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21.发明授权NON-AQUEOUS, HETEROGENEOUS POLYMERIZATION PROCESS AND REACTION PRODUCT OBTAINED THEREBY 有权NOT水性，非均相聚合，从而GOT反应产物
公开(公告)号：EP1037929B1
公开(公告)日：2006-07-12
申请号：EP98958014.7
申请日：1998-11-17
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna , CHUANG, Jui-Chang , SHIH, Jenn, S. , MENON, Anil , NERELLA, Nadhamuni, G.
CPC classification number: A61K8/062 , A61K8/06 , A61K8/064 , A61K8/8141 , A61K9/0014 , A61K47/14 , A61K47/32 , A61K47/44 , A61K2800/57 , A61Q17/04 , A61Q19/00 , C08F2/06 , C08F226/10 , Y10T428/2987 , C08F226/04 , C08F216/125
Abstract: A non-aqueous, heterogeneous polymerization process comprises heating a reaction mixture of about 5-70 %, preferably 10-30 %, by weight, of a vinyl monomer in an oil as solvent, and a free radical initiator, optionally in the presence of a crosslinking agent and/or a surfactant, wherein the oil solvent is present in an amount sufficient to keep the resultant polymer in a stirrable state throughout the polymerization. The polymer reaction product is capable of forming a uniform emulsion or gel upon addition of water thereto.
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22.发明授权CONTINUOUS, SOLVENT-FREE PROCESS FOR MAKING COPOLYMERS OF MALEIC ANHYDRIDE AND C 1-4? ALKYL VINYL ETHER 有权用于生产马来酸酐和C1-4的共聚物连续无溶剂法制？ 烷基乙烯基醚
公开(公告)号：EP1299425B1
公开(公告)日：2005-10-12
申请号：EP01930999.6
申请日：2001-05-02
Applicant: ISP INVESTMENTS INC.
Inventor： BISS, Russell , COHEN, Jeffrey, Dr. , ZAMORA, John , PLOCHOCKA, Krystyna , LYNN, Jeffrey, A.
IPC: C08F222/04 , C08F216/18
CPC classification number: C08F222/06 , C08F2/02 , C08F216/18 , Y02P20/582
Abstract: A continuous, solvent-free process for obtaining solvent-free, fine white powders of high molecular weight alternating copolymers of maleic anhydride and a C1-C4 alkyl vinyl ether, without odor or taste, having the molecular structure (A-B)n, where A is maleic anhydride, B is an alkyl vinyl ether and n is an integer indicative of the molecular weight of the copolymer, which comprises feeding alkyl vinyl ether as reactant and solvent in excess over the desired 1:1 mole ratio of A:B in the copolymer, molten maleic anhydride and a free radical initiator, continuously at predetermined feeding rates into a reactor heated at a reaction temperature of about 50 DEG to 100 DEG C, holding the reactants in the reactor for a predetermined average residence time, withdrawing reaction product, residual alkyl vinyl ether and initiator at the same rate as the feed rate of reactants into the reactor, stripping residual alkyl vinyl ether from the reaction product, drying the copolymer obtained of any remaining traces of alkyl vinyl ether, and recycling recovered alkyl vinyl ether back into reactor as reactant and solvent.
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23.发明授权SOLVENT-FREE, FINE WHITE POWDERS OF A COPOLYMER OF MALEIC ANHYDRIDE AND A C1-C4 ALKYL VINYL ETHER SUBSTANTIALLY FREE OF POLY(ALKYL VINYL ETHER) HOMOPOLYMER 有权不含溶剂，白色细粉马来酸酐以及C1-C4烷基乙烯基醚的共聚物，几乎不含由聚（烷基乙烯基醚）的均聚物
公开(公告)号：EP1198486B1
公开(公告)日：2005-10-05
申请号：EP00916073.0
申请日：2000-03-02
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna
IPC: C08F222/04 , C08F2/42
CPC classification number: A61K8/347 , A61K8/8164 , A61Q11/00 , C08F216/18 , C08F222/06 , C08K5/0008 , C08L35/08
Abstract: Solvent-free, fine white powders of a copolymer of maleic anhydride and a C1-C4 alkyl vinyl ether substantially free of poly(alkylvinyl ether) homopolymer.
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24.发明授权PROCESS FOR THE PRODUCTION OF SOLVENT-FREE, FINE WHITE POWDERS OF HIGH MOLECULAR WEIGHT COPOLYMERS OF MALEIC ANHYDRIDE AND A C1-C4 ALKYL VINYL ETHER WITHOUT ODOR OR TASTE 有权用于生产高分子量无溶剂，白色细粉，马来酸酐的共聚物和C1-C4烷基乙烯基醚WITHOUT气味或味道
公开(公告)号：EP1198483B1
公开(公告)日：2004-07-28
申请号：EP00916072.2
申请日：2000-03-02
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna
CPC classification number: C08F6/005 , C08F216/14 , C08K5/13 , C08L35/08
Abstract: Solvent-free, the white powders of high molecular weight copolymeers of maleic anhydride and C1-C4 alkyl vinyl ethers, which are particularly useful as starting materials for denture adhesives. A solvent-free process for making such copolymers also is described.
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25.发明公开CONTINUOUS, SOLVENT-FREE PROCESS FOR MAKING TERPOLYMERS OF MALEIC ANHYDRIDE, C 1-4? ALKYL VINYL ETHER AND ISOBUTYLENE 有权连续，无溶剂PROCESS FOR PRODUCING马来酸酐，C 1-4烷基乙烯基醚和异丁烯的三元共聚物
公开(公告)号：EP1297036A1
公开(公告)日：2003-04-02
申请号：EP01937529.4
申请日：2001-05-17
Applicant: ISP INVESTMENTS INC.
Inventor： BISS, Russell , COHEN, Jeffrey , ZAMORA, John , PLOCHOCKA, Krystyna , LYNN, Jeffrey, A.
IPC: C08F222/04 , C08F10/00 , C08F110/10 , C08F210/10
CPC classification number: C08F210/10 , C08F6/001 , Y02P20/582 , C08F222/04 , C08F216/04
Abstract: A continuous, solvent-free process for obtaining solvent-free, fine white powders of high molecular weight alternating terpolymers of maleic anhydride, a C1-C4 alkyl vinyl ether and isobutylene, without odor or taste.
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Patent Agency Ranking
公开(公告)号：EP0604454B1
公开(公告)日：1998-10-21
申请号：EP92916901.9
申请日：1992-07-31
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna , CHUANG, Jui-Chang , LOGIN, Robert, B.
CPC classification number: C08K5/005 , C08K3/30 , C08K5/175 , C08L35/08 , A61K6/0026
Abstract: What is provided herein is a stabilized aqueous solution of a C1-C5 alkyl vinyl ether and maleic acid copolymer which includes about 100 to 1,000 ppm of (1) an additive mixture of (a) about 30-70 % by weight of ethylenediaminetetraacetic acid EDTA and (b) about 30-70 % by weight of a secondary additive which is an organic antioxidant and/or free radical scavenger selected from t-butylhydroquinone, propyl gallate and N,N-diethylhydroxylamine; or (2) 10-500 ppm of an inorganic reducing agent such as sulfur dioxide and salts derived from sulfur dioxide and alkali metals such as sodium or potassium bisulfite, sodium or potassium metabisulfite, sodium or potassium thiosulfite, or sodium or potassium sulfite, said stabilized solution exhibiting a retention of at least about 85-90 % of its original viscosity after 3 months.
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公开(公告)号：EP1635781B1
公开(公告)日：2007-11-28
申请号：EP04751626.5
申请日：2004-05-07
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna
IPC: A61K8/89
CPC classification number: A61Q11/00 , A61K8/0208 , A61K8/8164 , A61K2800/57
Abstract: A polymer for use in an oral care composition which includes a monomer repeat unit containing an active material covalently bonded to a hydrolyzable side group of said monomer unit, and a spacer group positioned between the main chain of said polymer and said hydrolyzable side group, said polymer having a predetermined rapid rate of aqueous hydrolysis to release said active material therefrom.
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公开(公告)号：EP1551888A1
公开(公告)日：2005-07-13
申请号：EP03721684.3
申请日：2003-04-15
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna
IPC: C08F122/04
CPC classification number: C08F8/48 , C08F216/18 , C08F2800/10 , C08F222/02
Abstract: What is described herein is a terpolymer of maleic acid (MAA)/maleic anhydride (MAN)/alkylvinylether (AVE), made by partial cyclization, e.g. 1-99 %, of a maleic acid/alkylvinylether copolymer, preferably comprising, in mole %, 1-49 % MAA/1-49 % MAN/50 % AVE, and derivatized terpolymers thereof.
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29.发明公开CONTINUOUS, SOLVENT-FREE PROCESS FOR MAKING COPOLYMERS OF MALEIC ANHYDRIDE AND C 1-4? ALKYL VINYL ETHER 有权用于生产马来酸酐和C1-4的共聚物连续无溶剂法制？ 烷基乙烯基醚
公开(公告)号：EP1299425A1
公开(公告)日：2003-04-09
申请号：EP01930999.6
申请日：2001-05-02
Applicant: ISP INVESTMENTS INC.
Inventor： BISS, Russell , COHEN, Jeffrey , ZAMORA, John , PLOCHOCKA, Krystyna , LYNN, Jeffrey, A.
CPC classification number: C08F222/06 , C08F2/02 , C08F216/18 , Y02P20/582
Abstract: A continuous, solvent-free process for obtaining solvent-free, fine white powders of high molecular weight alternating copolymers of maleic anhydride and a C1-C4 alkyl vinyl ether, without odor or taste, having the molecular structure (A-B)n, where A is maleic anhydride, B is an alkyl vinyl ether and n is an integer indicative of the molecular weight of the copolymer, which comprises feeding alkyl vinyl ether as reactant and solvent in excess over the desired 1:1 mole ratio of A:B in the copolymer, molten maleic anhydride and a free radical initiator, continuously at predetermined feeding rates into a reactor heated at a reaction temperature of about 50° to 100 °C, holding the reactants in the reactor for a predetermined average residence time, withdrawing reaction product, residual alkyl vinyl ether and initiator at the same rate as the feed rate of reactants into the reactor, stripping residual alkyl vinyl ether from the reaction product, drying the copolymer obtained of any remaining traces of alkyl vinyl ether, and recycling recovered alkyl vinyl ether back into reactor as reactant and solvent.
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30.发明授权SOLVENT-FREE PROCESS FOR MAKING HIGH MOLECULAR WEIGHT TERPOLYMERS OF MALEIC ANHYDRIDE, C1-C4 ALKYL VINYL ETHER AND ISOBUTYLENE, AND DENTURE ADHESIVE AND DENTIFRICE COMPOSITIONS CONTAINING SUCH TERPOLYMERS 有权用于生产马来酸酐，C1-C4烷基乙烯基醚和异丁烯高的分子量和牙科修复体粘合剂的三元共聚物和无溶剂法制牙膏这些三元共聚物
公开(公告)号：EP1040144B1
公开(公告)日：2003-03-12
申请号：EP98948527.1
申请日：1998-09-22
Applicant: ISP INVESTMENTS INC.
Inventor： PLOCHOCKA, Krystyna , PROSISE, William, E. , ZHANG, Huixiang
IPC: C08F222/04 , C08F222/06 , C08F216/12 , C08F210/10 , C08L35/08 , C08K5/09
CPC classification number: C08F222/06 , A61K8/347 , A61K8/8164 , A61Q11/00 , C08K5/0008 , C08L35/08 , A61K6/0026
Abstract: This invention relates to high molecular weight terpolymers of maleic anhydride, C1-C4 alkyl vinyl ethers and isobutylene, and to a solvent-free process for making such terpolymers, which are particularly useful in denture adhesive and dentifrice compositions.
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