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    METHOD FOR AVOIDING THE GENERATION OF BY-PRODUCTS DURING THE PRODUCTION OF HALOALKANE COMPOUNDS
    2.
    发明申请
    METHOD FOR AVOIDING THE GENERATION OF BY-PRODUCTS DURING THE PRODUCTION OF HALOALKANE COMPOUNDS 审中-公开
    避免生成HALOALKANE化合物时副产物生成的方法

    公开(公告)号：WO2012166754A2

    公开(公告)日：2012-12-06

    申请号：PCT/US2012039914

    申请日：2012-05-30

    Applicant: HONEYWELL INT INC ,  CLOSE JOSHUA ,  WANG HAIYOU ,  TUNG HSUEH SUNG

    Inventor： CLOSE JOSHUA ,  WANG HAIYOU ,  TUNG HSUEH SUNG

    IPC: C07C17/275 ,  B01J23/745 ,  C07C19/01

    CPC classification number: C07C17/278 ,  B01J23/745 ,  B01J35/023 ,  C07C17/275 ,  C07C19/01

    Abstract: Disclosed is a process for the manufacture of haloalkane compounds, and more particularly, to an improved process for the manufacture of the compound 1,1,1,3,3-pentachloropropane (HCC-240fa), which mitigates the formation of by-products. The present invention is also useful in the manufacture of other haloalkane compounds such as HCC-250 and HCC-360. One embodiment of the process comprises a method and system for avoiding the formation of polyvinyl chloride during the production of HCC-240fa from CCl4, in which vinyl chloride (VCM) is fed into a reactor as a vapor instead of as a liquid, using a diffusing device to further increase the contact surface between VCM vapor and CCl4.

    Abstract translation: 公开了一种制备卤代烷烃化合物的方法，更具体地说，涉及制备化合物1,1,1,3,3-五氯丙烷（HCC-240fa）的改进方法，其减少了副产物的形成 。 本发明也可用于制备其它卤代烷烃化合物如HCC-250和HCC-360。 该方法的一个实施方案包括在CCl 4生产HCC-240fa期间避免形成聚氯乙烯的方法和系统，其中将氯乙烯（VCM）作为蒸气而不是作为液体加入到反应器中，使用 扩散装置进一步增加VCM蒸气与CCl4之间的接触面。

    METHOD FOR MITIGATING THE FORMATION OF BY-PRODUCTS DURING THE PRODUCTION OF HALOALKANE COMPOUNDS
    3.
    发明申请
    METHOD FOR MITIGATING THE FORMATION OF BY-PRODUCTS DURING THE PRODUCTION OF HALOALKANE COMPOUNDS 审中-公开
    在制备HALOALKANE化合物时减少副产物形成的方法

    公开(公告)号：WO2012166759A3

    公开(公告)日：2013-03-07

    申请号：PCT/US2012039922

    申请日：2012-05-30

    Applicant: HONEYWELL INT INC ,  CLOSE JOSHUA ,  WANG HAIYOU ,  TUNG HSUEH SUNG

    Inventor： CLOSE JOSHUA ,  WANG HAIYOU ,  TUNG HSUEH SUNG

    IPC: C07C17/275 ,  B01J23/745 ,  B01J31/02 ,  C07C19/01

    CPC classification number: C07C17/275 ,  B01J23/745 ,  B01J23/94 ,  B01J31/0257 ,  B01J35/023 ,  B01J37/04 ,  B01J38/00 ,  B01J2231/32 ,  C07C17/278 ,  Y02P20/584 ,  C07C19/01

    Abstract: Disclosed is a process for the manufacture of haloalkane compounds, and more particularly, an improved process for the manufacture of the compound 1,1,1,3,3-penta-chloropropane (HCC-240fa), which mitigates the formation of by-products from vinyl chloride (CH2=CHCl). The present invention is also useful in the manufacture of other haloalkane compounds such as HCC-250 and HCC-360. One embodiment of the invention comprises a method for mitigating 1,1,3,3,5,5-hexachloropentane and 1,1,1,3,5,5-hexachloropentane formation in the HCC-240fa manufacturing process, in which FeCl3, is introduced to a reactor only after the start-up phase has ended and a continuous operation has started. In a preferred embodiment, "pre-chelated" FeCl3, which is concentrated in a catalyst recovery column, is introduced to reactor after the continuous operation has started.

    Abstract translation: 公开了一种制备卤代烷烃化合物的方法，更具体地说，涉及制备化合物1,1,1,3,3-五氯丙烷（HCC-240fa）的改进方法，其减少副产物的形成， 氯乙烯（CH 2 = CHCl）的产物。 本发明也可用于制备其它卤代烷烃化合物如HCC-250和HCC-360。 本发明的一个实施方案包括在HCC-240fa制造方法中减轻1,1,3,3,5,5-六氯戊烷和1,1,1,3,5,5-六氯戊烷形成的方法，其中FeCl 3， 仅在启动阶段结束并且连续运行已经开始之后被引入反应器。 在优选的实施方案中，将浓缩在催化剂回收塔中的“预螯合的”​​FeCl 3在连续操作开始后引入反应器。

    METHOD FOR CAPTURING AND RECYCLING IRON CATALYST USED IN THE PRODUCTION OF HALOALKANE COMPOUNDS
    5.
    发明公开
    METHOD FOR CAPTURING AND RECYCLING IRON CATALYST USED IN THE PRODUCTION OF HALOALKANE COMPOUNDS 有权
    VERFAHRENFÜRERFASSUNG UND RECYCLING VON EISENKATALYSATOREN ZUR HERSTELLUNG VON HALOALKANVERBINDUNGEN

    公开(公告)号：EP2714270A4

    公开(公告)日：2015-03-11

    申请号：EP12792675

    申请日：2012-05-31

    Applicant: HONEYWELL INT INC

    Inventor： CLOSE JOSHUA ,  WANG HAIYOU ,  TUNG HSUEH SUNG ,  COTTRELL STEPHEN A

    IPC: B01J23/745 ,  B01J19/08 ,  B01J19/20 ,  B03C1/26 ,  C07C21/06

    CPC classification number: B01J8/10 ,  B01J8/005 ,  B01J8/0075 ,  B01J23/745 ,  B03C1/0335 ,  B03C5/00 ,  C07C17/275 ,  C07C17/278 ,  Y02P20/584 ,  C07C19/01

    Abstract: Disclosed is a method for capturing and recycling iron catalyst used in the production of haloalkane compounds and more particularly, to an improved process for the manufacture of the compound 1,1,1,3,3-pentachloropropane (HCC-240fa), in which an electromagnetic separation unit (EMSU) is used to facilitate the reaction. When energized, the EMSU functions to remove all iron particles from the reactor effluent; when de-energized, the iron particles captured by the EMSU can be flushed back into the reactor for re-use in the continued production of HCC-240fa. The present invention is also useful in the manufacturing processes for other haloalkane compounds such as HCC-250 and HCC-360.

    Abstract translation: 公开了一种用于捕获和再循环用于制备卤代烷烃化合物的铁催化剂的方法，更具体地说，涉及制备化合物1,1,1,3,3-五氯丙烷（HCC-240fa）的改进方法，其中 使用电磁分离单元（EMSU）来促进反应。 通电时，EMSU用于从反应器流出物中除去所有铁颗粒; 当断电时，由EMSU捕获的铁颗粒可以冲洗回反应器，以便在继续生产HCC-240fa时重新使用。 本发明也可用于其它卤代烷烃化合物如HCC-250和HCC-360的制备方法。

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