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    DICARBOXIMIDE AND HERBICIDE CONTAINING THE SAME
    4.
    发明专利
    DICARBOXIMIDE AND HERBICIDE CONTAINING THE SAME 失效

    公开(公告)号：JP2000297087A

    公开(公告)日：2000-10-24

    申请号：JP2000083348

    申请日：2000-03-24

    Applicant: BASF AG

    Inventor： MUENSTER PETER ,  FREUND WOLFGANG ,  STEINER GERD ,  WALTER HELMUT DR ,  WESTPHALEN KARL-OTTO ,  GERBER MATTHIAS

    IPC: A01N43/36 ,  A01N43/90 ,  C07D307/68 ,  C07D333/38 ,  C07D333/40 ,  C07D409/04 ,  C07D409/12 ,  C07D491/04 ,  C07D491/048 ,  C07D495/04

    Abstract: PROBLEM TO BE SOLVED: To obtain a new compound having herbicidal property and useful as an active ingredient of a herbicide preferably in the form of solution capable of directly scattering, emulsion, paste, oil dispersion, etc. SOLUTION: This compound is shown by formula I [X is O or S; R1 is H, hydroxyl, a 1-6C (substituted)alkyl or the like; R2 and R3 are each nitro, cyano, a halogen, H or the like; but in the case where X is O and R2 and R3 are each phenyl, R1 is not phenyl or H and all of R1 to R3 are not methyl or the like], for example N-isopropylthiophene-3,4-carboximide. For example, a compound of the formula I can be produced by reacting (A) a carboxylic acid anhydride of formula II with (B) an amine of the formula H2N-R1 in a molar ratio of the component A to the component B ranging from 0.9 to 1.5, (C) if necessary in the presence of an acid catalyst (ex. aromatic sulfonic acid), in a solvent at 0-150 deg.C, preferably 20-100 deg.C, preferably while removing a preparing reaction water or the like.

    HERBICIDAL SULPHONYL UREAS, PROCESS AND INTERMEDIATES FOR PRODUCING THE SAME
    7.
    发明申请
    HERBICIDAL SULPHONYL UREAS, PROCESS AND INTERMEDIATES FOR PRODUCING THE SAME 审中-公开
    除草剂磺酰脲，生产方法和中间体

    公开(公告)号：WO9305048A3

    公开(公告)日：1993-05-27

    申请号：PCT/EP9201879

    申请日：1992-08-25

    Applicant: BASF AG

    Inventor： HAMPRECHT GERHARD ,  MAYER HORST ,  WESTPHALEN KARL-OTTO ,  WALTER HELMUT ,  GERBER MATTHIAS ,  KARDORFF UWE

    IPC: A01N47/36 ,  C07D239/46 ,  C07D239/47 ,  C07D239/48 ,  C07D239/52 ,  C07D521/00

    CPC classification number: C07D521/00

    Abstract: Substituted sulphonyl ureas have the general formula (I), in which n and m equal 0 or 1 and the substituents have the following meaning: R1 is hydrogen, alkyl, alkenyl or alkinyl; R2 is halogen or trifluoromethyl, when m equals 0 or, when m equals 1, R2 is alkyl, alkenyl or alkinyl, and when X stands for O or S and m equals 1, trifluoromethyl or chlorodifluoromethyl; X is O, S or N-R4, whereas R4 is hydrogen or alkyl; R3 is hydrogen, halogen, alkyl, halogenalkyl, alkoxy or halogenalkoxy; A is NO¿2?, NH2, OH, CN, SCN, S(O)oR?5, SO¿2NR?6R7, ER7¿, whereas E stands for O, S or NR9, the groups (a), (b) possibly substituted C¿1?-C4-alkyl or C2-C4-alkenyl; R?5¿ is a possibly substituted alkyl group, a possibly substituted cycloalkyl group, an alkenyl group or an alkinyl group; R6 is hydrogen, an alkoxy group, an alkyl group, or represents together with R7 a C4-C6-alkylene chain, wherein a methylene group may be substituted by an oxygen atom or a C1-C4-alkylimino group; R7 is a possibly substituted alkyl, alkenyl or alkinyl group, a cycloalkyl group and may also represent, when E = NR9, methyl sulphone, trifluoromethyl sulphone, ethylsulphone, possibly halogen-substituted acetyl, dimethylcarbamoyl, dimethylsulphamoyl; o equals 0, 1 or 2; p, q equal 0 and/or 1 (when p = 0, q = 0); R8 is hydrogen or halogen; R9 is hydrogen, methyl, ethyl; R10 is alkyl, halogenalkyl, alkoxyalkyl, alkenyl, cycloalkyl, halogenalkenyl or, when p = 1 and q = 0, it may also be alkylamino or dialkylamino. Also disclosed are their environmentally compatible salts, a process and intermediates for producing the compounds having the formula (I) and their use as herbicides.

    Abstract translation: 取代的磺酰脲具有通式（I），其中n和m等于0或1，并且取代基具有以下含义：R 1是氢，烷基，烯基或炔基; 当m等于0或当m等于1时，R2是烷基，链烯基或炔基，并且当X代表O或S并且m等于1时，R2是卤素或三氟甲基; X是O，S或N-R4，而R4是氢或烷基; R3是氢，卤素，烷基，卤代烷基，烷氧基或卤代烷氧基; （a），（b）和（b）中，A代表O和S; NR代表O，S或NR 9; A代表O和S; NR 2代表NH 2，OH，CN，SCN，S（O）OR 5，SO＆ ）可能被取代的C 1 -C 4烷基或C 2 -C 4链烯基; 的R 5＆iquest？; 是可能被取代的烷基，可能被取代的环烷基，链烯基或炔基; R6是氢，烷氧基，烷基，或者与R7一起代表C4-C6-亚烷基链，其中亚甲基可以被氧原子或C1-C4-烷基亚氨基取代; 当E = NR9时，R7是可能被取代的烷基，烯基或炔基，环烷基并且还可以表示甲基砜，三氟甲基砜，乙基砜，可能被卤素取代的乙酰基，二甲基氨基甲酰基，二甲基氨磺酰基; o等于0,1或2; p，q等于0和/或1（当p = 0时，q = 0）; R8是氢或卤素; R9是氢，甲基，乙基; R10是烷基，卤代烷基，烷氧基烷基，链烯基，环烷基，卤代链烯基或当p = 1和q = 0时，它也可以是烷基氨基或二烷基氨基。 还公开了它们的环境相容性盐，用于制备具有式（I）的化合物的方法和中间体以及它们作为除草剂的用途。

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