公开(公告)号：BRPI0719214A2

公开(公告)日：2014-07-01

申请号：BRPI0719214

申请日：2007-10-12

Applicant: BASF SE

Inventor： SCHMIDT THOMAS ,  GEBHARDT JOACHIM ,  LOEHR SANDRA ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  ERK PETER ,  SAXELL HEIDI EMILIA ,  HAMPRECHT GERHARD ,  SEITZ WERNER ,  MAYER GUIDO ,  WOLF BERND ,  COX GERHARD ,  MICHEL ALFRED ,  ZAGAR CYRILL ,  REINHARD ROBERT ,  SIEVERNICH BERND

IPC: C07D239/54 ,  A01N43/48

Abstract: The present invention relates to hydrates of 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1-(2H)pyrimidinyl]-4-fluoro-N-[[methyl(1-methylethyl)amino]-sulfonyl]benzamide. The invention also relates to a process for the preparation of these hydrates and to plant protection formulations which comprise hydrates of the phenyluracil I.

公开(公告)号：CA2666196C

公开(公告)日：2013-05-28

申请号：CA2666196

申请日：2007-10-12

Applicant: BASF SE

Inventor： SCHMIDT THOMAS ,  GEBHARDT JOACHIM ,  LOEHR SANDRA ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  ERK PETER ,  SAXELL HEIDI EMILIA ,  HAMPRECHT GERHARD ,  SEITZ WERNER ,  MAYER GUIDO ,  WOLF BERND ,  COX GERHARD ,  MICHEL ALFRED ,  ZAGAR CYRILL ,  REINHARD ROBERT ,  SIEVERNICH BERND

IPC: C07D239/54 ,  A01N43/48

Abstract: The present invention relates to a crystalline form of 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1-(2H)-pyrimidinyl]-4-fluoro-N-[[methyl-(1-methylethyl)amino]sulphonyl]benzamide. The invention also relates to a method for preparing this crystalline form and to formulations for crop protection which comprise this crystalline form of the phenyluracil.

公开(公告)号：UA100677C2

公开(公告)日：2013-01-25

申请号：UAA200904213

申请日：2007-10-12

Applicant: BASF SE

Inventor： SCHMIDT THOMAS ,  GEBHARDT JOACHIM ,  LOEHR SANDRA ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  ERK PETER ,  SAXELL HEIDI EMILIA ,  HAMPRECHT GERHARD ,  SEITZ WERNER ,  MAYER GUIDO ,  WOLF BERND ,  COX GERHARD ,  MICHEL ALFRED ,  ZAGAR CYRILL ,  REINHARD ROBERT ,  SIEVERNICH BERND

IPC: C07D239/54 ,  A01N43/48 ,  A01N43/54

Abstract: Данноеизобретениекасаетсякристаллическойформы 2-хлор-5-[3,6-дигидро-3-метил-2,6-диоксо-4-(трифторметил)-1-(2Н)-пиримидинил]-4-фтор-N-[[метил-(1-метилэтил)амино] сульфонил]бензамида, способаегополучения, атакжепрепаратовдлязащитырастений, которыесодержатуказанноесоединение.

公开(公告)号：BRPI0618301A2

公开(公告)日：2012-05-08

申请号：BRPI0618301

申请日：2006-10-26

Applicant: BASF SE

Inventor： BRINK MONIKA ,  KNELL MARCUS ,  WEVERS JAN HENDRIK

IPC: C07D213/81 ,  C07D213/79

Abstract: The invention relates to a process for the preparation of pyridylcarboxylic amides and esters I, Formula (I) wherein Hal, X and R1 have the meanings given in claim 1, which comprises the following steps: (a) heating a mixture consisting essentially of trichloromethylpyridine II, Formula (II), wherein Hal has the meaning given, and 1.0 to 1.5 equivalents of concentrated sulfuric acid, characterized in that the trichloromethylpyridine II in a liquid form is added to the concentrated sulfuric acid at a temperature from 110° C. to 160° C.; and (b) reacting the intermediate product obtained in step (a) with an amine or alcohol III, HXR1, wherein X and R1 have the meaning given, optionally in the presence of a solvent and/or a base.

公开(公告)号：NZ575890A

公开(公告)日：2011-07-29

申请号：NZ57589007

申请日：2007-10-12

Applicant: BASF SE

Inventor： SCHMIDT THOMAS ,  GEBHARDT JOACHIM ,  LOHR SANDRA ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  ERK PETER ,  SAXELL HEIDI EMILIA ,  HAMPRECHT GERHARD ,  SEITZ WERNER ,  MAYER GUIDO ,  WOLF BERND ,  COX GERHARD ,  MICHEL ALFRED ,  ZAGAR CYRILL ,  REINHARD ROBERT ,  SIEVERNICH BERND

IPC: C07D239/54 ,  A01N43/48

Abstract: Disclosed is a crystalline form of 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1-(2H)-pyrimidinyl]-4-fluoro-N-[[methyl-(1-methylethyl)amino]sulphonyl]benzamide of formula I. Also disclosed is a method for preparing the phenyluracil crystalline form, and formulations for crop protection which comprise the crystalline form.

公开(公告)号：AT500232T

公开(公告)日：2011-03-15

申请号：AT07821246

申请日：2007-10-12

Applicant: BASF SE

Inventor： SCHMIDT THOMAS ,  GEBHARDT JOACHIM ,  LOEHR SANDRA ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  ERK PETER ,  SAXELL HEIDI EMILIA ,  HAMPRECHT GERHARD ,  SEITZ WERNER ,  MAYER GUIDO ,  WOLF BERND ,  COX GERHARD ,  MICHEL ALFRED ,  ZAGAR CYRILL ,  REINHARD ROBERT ,  SIEVERNICH BERND

IPC: C07D239/54 ,  A01N43/48

Abstract: The present invention relates to a crystalline form of 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1-(2H)pyrimidinyl]-4-fluoro-N-[[methyl(1-methylethyl)-amino]sulfonyl]benzamide. The invention also relates to a process for the preparation of this crystalline form and to plant protection formulations which comprise this crystalline form of the phenyluracil.

公开(公告)号：ZA200903230B

公开(公告)日：2010-07-28

申请号：ZA200903230

申请日：2009-05-11

Applicant: BASF SE

Inventor： SCHMIDT THOMAS ,  GEBHARDT JOACHIM ,  LOEHR SANDRA ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  ERK PETER ,  HAMPRECHT GERHARD ,  SEITZ WERNER ,  MAYER GUIDO ,  WOLF BERND ,  COX GERHARD ,  ZAGAR CYRILL ,  REINHARD ROBERT ,  SIEVERNICH BERND ,  SAXELL HEIDI EMILIA ,  MICHEL ALFRED

IPC: A01N20100101 ,  C07D20100101

Abstract: The present invention relates to hydrates of 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1-(2H)pyrimidinyl]-4-fluoro-N-[[methyl(1-methylethyl)amino]-sulfonyl]benzamide. The invention also relates to a process for the preparation of these hydrates and to plant protection formulations which comprise hydrates of the phenyluracil I.

公开(公告)号：DE602006012870D1

公开(公告)日：2010-04-22

申请号：DE602006012870

申请日：2006-10-26

Applicant: BASF SE

Inventor： BRINK MONIKA ,  KNELL MARCUS ,  WEVERS JAN HENDRIK

IPC: C07D213/81 ,  C07D213/79

Abstract: The invention relates to a process for the preparation of pyridylcarboxylic amides and esters I, Formula (I) wherein Hal, X and R1 have the meanings given in claim 1, which comprises the following steps: (a) heating a mixture consisting essentially of trichloromethylpyridine II, Formula (II), wherein Hal has the meaning given, and 1.0 to 1.5 equivalents of concentrated sulfuric acid, characterized in that the trichloromethylpyridine II in a liquid form is added to the concentrated sulfuric acid at a temperature from 110° C. to 160° C.; and (b) reacting the intermediate product obtained in step (a) with an amine or alcohol III, HXR1, wherein X and R1 have the meaning given, optionally in the presence of a solvent and/or a base.

公开(公告)号：PL1893586T3

公开(公告)日：2009-03-31

申请号：PL06755248

申请日：2006-05-18

Applicant: BASF SE

Inventor： GEBHARDT JOACHIM ,  LÖHR SANDRA ,  KEIL MICHAEL ,  SCHMIDT THOMAS ,  WEVERS JAN HENDRIK ,  ZECH HELMUT ,  HÄBERLE RUDOLF

IPC: C07D239/54

公开(公告)号：ES2311283T3

公开(公告)日：2009-02-01

申请号：ES06755248

申请日：2006-05-18

Applicant: BASF SE

Inventor： GEBHARDT JOACHIM ,  LOHR SANDRA ,  KEIL MICHAEL ,  SCHMIDT THOMAS ,  WEVERS JAN HENDRIK ,  ZECH HELMUT

IPC: C07D239/54

Abstract: Un proceso para preparar 1-alquil-3-feniluracilos de la fórmula I (Ver fórmula) donde las variables son como se define más abajo: R 1 es C1-C6-alquilo; R 2 y R 3 independientemente el uno del otro son hidrógeno, C1-C6-alquilo o C1-C6-haloalquilo; R 4 y R 5 independientemente el uno del otro son hidrógeno, halógeno, ciano, C1-C6-alquilo o C1-C6-haloalquilo; R 6 y R 7 independientemente el uno del otro son hidrógeno, C1-C6-alquilo, C1-C6-alcoxi, C3-C6-alquenilo, C3-C6-alquinilo, C3-C6-cicloalquilo, C3-C6-cicloalquenilo, fenilo o bencilo; haciendo reaccionar 3-feniluracilos de la fórmula II (Ver fórmula) donde las variables R 2 a R 7 son como se definió más arriba y agentes de alquilación de la fórmula III R 1 - L1 III, donde R 1 es como se definió más arriba y L1 es halógeno, hidrógenosulfato, C1-C6-alquilo sulfato, C1-C6-alquilo carbonato, C1-C6-alquilosulfoniloxi, C1-C6- haloalquilosulfoniloxi o fenilsulfoniloxi, donde el anillo fenilo puede portar uno o más sustituyentes del grupo consistente de halógeno, nitro, C1-C6-alquilo y C1-C6-haloalquilo, los unos con los otros en donde durante la reacción completa el pH es mantenido en un rango de 1 a 6 por adición de una base poco a poco.