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公开(公告)号:HUT71313A
公开(公告)日:1995-11-28
申请号:HU9400773
申请日:1994-03-16
Applicant: DEGUSSA
Inventor: BINDER WOLFRAM , FRIEDRICH HEINZ , DAHM FRANZ-LUDWIG , HERTZ ULRICH , LOTTER HERMANN , HOHN WOLFGANG , GREISSINGER DIETER , POLZER WOLFGANG
Abstract: 2. Animal feed additives based on fermentation broth further contain, in addition to the additive, other fermentation broth constituents. Such products, after spray-drying, generally have an excessively low bulk density and/or are sticky. To granulate these products, processing aids have therefore been added, e.g. perlite or sawdust. Alternatively, such products have been dewatered by azeotropic distillation with paraffin oil to give granules. The object of the invention is a highly concentrated animal feed additive which, in particular, is to have a bulk density of at least 550 kg/m and a standardisable active compound content. 2.2. By pelletising, stable granules can be produced from an animal feed additive-containing fermentation broth if the fermentation product is contained at at least 33% by weight. Granules can particularly readily be produced by pelletising if the pellets are built up of at least 30% by weight fine grain with at least 70% by weight having a particle size
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公开(公告)号:SK284392A3
公开(公告)日:1994-08-10
申请号:SK284392
申请日:1992-09-16
Applicant: DEGUSSA
Inventor: BINDER WOLFRAM , FRIEDRICH HEINZ , LOTTER HERMANN , TANNER HERBERT , HOLLDORFF HENNING , LEUCHTENBERGER WOLFGANG
Abstract: Fermentative preparation of amino acids for animal feed supplement purposes is a complex process, since the amino acid is present in the fermentation broth at 40 to 90 %, up to 10 % of proteins, 8 % of carboxyl acid with less that 8 C, up to 10 % of sugar, up to 5 % of fats and oils, 3 to 30 % of mineral substances. The method consists of the cultivating at least one microorganism, producing at least one amino acid in fermentative medium, comprising at least one source of carbon and nitrogen, mineral substances and trace elements, at the second step fermentation consists of at least 30 % of fermentation time is concentration of valuable sugar in fermentative medium max. 0.3 % wt. and at the end to obtain fermentative tan-liquor with valuable sugar max. 1g/l, at the third step there are partly reduced microorganisms of the biomass to max. 10 % wt. in dry matter and at the fourth step the additive is dried straight from fermentative tan-liquor.
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公开(公告)号:MX154999A
公开(公告)日:1988-01-19
申请号:MX778482
申请日:1982-07-20
Applicant: DEGUSSA
Inventor: BESCHKE HELMUT , DAHM FRANZ LUDWIG , FRIEDRICH HEINZ
IPC: A61K31/44 , C07D213/85
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公开(公告)号:CA1169864A
公开(公告)日:1984-06-26
申请号:CA407691
申请日:1982-07-21
Applicant: DEGUSSA
Inventor: BESCHKE HELMUT , DAHM FRANZ L , FRIEDRICH HEINZ
IPC: C07D213/84 , C07D213/85
Abstract: The gaseous mixture resulting from the catalytic reaction of 3-methylpyridine with ammonia and oxygen is treated with water to recover 3-cyanopyridine. The treatment takes place in two steps. In the first step there is used a temperature of about 30 to 60.degree.C and in the second step at a temperature about 10 to 30.degree.C lower than in the first step.
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公开(公告)号:CA1164437A
公开(公告)日:1984-03-27
申请号:CA397240
申请日:1982-02-26
Applicant: DEGUSSA
Inventor: BESCHKE HELMUT , FRIEDRICH HEINZ , HEILOS JOHANNES
IPC: B01J23/16 , B01J21/16 , B01J23/22 , B01J23/34 , B01J23/84 , B01J23/847 , B01J35/10 , C07B61/00 , C07D213/84 , C07D213/85
Abstract: For the catalytic reaction of 3-methyl pyridine with ammonia and oxygen to 3-cyanopyridine catalysts consisting of compounds of the elements antimony, vanadium and oxygen and at least one of the elements iron, copper, titanium, cobalt, manganese and nickel, the atomic ratio of antimony to vanadium being greater than 1, and containing in addition to these compounds layer lattice silicate and highly dispersed silicon dioxide are used. These catalysts are very selective and result in high yields and space time yields.
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公开(公告)号:MX5066E
公开(公告)日:1983-03-09
申请号:MX679178
申请日:1978-01-25
Applicant: DEGUSSA
Inventor: BESCHKE HELMUT , FRIEDRICH HEINZ
IPC: C07D213/10 , B01J21/00 , C07B61/00 , C07D213/04 , C07D213/12
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公开(公告)号:CA1136148A
公开(公告)日:1982-11-23
申请号:CA382803
申请日:1981-07-29
Applicant: DEGUSSA
Inventor: BESCHKE HELMUT , DAHM FRANZ , FRIEDRICH HEINZ , PRESCHER GUENTER
IPC: C07D213/82 , C07D213/81
Abstract: Crude nicotinamide is purified by a recrystallization and in this way freed especially from nicotinic acid and salts of nicotinic acid. As solvent there is used a 2-methylpropanol-1 containing water. The recrystallization takes place at a pH between about 7 and 10. In this process an outstandingly pure nicotamide is obtained with favorable yield with only a single recrystallization.
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公开(公告)号:FR2500829A1
公开(公告)日:1982-09-03
申请号:FR8202967
申请日:1982-02-23
Applicant: DEGUSSA
Inventor: BERGSTEIN WOLFGANG , BESCHKE HELMUT , FRIEDRICH HEINZ , KLEEMANN AXEL , PRESCHER GUNTHER
IPC: B01J21/16 , B01J23/22 , B01J23/34 , B01J23/84 , B01J35/10 , C07B61/00 , C07D241/24 , B01J21/08 , B01J23/16
Abstract: For the catalytic reaction of 2-methylpyrazine with ammonia and oxygen to form 2-cyanopyrazine there are used compounds of the elements antimony, vanadium, and oxygen and at least one of the elements iron, copper, titanium, cobalt, manganese, and nickel, whereby the atomic ratio of antimony to vanadium is greater than 1 and which contain besides these compounds a lattice layer silicate and a highly dispersed silica. These catalysts are very selective and result in high yields and high space-time-yields.
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公开(公告)号:CA1115705A
公开(公告)日:1982-01-05
申请号:CA288852
申请日:1977-10-17
Applicant: DEGUSSA
Inventor: BESCHKE HELMUT , FRIEDRICH HEINZ
IPC: C07D213/12 , C07D213/22 , C07D213/04
Abstract: The present invention provides a process for producing pyridines which are aromatically and heteroaromatically substituted in the 2 and 3 position, in which aromatically and heteroaromatically substituted ketones, which have at least one reactive methylene group adjacent to the keto group, are reacted with aliphatic oxo compounds, which have an unsaturated carbon bond adjacent to the oxo group, in the gas phase in the presence of ammonia and in the presence of a catalyst having dehydrating and dehydrogenating properties at temperatures from approximately 250 to550.degree.C.
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公开(公告)号:IN147406B
公开(公告)日:1980-02-16
申请号:IN75CA1978
申请日:1978-01-19
Applicant: DEGUSSA
Inventor: BESCHKE H , FRIEDRICH HEINZ
IPC: B01J21/00 , C07B61/00 , C07D213/12 , C07D213/09 , B01J11/32 , C07D31/06 , C07D31/08 , C07D31/20
Abstract: 2-Methyl pyridine and 3-methyl pyridine are produced by the catalytic reaction of acrolein and acetone with ammonia in the gas phase. There is used as the catalyst a highly dispersed aluminum silicate containing 3 to 30 weight percent aluminum oxide, a BET surface area of 200 to 800 m2/g, a pore volume of 0.4 to 1.0 cm3/g and a pore diameter of 20 to 100 x 10-8 cm.
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