FLOW CONTROL IN A THREE-PHASE MONOLITHIC CATALYST REACTOR
    331.
    发明申请
    FLOW CONTROL IN A THREE-PHASE MONOLITHIC CATALYST REACTOR 审中-公开
    三相催化反应器中的流量控制

    公开(公告)号:WO02051532A3

    公开(公告)日:2003-01-09

    申请号:PCT/US0150501

    申请日:2001-12-20

    Applicant: CORNING INC

    Abstract: A method is disclosed for maintaining a volumetric gas to liquid ratio in a segmented gas/liquid flow along a reactor of monolithic catalyst beds in series. The present invention includes the steps of: initiating the segmented gas/liquid flow at a first end of the reactor by introducing feed liquid and feed gas both at a predetermined volume and a predetermined flow rate; injecting an additional amount of gas at least once into any of the spaces between catalyst beds; and combining the segments of the segmented gas/liquid flow at a second end of the reactor. The injection of gas is controlled such that the segmented gas/liquid flow can be maintained near or at the Taylor regime.

    Abstract translation: 公开了一种用于在沿着整体式催化剂床的反应器串联的分段气/液流中维持体积气体与液体比的方法。 本发明包括以下步骤:通过以预定的体积和预定流量引入进料液体和进料气体来在反应器的第一端引发分段的气/液流; 将至少一次额外量的气体注入催化剂床之间的任何空间; 并且在反应器的第二端处组合分段的气体/液体流的段。 控制气体的注入使得分段的气体/液体流可以保持在泰勒状态附近或处于泰勒状态。

    METHOD OF PREPARING SALTS OF DINITROMETHANE
    332.
    发明申请
    METHOD OF PREPARING SALTS OF DINITROMETHANE 审中-公开
    制备DINITROMETHANE的盐的方法

    公开(公告)号:WO00034223A1

    公开(公告)日:2000-06-15

    申请号:PCT/SE1999/002301

    申请日:1999-12-08

    CPC classification number: C07D239/62 C07C201/12 C07C205/02

    Abstract: A method of preparing dinitromethane salts usable as intermediate products and starting material for production of explosives and propellants. Substituted 1,2-diazoles, 1,2,4-triazoles or 1,3-diazines, such as barbituric acid, are nitrated to obtain a gem-dinitro group on a carbon atom in the heterocyclic ring. The product is hydrolysed to split off dinitromethane which is neutralised with a neutralising agent to obtain a corresponding salt of dinitromethane.

    Abstract translation: 制备可用作中间产物的二硝基甲烷盐和用于生产爆炸物和推进剂的起始原料的方法。 将取代的1,2-二唑,1,2,4-三唑或1,3-二嗪如巴比妥酸硝化以在杂环的碳原子上得到偕二硝基。 将产物水解分离二硝基甲烷,用中和剂中和,得到相应的二硝基甲烷盐。

    PROCESS FOR CONCENTRATING DILUTED SULFURIC ACID

    公开(公告)号:US20230406704A1

    公开(公告)日:2023-12-21

    申请号:US18035946

    申请日:2021-11-11

    Applicant: BASF SE

    CPC classification number: C01B17/905 C01B17/88 C07C201/06 B01D1/0094

    Abstract: The invention relates to a process for concentrating diluted sulfuric acid (10) which may comprise at least one nitroaromatic compound and/or nitric acid as impurities, comprising: (a) feeding the diluted sulfuric acid (10) into a first stage (1) in which low boilers are removed by evaporation and/or stripping to obtain a first concentrated sulfuric acid (12); (b) optionally feeding the first concentrated sulfuric acid (12) into a second evaporation stage (2) to obtain a second concentrated sulfuric acid (14); (c) feeding the second concentrated sulfuric (14) acid into a third evaporation stage (3) if step (b) is carried out, or feeding the first concentrated sulfuric acid (12) into the third evaporation stage (3) if step (b) is not carried out, to obtain concentrated sulfuric acid (16) as product, wherein an oxidizing agent (17) and/or a precursor of an oxidizing agent is fed into the third evaporation stage (3).

    METHOD FOR CONTINUOUS PRODUCTION OF NITROBENZENE
    338.
    发明申请
    METHOD FOR CONTINUOUS PRODUCTION OF NITROBENZENE 有权
    连续生产硝基苯的方法

    公开(公告)号:US20150073180A1

    公开(公告)日:2015-03-12

    申请号:US14240058

    申请日:2012-08-29

    Abstract: The invention relates to a method for producing nitrobenzene, in which crude nitrobenzene is first produced by nitrating benzene and said crude nitrobenzene is then washed in succession in at least one acid wash, in at least one alkaline wash and in at least one neutral wash, at least one additional wash with an aqueous solution of a potassium salt being interposed between the last alkaline wash and the first neutral wash.

    Abstract translation: 本发明涉及生产硝基苯的方法,其中首先通过硝化苯生产粗硝基苯,然后将所述粗硝基苯在至少一种酸洗涤液,至少一种碱性洗涤液和至少一种中性洗涤液中连续洗涤, 在最后的碱性洗涤和第一中性洗涤之间插入钾盐水溶液至少一次另外的洗涤。

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