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    PROCESS FOR THE PRODUCTION OF HCFC-1233zd
    23.
    发明公开
    PROCESS FOR THE PRODUCTION OF HCFC-1233zd 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON HCFC-1233ZD

    公开(公告)号：EP2814795A4

    公开(公告)日：2015-09-30

    申请号：EP13748643

    申请日：2013-02-11

    Applicant: HONEYWELL INT INC

    Inventor： COTTRELL STEPHEN A ,  TUNG HSUEH SUNG ,  POKROVSKI KONSTANTIN A ,  WANG HAIYOU ,  MERKEL DANIEL C

    IPC: C07C17/20 ,  C07B61/00 ,  C07C21/18

    CPC classification number: C07C17/23 ,  C07C17/20 ,  C07C17/206 ,  C07C17/25 ,  C07C17/38 ,  C07C17/383 ,  C07C21/18

    Abstract: A process for the manufacture of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) at commercial scale from the reaction of HCC-240 and HF is disclosed. In one embodiment, HCC-240fa and HF are fed to a reactor operating at high pressure. Several different reactor designs useful in this process include; a stirred-tank reactor (batch and/or continuous flow); a plug flow reactor; a static mixer used as a reactor; at least one of the above reactors operating at high pressure; optionally combined with a distillation column running at a lower pressure; and combinations of the above; and/or with a distillation column. The resulting product stream consisting of 1233zd, HCl, HF, and other byproducts is partially condensed to recover HF by phase separation. The recovered HF phase is recycled to the reactor. The HCl is scrubbed from the vapor stream and recovered as an aqueous solution. The remaining organic components including the desired HCFC-1233zd are scrubbed, dried and distilled to meet commercial product specifications.

    Abstract translation: 公开了从HCC-240和HF的反应制备商业规模的1-氯-3,3,3-三氟丙烯（HCFC-1233zd）的方法。 在一个实施方案中，将HCC-240fa和HF加入到在高压下操作的反应器中。 在这个过程中有用的几种不同的反应器设计包括： 搅拌釜反应器（批次和/或连续流动）; 活塞流反应器; 用作反应器的静态混合器; 上述反应器中的至少一个在高压下运行; 任选地与在较低压力下运行的蒸馏塔组合; 和上述的组合; 和/或用蒸馏塔。 由1233zd，HCl，HF和其他副产物组成的产物流部分冷凝，通过相分离回收HF。 将回收的HF相再循环到反应器中。 将HCl从蒸汽流中洗涤并作为水溶液回收。 将包含所需HCFC-1233zd的剩余有机组分进行洗涤，干燥和蒸馏以满足商业产品规格。

    METHOD FOR CAPTURING AND RECYCLING IRON CATALYST USED IN THE PRODUCTION OF HALOALKANE COMPOUNDS
    28.
    发明公开
    METHOD FOR CAPTURING AND RECYCLING IRON CATALYST USED IN THE PRODUCTION OF HALOALKANE COMPOUNDS 有权
    VERFAHRENFÜRERFASSUNG UND RECYCLING VON EISENKATALYSATOREN ZUR HERSTELLUNG VON HALOALKANVERBINDUNGEN

    公开(公告)号：EP2714270A4

    公开(公告)日：2015-03-11

    申请号：EP12792675

    申请日：2012-05-31

    Applicant: HONEYWELL INT INC

    Inventor： CLOSE JOSHUA ,  WANG HAIYOU ,  TUNG HSUEH SUNG ,  COTTRELL STEPHEN A

    IPC: B01J23/745 ,  B01J19/08 ,  B01J19/20 ,  B03C1/26 ,  C07C21/06

    CPC classification number: B01J8/10 ,  B01J8/005 ,  B01J8/0075 ,  B01J23/745 ,  B03C1/0335 ,  B03C5/00 ,  C07C17/275 ,  C07C17/278 ,  Y02P20/584 ,  C07C19/01

    Abstract: Disclosed is a method for capturing and recycling iron catalyst used in the production of haloalkane compounds and more particularly, to an improved process for the manufacture of the compound 1,1,1,3,3-pentachloropropane (HCC-240fa), in which an electromagnetic separation unit (EMSU) is used to facilitate the reaction. When energized, the EMSU functions to remove all iron particles from the reactor effluent; when de-energized, the iron particles captured by the EMSU can be flushed back into the reactor for re-use in the continued production of HCC-240fa. The present invention is also useful in the manufacturing processes for other haloalkane compounds such as HCC-250 and HCC-360.

    Abstract translation: 公开了一种用于捕获和再循环用于制备卤代烷烃化合物的铁催化剂的方法，更具体地说，涉及制备化合物1,1,1,3,3-五氯丙烷（HCC-240fa）的改进方法，其中 使用电磁分离单元（EMSU）来促进反应。 通电时，EMSU用于从反应器流出物中除去所有铁颗粒; 当断电时，由EMSU捕获的铁颗粒可以冲洗回反应器，以便在继续生产HCC-240fa时重新使用。 本发明也可用于其它卤代烷烃化合物如HCC-250和HCC-360的制备方法。

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