METHOD FOR PRODUCING HIGHLY PURE MONOETHYLENE GLYCOL

    公开(公告)号:CA2345053C

    公开(公告)日:2008-07-15

    申请号:CA2345053

    申请日:1999-09-21

    Applicant: BASF AG

    Abstract: The invention relates to a method for obtaining highly pure monoethylene glycol from the product of hydrolysis of ethylene oxide by distillation, by means of dehydration under pressure, preferably in a cascade, vacuum dehydration and subsequent pure distillation. During the vacuum dehydration, an aqueous stream containing monoethylene glycol in a concentration of less than 1 wt. %, preferably less than 0.1 wt. %, medium boilers and light boilers is drawn off and then sluiced out, optionally after reprocessing.

    EVAPORATION OF OXIDATION-SENSITIVE COMPOUNDS AND EVAPORATOR FOR THIS PURPOSE

    公开(公告)号:CA2244271C

    公开(公告)日:2005-11-29

    申请号:CA2244271

    申请日:1997-01-20

    Applicant: BASF AG

    Abstract: The invention concerns a method of vaporizing a fluid containing vaporizable oxidation-sensitive compounds in a vaporizer in which, for vaporization purposes, the fluid is brought into contact with a heated solid surface, direct contact between the resultant vapour phase and the heated solid surface axing largely prevented. The invention further concerns a vaporizer comprising a heatable solid surface (16), a device (2, 3) for heating the solid surface, and a device (10) for feeding a fluid containing vaporizable compounds to the healable solid surface. The fluid-feeding device is designe d and disposed (12, 14, 18) in the vaporizer such that direct contact between the resultant vapour phase and the healable solid surface is largely prevented.

    36.
    发明专利
    未知

    公开(公告)号:DE19855910A1

    公开(公告)日:2000-06-08

    申请号:DE19855910

    申请日:1998-12-03

    Applicant: BASF AG

    Abstract: The rinsing apparatus for removing residue from the sump run-off of an evaporator comprises (a) a run-off container (7), (b) a collector container (8), (c) a run-off valve (10), (d) a rinsing water valve (11), (e) run-off container valve (12), (f) rinsing run-off valve (13), (g) vent valve (14), (h) a delivery pipe (17) from the sump to the run-off valve (10), (i) a inlet pipe (3) for the rinsing agent, (j) a run-off pipe device (6,16) and a connector to the devices (a) to (j). An Independent claim is included for the use of a rinsing apparatus.

    Method for producing highly pure monoethylene glycol

    公开(公告)号:AU6466399A

    公开(公告)日:2000-04-10

    申请号:AU6466399

    申请日:1999-09-21

    Applicant: BASF AG

    Abstract: A process for the distillative recovery of high purity monoethylene glycol from the hydrolysis product of ethylene oxide by pressure dewatering, vacuum dewatering and subsequent purifying distillation, which includes the pressure dewatering columns or at least the first pressure dewatering column of the battery (2, 3, 4) having a stripping section with at least one separating stage, preferably with from 2 to 10 separating stages, particularly preferably with from 3 to 6 stages, and a portion of the overhead stream of the pressure dewatering column(s) (2, 3, 4) having a stripping section being removed from the system.

    38.
    发明专利
    未知

    公开(公告)号:DE19843697A1

    公开(公告)日:2000-03-30

    申请号:DE19843697

    申请日:1998-09-23

    Applicant: BASF AG

    Abstract: The invention relates to a method for obtaining highly pure monoethylene glycol from the product of hydrolysis of ethylene oxide by distillation, by means of dehydration under pressure, preferably in a cascade, vacuum dehydration and subsequent pure distillation. During the vacuum dehydration, an aqueous stream containing monoethylene glycol in a concentration of less than 1 wt. %, preferably less than 0.1 wt. %, medium boilers and light boilers is drawn off and then sluiced out, optionally after reprocessing.

    39.
    发明专利
    未知

    公开(公告)号:DE19843652A1

    公开(公告)日:2000-03-30

    申请号:DE19843652

    申请日:1998-09-23

    Applicant: BASF AG

    Abstract: The invention relates to a method for obtaining highly pure monoethylene glycol from the product of hydrolysis of ethylene oxide by distillation, by means of dehydration under pressure, preferably in a cascade, vacuum dehydration and subsequent pure distillation. According to the inventive method, the pressure dehydration column or at least the first pressure dehydration column of the cascade (2, 3, 4) has a stripping section with at least one separation stage, preferably 2-10 separation stages, especially 3-6 stages, and in that part of the top flow of the dehydration column(s) (2, 3, 4) is sluiced out with the stripping section.

Patent Agency Ranking