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    VERFAHREN ZUR HERSTELLUNG VON POLYETHEROLEN
    22.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON POLYETHEROLEN 审中-公开

    公开(公告)号：EP1539855A1

    公开(公告)日：2005-06-15

    申请号：EP03748004.3

    申请日：2003-09-11

    Applicant: BASF AKTIENGESELLSCHAFT

    Inventor： BOHRES, Edward ,  HIBST, Hartmut ,  STÖSSER, Michael ,  RUPPEL, Raimund ,  BAUM, Eva

    IPC: C08G65/26

    CPC classification number: C08G65/2645 ,  C08G65/266

    Abstract: The invention relates to a method for the production of a polyetherol, wherein at least one alkylene oxide is reacted with at least one starter compound in the presence of one catalyst of general formula (I): M1p[M2qOn(OH)2(3-n)]x, The invention also relates to polyetherols produced according one inventive method and the use thereof for polyurethane synthesis, as a fuel additive or as a surfactant.

    Abstract translation: 本发明涉及一种生产聚醚醇的方法，其中至少一种烯化氧在至少一种通式（I）的催化剂存在下与至少一种起始化合物反应：M1p [M2qOn（OH）2（3- 本发明还涉及根据一种发明方法生产的聚醚醇及其在聚氨酯合成中的用途，作为燃料添加剂或作为表面活性剂。

    MULTIMETALLCYANID-KATALYSATOREN
    24.
    发明公开
    MULTIMETALLCYANID-KATALYSATOREN 有权
    用于生产聚醚多元醇使用结晶多金属氰化物催化剂

    公开(公告)号：EP1185367A1

    公开(公告)日：2002-03-13

    申请号：EP00935078.6

    申请日：2000-05-19

    Applicant: BASF AKTIENGESELLSCHAFT

    Inventor： GROSCH, Georg, Heinrich ,  HARRE, Kathrin ,  ERBES, Jörg ,  LORENZ, Reinhard ,  BAUER, Stephan ,  OSTROWSKI, Thomas ,  BAUM, Eva ,  JUNGE, Dieter

    IPC: B01J27/26 ,  C08G65/10

    CPC classification number: C08G65/2663 ,  B01J27/26

    Abstract: The invention relates to multi-metal cyanide compounds of the general formula (I). In said formula: M1 represents at least one metal ion, selected from the group containing Zn?2+, Fe2+, Co3+, Ni2+, Mn2+, Pb2+, Fe3+, Mo4+, Mo6+, Al3+, V5+, Sr2+, W4+, W6+, Cu2+, Cr2+, Cr3+, Cd2+, Hg2+, Pd2+, Pt2+, V2+, Mg2+, Ca2+, Ba2+; M2¿ represents at least one metal ion, selected from the group containing Fe?2+, Fe3+, Co3+, Cr3+, Mn2+, Mn3+, Rh3+, Ru2+, Ru3+, V4+, V5+, Co2+, Ir3+ and Cr2+ and M2¿ is different from M1; X represents at least one anion, selected from the group containing halide, hydroxide, sulphate, carbonate, cyanide, thiocyanate, isocyanate, carboxylate, in particular, formiate, acetate, propionate, oxalate, nitrate; A represents at least one anion, selected from the group containing halide, hydroxide, sulphate, carbonate, cyanate, thiocyanate, isocyanate, carboxylate or nitrate, in particular, cyanide; a, b, c and d are whole or fractional numbers which are selected in such a way, that the electroneutrality of the cyanide compound is guaranteed, whereby a, b and d are greater than zero and c is greater than or equal to zero; e is a whole or fractional number greater than zero and h is a whole or fractional number greater than or equal to zero; and f and g are whole or fractional numbers which are selected in such a way that the electroneutrality of M1fXg is guaranteed.

    PROCESS FOR PREPARING REACTIVE POLYETHER POLYOLS HAVING AN ETHYLENE OXIDE END BLOCK
    25.
    发明授权
    PROCESS FOR PREPARING REACTIVE POLYETHER POLYOLS HAVING AN ETHYLENE OXIDE END BLOCK 有权
    用于生产环氧乙烷末端块活性聚醚多元醇

    公开(公告)号：EP1753802B1

    公开(公告)日：2008-01-23

    申请号：EP05744275.8

    申请日：2005-04-21

    Applicant: BASF Aktiengesellschaft

    Inventor： OSTROWSKI, Thomas ,  RUPPEL, Raimund ,  HÖPPNER, Gerd ,  BERGMANN, Sascha ,  VANDEWALLE, Koen ,  BAUM, Eva

    IPC: C08G65/26 ,  C08G18/48

    CPC classification number: C08G65/2696 ,  C08G18/4841 ,  C08G18/4866 ,  C08G65/2663

    Abstract: Process for preparing polyether polyols having an end block of ethylene oxide by addition of alkylene oxides onto H-functional starter substances, in which A) a polyether polyol precursor is prepared by means of double metal cyanide (DMC) catalysis in a semicontinuous mode of operation in which previously prepared polyether polyol together with the DMC catalyst are placed in a reactor and H-functional starter substance and propylene oxide are added continuously; B) the polyether polyol precursor from stage A) is reacted with propylene oxide or an ethylene oxide/propylene oxide mixture in the presence of the DMC catalyst in a continuously operating reactor to give a polyether polyol intermediate; C) the intermediate from stage B) is mixed with an alkali metal hydroxide as catalyst and D) reacted with ethylene oxide in a continuously operating reactor to give the final product; E) the catalyst is separated off from the final product obtained in stage D).

    PROCESS FOR PREPARING REACTIVE POLYETHER POLYOLS HAVING AN ETHYLENE OXIDE END BLOCK
    26.
    发明公开
    PROCESS FOR PREPARING REACTIVE POLYETHER POLYOLS HAVING AN ETHYLENE OXIDE END BLOCK 有权
    用于生产环氧乙烷末端块活性聚醚多元醇

    公开(公告)号：EP1753802A1

    公开(公告)日：2007-02-21

    申请号：EP05744275.8

    申请日：2005-04-21

    Applicant: BASF Aktiengesellschaft

    Inventor： OSTROWSKI, Thomas ,  RUPPEL, Raimund ,  HÖPPNER, Gerd ,  BERGMANN, Sascha ,  VANDEWALLE, Koen ,  BAUM, Eva

    IPC: C08G65/26 ,  C08G18/48

    CPC classification number: C08G65/2696 ,  C08G18/4841 ,  C08G18/4866 ,  C08G65/2663

    Abstract: Process for preparing polyether polyols having an end block of ethylene oxide by addition of alkylene oxides onto H-functional starter substances, in which A) a polyether polyol precursor is prepared by means of double metal cyanide (DMC) catalysis in a semicontinuous mode of operation in which previously prepared polyether polyol together with the DMC catalyst are placed in a reactor and H-functional starter substance and propylene oxide are added continuously; B) the polyether polyol precursor from stage A) is reacted with propylene oxide or an ethylene oxide/propylene oxide mixture in the presence of the DMC catalyst in a continuously operating reactor to give a polyether polyol intermediate; C) the intermediate from stage B) is mixed with an alkali metal hydroxide as catalyst and D) reacted with ethylene oxide in a continuously operating reactor to give the final product; E) the catalyst is separated off from the final product obtained in stage D).

    VERFAHREN ZUR HERSTELLUNG VON POLYETHERALKOHOLEN
    27.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON POLYETHERALKOHOLEN 有权

    公开(公告)号：EP1516007A1

    公开(公告)日：2005-03-23

    申请号：EP03740194.0

    申请日：2003-06-06

    Applicant: BASF AKTIENGESELLSCHAFT

    Inventor： RUPPEL, Raimund ,  BAUM, Eva ,  WINKLER, Jürgen ,  BOHRES, Edward

    IPC: C08G65/26

    CPC classification number: C08G65/2663 ,  C08G65/2648 ,  C08G65/2696

    Abstract: The invention relates to a method for producing polyether alcohols, comprising the following steps: a) reacting a low-molecular alcohol with alkylene oxide in the presence of a basic catalyst in order to form an alkylene oxide addition product having a molecular weight ranging from 200 to 900 g/mol; b) separating the basic catalyst from the product obtained in step a), and; c) reacting the product obtained in step b) with another alkylene oxide in order to produce the desired final product while using at least one DMC catalyst. The inventive method is characterized in that sodium hydroxide is used as the basic catalyst in step a).

    Abstract translation: 本发明涉及一种生产聚醚醇的方法，该方法包括以下步骤：a）使低分子量醇与烯化氧在碱性催化剂存在下反应以形成分子量为200的烯化氧加成产物 至900克/摩尔; b）从步骤a）中获得的产物中分离碱性催化剂，并且; c）使用至少一种DMC催化剂，使步骤b）中获得的产物与另一种烯化氧反应以产生所需的最终产物。 本发明方法的特征在于，在步骤a）中使用氢氧化钠作为碱性催化剂。

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