstract: Herbicidal mixt. comprises: (a) at least one fluoro-substd. sulphonyl urea derivs. of formula (I) or their salts; and (b) at least one herbicide in a synergistic amt. selected from e.g. buthidazole or cyprazole; allidochlor (CDDA), benzoylprop-ethyl, bromobutide, chlorthiamid, dimepiperate, dimethenamid, diphenamid, etobenzanid (benzchlomet), flampropmethyl, fosamin, isoxaben, monalide, naptalame, pronamid (propyzamid) or propanil; bilanafos (bialophos), buminafos, glufosinate ammonium, glyphospate or sulfosate; amitrole, anilofos or mefenacet; 2,4-D, 2,4-DB, clomeprop, dichlorprop, dichlorprop-P, dichlorprop-P (2,4-DP-P), fenoprop (2,4,5-TP, fluoroxypyr, MCPA, MCPB, mecoprop, mecoprop-P, napropamide, napropanilide or triclopyr, or salts of these. Z = N or CH; R1 = 1-6C alkyl opt. substd. by 1-5 OMe, OEt, SO2Me; CN; Cl; F; SMe; or S(O)Me; halo; ER6; COOR8; NO2; S(O)oR9, SO2NR10R11,; or CONR10R11; E = O; S or NR7; R2 = H; 1-4C alkyl or 1-4C alkoxy opt. substd. by halo; 2-4C alkenyl; 2-4C alkynyl; halo; SO2Me; SO2Et; NO2; CN; or 1-4C alkylthio; R3 = F, CF3; CF2Cl; CF2H; OCF3; OCF2Cl; Cl (when R1 - CO2Me and R2 = F); Me (when R1 = CH2CF3 or CF2CF3); or OCF2H or OCF2Br (when R4 =- OCF3 or OCF2Cl); R4 = OMe; OEt; Me or Et opt. substd. by halo; SMe; SEt; NHMe; NHEt; N(1-2C alkyl)2; or halo; R5 = H, OMe; OEt; or 1-4C alkyl; R6 = 1-4C alkyl, 2-4C alkenyl, 2-4C alkynyl or 3-6C cycloalkyl opt. substd by 1-5 halo (except allyl, OCH2F, OCF2Cl or 2-Cl-Et) when E = O or S; or SO2Me, SO2Et, SO2CF3, SO2-allyl or SO2-propargyl when E = O or NR7; R7 = H; Me; or Et; R8 = 1-6C alkyl opt. mono-, di- or trisubstd. by halo, 1-4C alkoxy, 1-4C alkylthio, 1-4C haloalkoxy, 1-4C alkoxy-1-2C alkoxy, 3-7C cycloalkyl and/or Ph; 5-7C cycloalkyl opt. mono-, di- or trisubstd. by 1-4C alkyl; 3-6C alkenyl; or 3-6C alkynyl; R10 = H; OMe; OEt; or 1-6C alkyl; and R11 = 1-4C alkyl opt. substd by 1-4 halo or 1-4C alkoxy; or 3-6C cycloalkyl; or R10+R11 = 4-6C alkylene with 1 CH2 opt. replaced by O or 1-4C alkylimino; n = 0-3; and o = 1-2.

    30.
    发明专利
    未知

    公开(公告)号：DE59404115D1

    公开(公告)日：1997-10-23

    申请号：DE59404115

    申请日：1994-10-10

    Applicant: BASF AG

    Inventor： SCHAEFER BERND ,  MAYER HORST

    IPC: C07D251/46 ,  B01J27/122 ,  B01J27/138 ,  B01J31/04 ,  B01J31/22 ,  C07D251/16

    Abstract: PCT No. PCT/EP94/03331 Sec. 371 Date Mar. 29, 1996 Sec. 102(e) Date Mar. 29, 1996 PCT Filed Oct. 10, 1994 PCT Pub. No. WO95/11237 PCT Pub. Date Apr. 27, 1995A process for preparing asymmetrically substituted triazines of the formula I I where R1 is hydrogen, methyl or ethyl, R2 and R3 independently of one another are an unsubstituted or substituted hydrocarbon radical, by reaction of a cyanoguanidine of the formula II II with a carboxylic acid derivative in the presence of an alcohol of the formula III R2-OHIII,which comprises reacting a carboxylic acid ester of the formula IV R3-COOR4IV,where R3 has the abovementioned meaning and R4 is an unsubstituted or substituted hydrocarbon radical, in the presence of a base or of a carboxamide selected from the group consisting of N,N-dialkylformamide, N,N-dialkylacetamide and N-methylpyrrolidone and in the presence of a salt or of a salt-like compound of the elements magnesium, calcium, aluminum, zinc, copper, iron, cobalt, nickel or chromium, is described.

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